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917-64-6

Basic Information
CAS No.: 917-64-6
Name: Magnesium, iodomethyl-
Molecular Structure:
Molecular Structure of 917-64-6 (Magnesium, iodomethyl-)
Formula: CH3 I Mg
Molecular Weight: 166.25
Synonyms: Methylmagnesiumiodide (6CI);Iodomethylmagnesium;methylmagnesium iodine;
EINECS: 213-031-1
Density: g/cm3
Melting Point:
Boiling Point: °Cat760mmHg
Flash Point: °C
Solubility:
Appearance:
Hazard Symbols:
Risk Codes: 12-14/15-22-34-66-67
Safety: Toxic. Explosive reaction with thiophosphoryl chloride or vanadium trichloride. A Grignard reagent. When heated to decomposition it emits toxic fumes of I. See also IODIDES and MAGNESIUM COMPOUNDS.
Transport Information:
PSA: 0.00000
LogP: 1.46950
Synthetic route
74-88-4

methyl iodide

917-64-6

methyl magnesium iodide

Conditions
ConditionsYield
With magnesium In diethyl ether at 25℃; under 5171.62 Torr; Inert atmosphere; Flow reactor;94%
With magnesium In diethyl ether
With magnesium In solid matrix at -258.2℃;
142-68-7

TETRAHYDROPYRANE

917-64-6

methyl magnesium iodide

Conditions
ConditionsYield
Katalytischer Einfluss;
60-29-7

diethyl ether

74-88-4

methyl iodide

magnesium

magnesium

917-64-6

methyl magnesium iodide

74-88-4

methyl iodide

magnesium

magnesium

917-64-6

methyl magnesium iodide

Conditions
ConditionsYield
With diethyl ether
4363-93-3

quinoline-4-carboxaldehyde

917-64-6

methyl magnesium iodide

55908-34-4

1-Quinolin-4-yl-ethanol

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at -78 - 20℃; Nitrogen atmosphere;100%
With diethyl ether
917-64-6

methyl magnesium iodide

7044-91-9

9,10-diformylanthracene

101789-38-2

9,10-bis(1-hydroxymethyl)anthracene

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at 40℃; for 8h;100%
In tetrahydrofuran; diethyl ether at 20℃; for 18h;100%
917-64-6

methyl magnesium iodide

5392-10-9

2-bromo-4,5-dimethoxybenzaldehyde

5293-52-7

6-bromo-3,4-dimethoxy-α-methylbenzyl alcohol

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 0.5h;100%
In tetrahydrofuran; diethyl ether for 1h; Heating;100%
In diethyl ether at 0 - 20℃; for 3h; Inert atmosphere;90%
In diethyl ether at 20℃; for 0.5h;
917-64-6

methyl magnesium iodide

93860-79-8

7β-acetyl-4aβ-methyl-1aα-decahydrocyclopropanaphthalene

71962-31-7

(+)-7β-(1-hydroxy-1-methylethyl)-4aB-methyl-1aα-decahydrocyclopropanaphthalene

Conditions
ConditionsYield
In diethyl ether for 2h; Ambient temperature;100%
917-64-6

methyl magnesium iodide

24306-23-8

methyl 4-(4-methylphenyl)butanoate

22184-00-5

2-(methyl-5-(4-methylphenyl))-2-pentanol

Conditions
ConditionsYield
In diethyl ether for 24h; Ambient temperature;100%
917-64-6

methyl magnesium iodide

61203-53-0

2-iodo-4,5-dimethoxybenzaldehyde

4-iodo-5-(1-hydroxyethyl)veratrole

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 1h; Heating;100%
917-64-6

methyl magnesium iodide

3558-68-7

2,6-diphenylpyrylium perchlorate

55696-71-4

4-methyl-2,6-diphenyl-4H-pyran

Conditions
ConditionsYield
With copper(l) iodide In diethyl ether at -15 - -10℃;100%
In diethyl ether for 2h; Ambient temperature;94%
In diethyl ether at 20℃; Inert atmosphere;790 mg
917-64-6

methyl magnesium iodide

81805-47-2

6,9-dimethylnaphtho<1,8-bc>pyran-3(2H)-one

107686-35-1

3,6,9-trimethyl-2,3-dihydronaphtho<1,8-bc>pyran-3-ol

Conditions
ConditionsYield
In diethyl ether for 1h; Ambient temperature;100%
Yield given;
917-64-6

methyl magnesium iodide

86253-84-1

methyl 2-(2,6-dimethoxy-4-pentylphenyl)-3-methoxy-4-methylbenzoate

86253-85-2

6'-(1-hydroxy-1-methylethyl)-2,2',6-trimethoxy-3'-methyl-4-pentylbiphenyl

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 1.16667h; Heating;100%
917-64-6

methyl magnesium iodide

68781-89-5, 123930-74-5, 129569-63-7, 146727-49-3

exo-4,5-epoxy-endo-tricyclo[5.2.1.02,6]dec-8-en-3-one

135441-20-2

endo-4,5-epoxy-exo-5-methyl-endo-tricyclo<5.2.1.02,6>dec-8-en-exo-3-ol

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 72h;100%
917-64-6

methyl magnesium iodide

139592-64-6

methyl 2-(2-bromophenyl)pent-4-enoate

139592-68-0

3-(o-bromophenyl)-2-methylhex-5-en-2-ol

Conditions
ConditionsYield
In diethyl ether for 2h; Heating;100%
917-64-6

methyl magnesium iodide

101472-25-7

(2R,4S)-4-Methyl-tricyclo[11.2.2.25,8]nonadeca-1(16),5(19),6,8(18),13(17),14-hexaene-2-carbaldehyde

101472-33-7

cis-1-(1-hydroxyethyl)-3-methyl<3.4>paracyclophane

Conditions
ConditionsYield
In diethyl ether100%
917-64-6

methyl magnesium iodide

145513-97-9

(S)-(+)-2-phenyl-N-(trifluoroacetyl)glycine methyl ester

145439-97-0

(S)-2,2,2-trifluoro-N-[2-hydroxy-2-methyl-1-phenylpropyl]acetamide

Conditions
ConditionsYield
Stage #1: methyl magnesium iodide; (S)-(+)-2-phenyl-N-(trifluoroacetyl)glycine methyl ester In diethyl ether at 20℃; for 16h;
Stage #2: With water; ammonium chloride In diethyl ether
100%
at 23℃; for 2.5h;90%
917-64-6

methyl magnesium iodide

345976-80-9, 84021-69-2, 84048-79-3

9-(2-acetyl-1-naphthyl)fluorene

148648-28-6

9-<2-(1-hydroxy-1-methylethyl)-1-naphthyl>fluorene

Conditions
ConditionsYield
In diethyl ether for 1.5h;100%
917-64-6

methyl magnesium iodide

95512-49-5

1-acetyl-9,9-bis(methylthio)fluorene

65223-17-8

9,9-bis(methylthio)-α,α-dimethyl-1-fluorenemethanol

Conditions
ConditionsYield
100%
917-64-6

methyl magnesium iodide

4445-36-7

6H-benzo[c]thiochromen-6-one

87221-18-9

6-methyl-6H-dibenzo-thiopyran-6-ol

Conditions
ConditionsYield
In tetrahydrofuran for 0.5h; Heating;100%
917-64-6

methyl magnesium iodide

171-74-4

Spiroindole>

97961-94-9

2'-methylspiro

Conditions
ConditionsYield
With copper(I) chloride In toluene at 120℃; for 2h;100%
917-64-6

methyl magnesium iodide

167367-79-5

2-[(E)-3-(tert-Butyl-dimethyl-silanyloxy)-4,4-dimethyl-pent-1-enyl]-benzaldehyde

1-{2-[(E)-3-(tert-Butyl-dimethyl-silanyloxy)-4,4-dimethyl-pent-1-enyl]-phenyl}-ethanol

Conditions
ConditionsYield
In diethyl ether100%
917-64-6

methyl magnesium iodide

183549-74-8

3-(7,7-Dimethyl-1,4-dioxa-spiro[4.5]dec-6-yl)-propionaldehyde

183549-76-0

4-(7,7-Dimethyl-1,4-dioxa-spiro[4.5]dec-6-yl)-butan-2-ol

Conditions
ConditionsYield
100%
917-64-6

methyl magnesium iodide

828932-99-6

4-benzyloxy-5,6,8-trimethoxy-3-(prop-2'-enyl)naphthalene-2-carbaldehyde

828933-03-5

4-benzyloxy-2-(1''-hydroxyethyl)-5,6,8-trimethoxy-3-(prop-2'-enyl)-naphthalene

Conditions
ConditionsYield
With methyl iodide In diethyl ether at 25℃; for 1h;100%
847469-01-6

(R)-2-(2-(benzyloxy)-1-phenylethyl)isoindoline-1,3-dione

917-64-6

methyl magnesium iodide

847469-02-7

2-((R)-2-Benzyloxy-1-phenyl-ethyl)-3-hydroxy-3-methyl-2,3-dihydro-isoindol-1-one

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at -10℃; for 4h;100%
917-64-6

methyl magnesium iodide

92862-87-8

(rac)-3-(4-methylphenyl)-3-methylcyclohexanone

(1S,3R)-1,3-Dimethyl-3-p-tolyl-cyclohexanol

Conditions
ConditionsYield
In diethyl ether at 0℃; for 0.5h;100%
917-64-6

methyl magnesium iodide

26218-75-7

methyl 6-Bromopicolinate

638218-78-7

2-(6-bromopyridin-2- yl)propan-2-ol

Conditions
ConditionsYield
In diethyl ether at 20℃; for 0.5h; Inert atmosphere;100%
In diethyl ether at 20℃; for 0.0833333h; Inert atmosphere;85%
In diethyl ether at 20℃; for 0.0833333h; Inert atmosphere;85%
917-64-6

methyl magnesium iodide

218780-54-2

ethyl [1-(methylsulfonyl)piperidin-4-ylidenyl]cyanoacetate

218780-55-3

ethyl [4-methyl-1-(methylsulfonyl)piperidin-4-yl]cyanoacetate

Conditions
ConditionsYield
With copper(l) chloride In tetrahydrofuran; diethyl ether at 0 - 20℃; for 3h;100%
917-64-6

methyl magnesium iodide

42460-90-2

(S)-Pyrrolidine-2-carboxylic acid methyl ester; compound with trifluoro-acetic acid

672324-99-1

C2HF3O2*C7H15NO

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at 0 - 25℃; for 16h;100%
917-64-6

methyl magnesium iodide

656257-69-1

2-bromo-N-methyl-N-(methyloxy)-4-pyridinecarboxamide

111043-06-2

1-(2-bromo-4-pyridinyl)ethanone

Conditions
ConditionsYield
Stage #1: methyl magnesium iodide; 2-bromo-N-methyl-N-(methyloxy)-4-pyridinecarboxamide In tetrahydrofuran; diethyl ether at 0 - 5℃; for 2h;
Stage #2: With water; ammonium chloride In tetrahydrofuran; diethyl ether
100%
917-64-6

methyl magnesium iodide

40320-60-3

N-benzhydryl 3-azetidinone

40320-63-6

1-benzhydryl-3-methylazetidin-3-ol

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at 0℃; for 1h;100%
Stage #1: methyl magnesium iodide; N-benzhydryl 3-azetidinone In diethyl ether at 0℃; for 1h; Grignard Reaction;
Stage #2: With methanol In diethyl ether; dichloromethane
68%
917-64-6

methyl magnesium iodide

12181-92-9, 71327-35-0, 36249-94-2

(+)-(1S)-tricarbonyl(2-methoxybenzaldehyde)chromium

(1S)-o-CH3OC6H4CHOHCH3-(S)-Cr(CO)3

Conditions
ConditionsYield
In tetrahydrofuran -78°C.;100%
917-64-6

methyl magnesium iodide

210223-43-1

(2,2'-ethylenebis(N,N'-(triisopropylsilyl)anilido))ZrCl2

(2,2'-ethylenebis(N,N'-(triisopropylsilyl)anilido))ZrMe2

Conditions
ConditionsYield
In not given elem. anal.;100%
917-64-6

methyl magnesium iodide

1204978-36-8

(R)-4-(6-chloro-4,5-dimethyl-pyridazin-3-yl)-2-methyl-3,4,5,6-tetrahydro-2H-[1,2']bipyrazinyl-5'-carboxylic acid methyl ester

2-[(R)-4-(6-Chloro-4,5-dimethyl-pyridazin-3-yl)-2-methyl-3,4,5,6-tetrahydro-2H-[1,2']bipyrazinyl-5'-yl]-propan-2-ol

Conditions
ConditionsYield
Stage #1: methyl magnesium iodide; (R)-4-(6-chloro-4,5-dimethyl-pyridazin-3-yl)-2-methyl-3,4,5,6-tetrahydro-2H-[1,2']bipyrazinyl-5'-carboxylic acid methyl ester In tetrahydrofuran; diethyl ether at -78 - 0℃;
Stage #2: With water; ammonium chloride In tetrahydrofuran; diethyl ether
100%
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    METHYLMAGNESIUM IODIDE

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    Product Name: METHYLMAGNESIUM IODIDE CAS: 917-64-6 MF: CH3IMg MW: 166.24 EINECS: 213-031-1 Mol File: 917-64-6.mol METHYLMAGNESIUM IODIDE Structure METHYLMAGNESIUM IODIDE Chemical Properties density 1.26 g/mL at 20 °C Fp

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    Magnesium, iodomethyl-

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    Methylmagnesium iodide

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  • Magnesium, iodomethyl-CAS NO.: 917-64-6

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    Magnesium, iodomethyl-CAS NO.: 917-64-6

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  • methylmagnesium iodide

  • Casno:

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    methylmagnesium iodide

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Chemistry

The Molecular Structure of Magnesium, iodomethyl- (CAS NO.917-64-6):
Molecular Formula: CH3IMg
Molecular Weight: 166.24  
Density: 1.26 g/mL at 20 °C
Product Categories: Classes of Metal Compounds;Grignard Reagents;Grignard Reagents & Alkyl Metals;Mg (Magnesium) Compounds;Synthetic Organic Chemistry;Typical Metal Compounds;AlkylChemical Synthesis;Grignard Reagents;Organic Bases;Organometallic Reagents;Synthetic Reagents
ACD/LogP: 1.09  
ACD/LogD (pH 5.5): 1.09 
ACD/LogD (pH 7.4): 1.09 
ACD/BCF (pH 5.5): 3.97 
ACD/BCF (pH 7.4): 3.97 
ACD/KOC (pH 5.5): 93.32 
ACD/KOC (pH 7.4): 93.32  
Enthalpy of Vaporization: 8.17 kJ/mol  
Vapour Pressure: 205000 mmHg at 25°C 

Safety Profile

Toxic. Explosive reaction with thiophosphoryl chloride or vanadium trichloride. A Grignard reagent. When heated to decomposition it emits toxic fumes of I. See also IODIDES and MAGNESIUM COMPOUNDS.
Hazard Codes:HighlyF+,CorrosiveC
Risk Statements: 12-14/15-22-34-66-67
R12:Extremely flammable
R14/15: Reacts violently with water, liberating extremely flammable gases 
R22: Harmful if swallowed
R34: Causes burns
R66: Repeated exposure may cause skin dryness or cracking
R67: Vapours may cause drowsiness and dizziness
Safety Statements: 16-26-36/37/39-43-45-7/8
S16: Keep away from sources of ignition
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice|
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S43: In case of fire use ... (there follows the type of fire-fighting equipment to be used.) 
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
7/8: Keep container tightly closed and dry
RIDADR: UN 3399 4.3/PG 1
WGK Germany: 1
F: 1-3-10
F1: Sensitive to air and humidity
F3: Hygroscopic
F10: Keep under argon
HazardClass: 4.2
PackingGroup: I

Specification

 Magnesium, iodomethyl- (CAS NO.917-64-6) is also called as Iodomethylmagnesium ; Magnesium, iodomethyl- .