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Basic Information
CAS No.: 915095-84-0
Name: (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone
Article Data: 9
Molecular Structure:
Molecular Structure of 915095-84-0 ((S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone)
Formula: C17H14BrClO3
Molecular Weight: 381.653
Synonyms: (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone;(5-Bromo-2-chlorophenyl)[4-[[(3S)-tetrahydro-3-furanyl]oxy]phenyl]methanone
Density: 1.493±0.06 g/cm3(Predicted)
Boiling Point: 505.1±50.0 °C(Predicted)
PSA: 35.53000
LogP: 4.50120
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915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 100 - 110℃;93%
With potassium tert-butylate In tetrahydrofuran at 7 - 10℃; for 0.5h;87%
With potassium tert-butylate In tetrahydrofuran at 0 - 10℃; for 2h;85.3%
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(5-bromo-2-chlorophenyl)(4-hydroxyphenyl)methanone

R-3-chloro-tetrahydrofuran

915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In acetonitrile at 50 - 55℃;91%
21739-92-4

5-bromo-2-chlorobenzoic acid

915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / fluorobenzene / 2 h / 15 - 25 °C
2: aluminum (III) chloride / 1 h / 0 - 25 °C
3: potassium tert-butylate / tetrahydrofuran / 0.5 h / 7 - 10 °C
View Scheme
Multi-step reaction with 3 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / fluorobenzene / 15 - 25 °C / Inert atmosphere
2: aluminum (III) chloride / 25 °C / Inert atmosphere
3: potassium tert-butylate / tetrahydrofuran / 2 - 10 °C
View Scheme
Multi-step reaction with 2 steps
1: polyphosphoric acid / 50 - 85 °C
2: potassium iodide; potassium carbonate / acetonitrile / 50 - 55 °C
View Scheme
21900-52-7

5-bromo-2-chloro-benzoyl chloride

915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 1 h / 0 - 25 °C
2: potassium tert-butylate / tetrahydrofuran / 0.5 h / 7 - 10 °C
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 25 °C / Inert atmosphere
2: potassium tert-butylate / tetrahydrofuran / 2 - 10 °C
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 5 h / 0 - 20 °C
2: potassium tert-butylate / tetrahydrofuran / 2 h / 0 - 10 °C
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 8 h / 0 - 10 °C
2: 18-crown-6 ether; sodium hydroxide / toluene; water / 8 h / 50 - 60 °C
View Scheme
108-95-2

phenol

915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: polyphosphoric acid / 50 - 85 °C
2: potassium iodide; potassium carbonate / acetonitrile / 50 - 55 °C
View Scheme
462-06-6

fluorobenzene

915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide; oxalyl dichloride / 0 - 25 °C
1.2: 25 °C
2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 7 - 10 °C
View Scheme
915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

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(S)-4-bromo-1-chloro-2-(4-tetrahydrofuran-3-yloxy-benzyl)benzene

Conditions
ConditionsYield
With aluminum (III) chloride; hydrogen In toluene at 20 - 25℃; for 3h; Temperature;95%
With aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane In toluene at 0 - 23℃; for 2.5h;92%
With aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane In toluene at 0 - 23℃;91.28%
915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

C17H16BrClO3

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol at 20 - 25℃;98 g
915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

C20H24BrClO3Si

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / ethanol / 20 - 25 °C
2: triethylamine / dichloromethane / 0 - 35 °C
View Scheme
915095-84-0

(S)-(5-bromo-2-chlorophenyl)(4-((tetrahydrofuran-3-yl)oxy)phenyl)methanone

C18H18BrClO3

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / ethanol / 20 - 25 °C
2: methanesulfonic acid / 20 - 30 °C
View Scheme
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  • (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone

  • Casno:

    915095-84-0

    (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone

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    J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

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  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

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    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food, cosmetics and other fine chemicals. Our products including but not li

    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food,

  •  Koning Pharmchem Co., Ltd.

    China (Mainland)  |  Contact Details

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  • (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone

  • Casno:

    915095-84-0

    (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

    Wuhan Circle Star Bio-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of nin

  •  Wuhan Circle Star Chem-medical Technology co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

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  • (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone

  • Casno:

    915095-84-0

    (S)-(5-broMo-2-chlorophenyl)(4-(tetrahydrofuran-3-yloxy)phenyl)Methanone

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:intermediate

    HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou . We are a high-tech enterprise specialized in technical research and development, produc

  •  HANGZHOU TIANYE CHEMICALS CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:1208# HuaCe Building-B,Wuchanggang Road,XIHU District,Hangzhou City,Zhejiang Province ,China

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