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| CAS No.: | 917-64-6 |
|---|---|
| Name: | METHYLMAGNESIUM IODIDE |
| Article Data: | 59 |
| Molecular Structure: | |
|
|
|
| Formula: | CH3 I Mg |
| Molecular Weight: | 166.244 |
| Synonyms: | Methylmagnesiumiodide (6CI);Iodomethylmagnesium;methylmagnesium iodine; |
| EINECS: | 213-031-1 |
| Density: | g/cm3 |
| Boiling Point: | °Cat760mmHg |
| Flash Point: | °C |
| Hazard Symbols: |
 
|
| Risk Codes: | 12-14/15-22-34-66-67 |
| Safety: | Toxic. Explosive reaction with thiophosphoryl chloride or vanadium trichloride. A Grignard reagent. When heated to decomposition it emits toxic fumes of I−. See also IODIDES and MAGNESIUM COMPOUNDS. |
| PSA: | 0.00000 |
| LogP: | 1.46950 |
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| Conditions | Yield |
|---|---|
| With magnesium In diethyl ether at 25℃; under 5171.62 Torr; Inert atmosphere; Flow reactor; | 94% |
| With magnesium In diethyl ether | |
| With magnesium In solid matrix at -258.2℃; |
| Conditions | Yield |
|---|---|
| Katalytischer Einfluss; |
| Conditions | Yield |
|---|---|
| With diethyl ether |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran; diethyl ether at -78 - 20℃; Nitrogen atmosphere; | 100% |
| With diethyl ether |
- 917-64-6
methyl magnesium iodide
- 7044-91-9
9,10-diformylanthracene
- 101789-38-2
9,10-bis(1-hydroxymethyl)anthracene
| Conditions | Yield |
|---|---|
| In tetrahydrofuran; diethyl ether at 40℃; for 8h; | 100% |
| In tetrahydrofuran; diethyl ether at 20℃; for 18h; | 100% |
- 917-64-6
methyl magnesium iodide
- 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde
- 5293-52-7
6-bromo-3,4-dimethoxy-α-methylbenzyl alcohol
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; for 0.5h; | 100% |
| In tetrahydrofuran; diethyl ether for 1h; Heating; | 100% |
| In diethyl ether at 0 - 20℃; for 3h; Inert atmosphere; | 90% |
| In diethyl ether at 20℃; for 0.5h; |
- 917-64-6
methyl magnesium iodide
- 93860-79-8
7β-acetyl-4aβ-methyl-1aα-decahydrocyclopropanaphthalene
- 71962-31-7
(+)-7β-(1-hydroxy-1-methylethyl)-4aB-methyl-1aα-decahydrocyclopropanaphthalene
| Conditions | Yield |
|---|---|
| In diethyl ether for 2h; Ambient temperature; | 100% |
- 917-64-6
methyl magnesium iodide
- 24306-23-8
methyl 4-(4-methylphenyl)butanoate
- 22184-00-5
2-(methyl-5-(4-methylphenyl))-2-pentanol
| Conditions | Yield |
|---|---|
| In diethyl ether for 24h; Ambient temperature; | 100% |
- 917-64-6
methyl magnesium iodide
- 61203-53-0
2-iodo-4,5-dimethoxybenzaldehyde
| Conditions | Yield |
|---|---|
| In tetrahydrofuran; diethyl ether for 1h; Heating; | 100% |
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Chemistry
The Molecular Structure of Magnesium, iodomethyl- (CAS NO.917-64-6):
Molecular Formula: CH3IMg
Molecular Weight: 166.24
Density: 1.26 g/mL at 20 °C
Product Categories: Classes of Metal Compounds;Grignard Reagents;Grignard Reagents & Alkyl Metals;Mg (Magnesium) Compounds;Synthetic Organic Chemistry;Typical Metal Compounds;AlkylChemical Synthesis;Grignard Reagents;Organic Bases;Organometallic Reagents;Synthetic Reagents
ACD/LogP: 1.09
ACD/LogD (pH 5.5): 1.09
ACD/LogD (pH 7.4): 1.09
ACD/BCF (pH 5.5): 3.97
ACD/BCF (pH 7.4): 3.97
ACD/KOC (pH 5.5): 93.32
ACD/KOC (pH 7.4): 93.32
Enthalpy of Vaporization: 8.17 kJ/mol
Vapour Pressure: 205000 mmHg at 25°C
Safety Profile
Toxic. Explosive reaction with thiophosphoryl chloride or vanadium trichloride. A Grignard reagent. When heated to decomposition it emits toxic fumes of I−. See also IODIDES and MAGNESIUM COMPOUNDS.
Hazard Codes:
F+,
C
Risk Statements: 12-14/15-22-34-66-67
R12:Extremely flammable
R14/15: Reacts violently with water, liberating extremely flammable gases
R22: Harmful if swallowed
R34: Causes burns
R66: Repeated exposure may cause skin dryness or cracking
R67: Vapours may cause drowsiness and dizziness
Safety Statements: 16-26-36/37/39-43-45-7/8
S16: Keep away from sources of ignition
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice|
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S43: In case of fire use ... (there follows the type of fire-fighting equipment to be used.)
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
7/8: Keep container tightly closed and dry
RIDADR: UN 3399 4.3/PG 1
WGK Germany: 1
F: 1-3-10
F1: Sensitive to air and humidity
F3: Hygroscopic
F10: Keep under argon
HazardClass: 4.2
PackingGroup: I
Specification
Magnesium, iodomethyl- (CAS NO.917-64-6) is also called as Iodomethylmagnesium ; Magnesium, iodomethyl- .