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868540-16-3

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Basic Information
CAS No.: 868540-16-3
Name: (alphaS)-alpha-[(4-Morpholinylacetyl)aMino]benzenebutanoyl-L-leucyl-L-phenylalanine
Article Data: 7
Molecular Structure:
Molecular Structure of 868540-16-3 ((alphaS)-alpha-[(4-Morpholinylacetyl)aMino]benzenebutanoyl-L-leucyl-L-phenylalanine)
Formula: C31H42N4O6
Molecular Weight: 566.698
Synonyms: (alphaS)-alpha-[(4-Morpholinylacetyl)aMino]benzenebutanoyl-L-leucyl-L-phenylalanine;(alphaS) - alpha - [(4 - acetyl Morpholine base) aMino] benzene ding acyl - L - bright aMMonia acyl - L - phenylalanine;L-Phenylalanine, (αS)-α-[[2-(4-Morpholinyl)acetyl]aMino]benzenebutanoyl-L-leucyl-;(alphaS)-alpha-[(4-Morpholinylacetyl)aMino]benzene;(S)-2-((S)-4-Methyl-2-((S)-2-(2-MorpholinoacetaMido)-4-phenylbutanaMido)pentanaMido)-3-phenylpropanoic acid;Carfilzomib intermidate
EINECS: 1592732-453-0
Density: 1.190±0.06 g/cm3(Predicted)
Boiling Point: 865.6±65.0 °C(Predicted)
PSA: 137.07000
LogP: 2.88980
Related products
Synthetic route
875309-92-5

(S)-benzyl 2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido) pentanamido)-3-phenylpropanoate

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
With methanol; hydrogen; palladium 10% on activated carbon In ethyl acetate under 760.051 Torr; for 2h;
With palladium on activated charcoal; ammonium formate In methanol at 25 - 30℃; for 2h; Solvent; Reagent/catalyst;77 g
With 5 mol% Pd/C; hydrogen In methanol for 0.5h;
13139-15-6

N-tert-butoxycarbonyl-L-leucine

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
2.2: 0 - 20 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
3.2: 0 - 20 °C / Inert atmosphere
4.1: potassium iodide / tetrahydrofuran / Inert atmosphere
5.1: lithium hydroxide / methanol; water / 12 h / 0 - 5 °C
View Scheme
Multi-step reaction with 6 steps
1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
2: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
3: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
4: hydrogenchloride / ethyl acetate / 2 h / 25 - 30 °C
5: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
6: lithium hydroxide monohydrate; water / tetrahydrofuran / 3 h / 25 - 30 °C
View Scheme
Multi-step reaction with 4 steps
1.1: benzotriazol-1-ol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 - 30 °C
2.1: trifluoroacetic acid / dichloromethane / 2 h / 2 - 30 °C
2.2: 2 - 30 °C
3.1: trifluoroacetic acid / dichloromethane / 2 h / 2 - 30 °C
3.2: 2 - 30 °C
4.1: ammonium formate; palladium on activated charcoal / methanol / 2 h / 25 - 30 °C
View Scheme
Multi-step reaction with 5 steps
1.1: benzotriazol-1-ol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 - 30 °C
2.1: dichloromethane / 2 h / 0 - 30 °C
3.1: benzotriazol-1-ol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 0 - 30 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 2 h / 2 - 30 °C
4.2: 2 - 30 °C
5.1: ammonium formate; palladium on activated charcoal / methanol / 2 h / 25 - 30 °C
View Scheme
Multi-step reaction with 6 steps
1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / dichloromethane / 18 h / 20 °C
2: dichloromethane / 1 h / 20 °C
3: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / dichloromethane / 18 h / 20 °C
4: dichloromethane / 1 h / 20 °C
5: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / dichloromethane / 18 h / 20 °C
6: 5 mol% Pd/C; hydrogen / methanol / 0.5 h
View Scheme
2577-90-4

methyl (2S)-2-amino-3-phenylpropanoate

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
2.2: 0 - 20 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
3.2: 0 - 20 °C / Inert atmosphere
4.1: potassium iodide / tetrahydrofuran / Inert atmosphere
5.1: lithium hydroxide / methanol; water / 12 h / 0 - 5 °C
View Scheme
Multi-step reaction with 6 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
2: dichloromethane / 3 h / 0 - 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
4: dichloromethane / 3 h / 0 - 20 °C
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
6: lithium hydroxide monohydrate / methanol / 3 h / 0 - 20 °C
View Scheme
15136-32-0, 87976-66-7, 120342-25-8, 5874-73-7

(N-(tert-butoxycarbonyl)-L-leucinyl)-L-phenylalanine methyl ester

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
1.2: 0 - 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
2.2: 0 - 20 °C / Inert atmosphere
3.1: potassium iodide / tetrahydrofuran / Inert atmosphere
4.1: lithium hydroxide / methanol; water / 12 h / 0 - 5 °C
View Scheme
Multi-step reaction with 5 steps
1: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
2: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
3: hydrogenchloride / ethyl acetate / 2 h / 25 - 30 °C
4: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
5: lithium hydroxide monohydrate; water / tetrahydrofuran / 3 h / 25 - 30 °C
View Scheme
Multi-step reaction with 5 steps
1: dichloromethane / 3 h / 0 - 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
3: dichloromethane / 3 h / 0 - 20 °C
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
5: lithium hydroxide monohydrate / methanol / 3 h / 0 - 20 °C
View Scheme
868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
1.2: 0 - 20 °C / Inert atmosphere
2.1: potassium iodide / tetrahydrofuran / Inert atmosphere
3.1: lithium hydroxide / methanol; water / 12 h / 0 - 5 °C
View Scheme
Multi-step reaction with 3 steps
1: hydrogenchloride / ethyl acetate / 2 h / 25 - 30 °C
2: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
3: lithium hydroxide monohydrate; water / tetrahydrofuran / 3 h / 25 - 30 °C
View Scheme
Multi-step reaction with 3 steps
1: dichloromethane / 3 h / 0 - 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
3: lithium hydroxide monohydrate / methanol / 3 h / 0 - 20 °C
View Scheme
868540-08-3

C28H36ClN3O5

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium iodide / tetrahydrofuran / Inert atmosphere
2: lithium hydroxide / methanol; water / 12 h / 0 - 5 °C
View Scheme

C32H44N4O6

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
With lithium hydroxide In methanol; water at 0 - 5℃; for 12h;
With lithium hydroxide monohydrate; water In tetrahydrofuran at 25 - 30℃; for 3h;48.0 g
With lithium hydroxide monohydrate In methanol at 0 - 20℃; for 3h;
6461-07-0

(S)-methyl 2-((S)-2-amino-4-methylpentanamido)-3-phenylpropanoate hydrochloride

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
2: hydrogenchloride / ethyl acetate / 2 h / 25 - 30 °C
3: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
4: lithium hydroxide monohydrate; water / tetrahydrofuran / 3 h / 25 - 30 °C
View Scheme
82732-07-8, 108524-68-1, 142926-43-0, 100564-78-1

Boc-L-homophenylalanine

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
2: hydrogenchloride / ethyl acetate / 2 h / 25 - 30 °C
3: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
4: lithium hydroxide monohydrate; water / tetrahydrofuran / 3 h / 25 - 30 °C
View Scheme

(S)-methyl 2-((S)-2-((S)-2-amino-4-phenyIbutanamido)-4-methylpentanamido)-3-phenylpropanoate hydrochloride

868540-16-3

(S)-2-((S)-4-methyl-2-((S)-2-(2-morpholinoacetamido)-4-phenylbutanamido)pentanamido)-3-phenyipropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
2: lithium hydroxide monohydrate; water / tetrahydrofuran / 3 h / 25 - 30 °C
View Scheme
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  • (alphaS)-alpha-[(4-Morpholinylacetyl)amino]benzenebutanoyl-L-leucyl-L-phenylalanine

  • Casno:

    868540-16-3

    (alphaS)-alpha-[(4-Morpholinylacetyl)amino]benzenebutanoyl-L-leucyl-L-phenylalanine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

    As a member of TAIHO Group,Hubei Taiho Chemical Co.,Ltd,is a professional new-type chemicals enterprise combined into research and development,production and sales.We adhere to the

  •  Hubei Taiho Chemical Co.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-18120399543

    Address:No. 49 taifeng Road,Qianjiang City,Hubei,China

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  • (alphaS)-alpha-[(4-Morpholinylacetyl)aMino]benzenebutanoyl-L-leucyl-L-phenylalanine

  • Casno:

    868540-16-3

    (alphaS)-alpha-[(4-Morpholinylacetyl)aMino]benzenebutanoyl-L-leucyl-L-phenylalanine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • (alphaS)-alpha-[(4-Morpholinylacetyl)amino]benzenebutanoyl-L-leucyl-L-phenylalanine

  • Casno:

    868540-16-3

    (alphaS)-alpha-[(4-Morpholinylacetyl)amino]benzenebutanoyl-L-leucyl-L-phenylalanine

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food, cosmetics and other fine chemicals. Our products including but not li

    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food,

  •  Koning Pharmchem Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-574-87369228

    Address:Lingqiao Road

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