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919-30-2

Basic Information
CAS No.: 919-30-2
Name: 3-Aminopropyltriethoxysilane
Molecular Structure:
Molecular Structure of 919-30-2 (3-Aminopropyltriethoxysilane)
Formula: C9H23NO3Si
Molecular Weight: 221.37
Synonyms: gamma-Aminopropyltriethoxysilane;(3-Aminopropyl)triethoxysilane;(gamma-Aminopropyl)triethoxysilane;1-Propanamine, 3-(triethoxysilyl)-;3-(Triethoxysilyl)-1-propanamine;3-Aminopropyltriethoxysilane;4-04-00-04273 (Beilstein Handbook Reference);A 1100;A 1112;AGM-9;APTES;BRN 1754988;HSDB 5767;NSC 95428;Nuca 1100;Propylamine, 3-(triethoxysilyl)-;Silane 1100;Silane amg-9;Silane, (3-aminopropyl)triethoxy-;Silane, gamma-aminopropyltriethoxy-;Silicone A-1100;Triethoxy(3-aminopropyl)silane;Uc-A 1100;3-(Triethoxysilyl)propylamine;γ-Aminopropyltriethoxysilane;
EINECS: 213-048-4
Density: 0.939 g/cm3
Melting Point: -70 °C
Boiling Point: 222.1 °C at 760 mmHg
Flash Point: 104.4 °C
Solubility: reacts with water
Appearance: colorless transparent liquid
Hazard Symbols: CorrosiveC
Risk Codes: 22-34
Safety: 26-36/37/39-45
Transport Information: UN 2735 8/PG 2
PSA: 53.71000
LogP: 2.08390
Synthetic route

C12H27NO3Si

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
In water at 65 - 75℃; for 3h; Concentration; Temperature;98%
1310-73-2

sodium hydroxide

rhodium(III) chloride trihydrate

998-30-1

Triethoxysilane

107-11-9

1-amino-2-propene

A

53218-21-6

beta-aminopropyl triethoxy silane

B

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
In 5,5-dimethyl-1,3-cyclohexadieneA 90%
B n/a
5089-70-3

(3-chloropropyl)triethoxysilane

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
With ammonia81%
With ammonia
With ammonia
998-30-1

Triethoxysilane

107-11-9

1-amino-2-propene

A

53218-21-6

beta-aminopropyl triethoxy silane

B

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
In para-xyleneA 81%
B n/a
In tolueneA 78%
B n/a
In tolueneA 78%
B n/a
998-30-1

Triethoxysilane

107-11-9

1-amino-2-propene

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
75%
rhodium hydride carbonyl-tris(triphenylphosphine)34%
rhodium hydride carbonyl-tris(triphenylphosphine)34%
With rhodium(III) trichloride hydrate; triphenylphosphine at 95℃;
1552-12-1, 111-78-4

1,5-cis,cis-cyclooctadiene

998-30-1

Triethoxysilane

107-11-9

1-amino-2-propene

A

53218-21-6

beta-aminopropyl triethoxy silane

B

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
In 5,5-dimethyl-1,3-cyclohexadieneA 75%
B n/a
In 5,5-dimethyl-1,3-cyclohexadieneA 75%
B n/a
998-30-1

Triethoxysilane

107-11-9

1-amino-2-propene

A

78-10-4

tetraethoxy orthosilicate

B

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
With dihydrogen hexachloroplatinate; 7,8-dicarba-nido-undecaborate(1-) for 10h; Product distribution; Heating; other reaction time, various catalyst composition, other catalysts;A 11.1%
B 69.9%
With dihydrogen hexachloroplatinate; 7,8-dicarba-nido-undecarborate(1-) for 10h;A 11.1%
B 69.9%
10519-97-8

allylamino-trimethyl-silane

998-30-1

Triethoxysilane

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
With dihydrogen hexachloroplatinate; ethanol
919-31-3

2-cyanoethyltriethoxysilane

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
With nickel Hydrogenation;
998-30-1

Triethoxysilane

107-11-9

1-amino-2-propene

A

919-30-2

3-aminopropyltriethoxysilane

B

36957-84-3

(2-amino-1-methylethyl)triethoxysilane

Conditions
ConditionsYield
With Allyl glycidyl ether; dihydrogen hexachloroplatinate; isopropyl alcohol for 13h; Product distribution; Mechanism; influence unsaturated Si-comp. on rate of hydrosilylation; effect of other additives;A 74.8 % Chromat.
B n/a
With (dicyclopentadiene)platinum(II) dichloride at 85℃; for 20h; Inert atmosphere; Schlenk technique; Overall yield = 84 %Spectr.;
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex at 80℃; for 20h; Schlenk technique; Inert atmosphere; Overall yield = 94.2 %Spectr.; regioselective reaction;
5089-70-3

(3-chloropropyl)triethoxysilane

A

919-30-2

3-aminopropyltriethoxysilane

B

bis-<3-triethoxysilanyl-propyl>-amine and tris-<3-triethoxysilanyl-propyl>-amine

bis-<3-triethoxysilanyl-propyl>-amine and tris-<3-triethoxysilanyl-propyl>-amine

Conditions
ConditionsYield
With ammonia
64-17-5

ethanol

C11H27NO4Si

A

110-80-5

2-ethoxy-ethanol

B

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
at 20℃; Kinetics; Equilibrium constant;

2,2-diethoxy-1,2-azasilolidine

64-17-5

ethanol

919-30-2

3-aminopropyltriethoxysilane

140236-87-9

3-(triethoxysilyl)propylammonium 3-(triethoxysilyl)propylcarbamate

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
at 120℃; for 2h;
at 69℃;
64-17-5

ethanol

C3H11NSi*TiO2

919-30-2

3-aminopropyltriethoxysilane

Conditions
ConditionsYield
With hydrogenchloride In water for 1h;
919-30-2

3-aminopropyltriethoxysilane

162435-10-1

<3-(2-Pyridyl)-1-pyrazolyl>essigsaeure-ethylester

N-(3-triethoxysilylpropyl)-[3-(2-pyridyl)-1-pyrazolyl]acetamide

Conditions
ConditionsYield
at 150℃; for 2h;100%
In tetrahydrofuran at 150℃; for 2h;
108-31-6

maleic anhydride

919-30-2

3-aminopropyltriethoxysilane

(E)-butenedioic acid 3-(triethoxysilyl)propylamide

Conditions
ConditionsYield
100%
at 50 - 60℃;99%
919-30-2

3-aminopropyltriethoxysilane

107-13-1

acrylonitrile

13497-26-2

N-(3-triethoxysilylpropyl)-3-aminopropanenitrile

Conditions
ConditionsYield
In tetrahydrofuran at 40℃; for 4h;100%
at 120℃; for 6h;65%
1942-45-6

4-Octyne

919-30-2

3-aminopropyltriethoxysilane

853411-25-3

(1-propylpent-1-enyl)phosphinic acid ethyl ester

Conditions
ConditionsYield
With hypophosphorous acid; trifluoroacetic acid; nickel dichloride In acetonitrile for 13h; Heating;100%
919-30-2

3-aminopropyltriethoxysilane

556-52-5

oxiranyl-methanol

Gly-APTES

Conditions
ConditionsYield
at 0 - 50℃; for 1h;100%
2598-30-3

8-hydroxyquinoline-5-carbaldehyde

919-30-2

3-aminopropyltriethoxysilane

5-(CHN(CH2)3Si(OC2H5)3)-8-hydroxyquinoline

Conditions
ConditionsYield
In ethanol for 12h; Heating;100%
919-30-2

3-aminopropyltriethoxysilane

112-96-9

octadecyl isocyanate

106868-86-4

N-octadecyl-N'-(3-triethoxysilyl)propyl urea

Conditions
ConditionsYield
100%
In chloroform for 12h; Reflux;82%
919-30-2

3-aminopropyltriethoxysilane

27742-33-2

3,6-epoxy-N-phenyl-1,2,3,6-tetrahydrophthalimide

N-(propyltriethoxysilane)maleimide-furan adduct

Conditions
ConditionsYield
Stage #1: 3-aminopropyltriethoxysilane; 3,6-epoxy-N-phenyl-1,2,3,6-tetrahydrophthalimide In toluene at 20℃; for 12h;
Stage #2: With 1,2-dichloro-benzene at 140℃; for 5h;
100%

2,7,12,17-tetra-n-propylporphycene-3-sulfonyl chloride

919-30-2

3-aminopropyltriethoxysilane

C41H59N5O5SSi

Conditions
ConditionsYield
In dichloromethane at 20℃; for 1h;100%
108-30-5

succinic acid anhydride

919-30-2

3-aminopropyltriethoxysilane

32267-20-2

4-oxo-4-((3-(triethoxysilyl)propyl)amino)butanoic acid

Conditions
ConditionsYield
In tetrahydrofuran100%
In tetrahydrofuran at -5 - 5℃; for 6h; Inert atmosphere;99%
In 1,4-dioxane at 20℃; for 1h; Inert atmosphere;94%
919-30-2

3-aminopropyltriethoxysilane

17527-29-6

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-propenoate

497841-73-3

C31H37F26NO7Si

Conditions
ConditionsYield
In ethanol at 60℃; for 5h;100%
919-30-2

3-aminopropyltriethoxysilane

56281-05-1

acrylic acid 3,3,5,5,6,6,7,7,8,8,8-undecafluoro-octyl ester

1159854-22-4

C31H41F22NO7Si

Conditions
ConditionsYield
In ethanol at 60℃; for 5h;100%
919-30-2

3-aminopropyltriethoxysilane

1030617-61-8

acrylic acid 3,3,4,4-tetrafluoro-4-heptafluoropropyloxy-butyl ester

1159854-27-9

C29H37F22NO9Si

Conditions
ConditionsYield
In ethanol at 60℃; for 5h; Michael Addition;100%
49676-59-7

acrylic acid 3,3,5,5,6,6,7,7,8,8,9,9,10,10,10-pentadecafluoro-decyl ester

919-30-2

3-aminopropyltriethoxysilane

1159854-25-7

C35H41F30NO7Si

Conditions
ConditionsYield
In ethanol at 60℃; for 5h;100%
932747-91-6

acrylic acid 3,3,5,5,7,7,8,8,9,9,10,10,10-tridecafluoro-decyl ester

919-30-2

3-aminopropyltriethoxysilane

1159854-26-8

C35H45F26NO7Si

Conditions
ConditionsYield
In ethanol at 60℃; for 5h; Michael Addition;100%
919-30-2

3-aminopropyltriethoxysilane

516-06-3

D,L-valine

C14H32N2O4Si

Conditions
ConditionsYield
at 170℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
919-30-2

3-aminopropyltriethoxysilane

302-72-7

rac-Ala-OH

C12H28N2O4Si

Conditions
ConditionsYield
at 200℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
919-30-2

3-aminopropyltriethoxysilane

56-40-6

glycine

76444-79-6

C11H26N2O4Si

Conditions
ConditionsYield
at 200℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
919-30-2

3-aminopropyltriethoxysilane

C15H35N3O4Si

Conditions
ConditionsYield
at 200℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
919-30-2

3-aminopropyltriethoxysilane

150-30-1

Phenylalanine

C18H32N2O4Si

Conditions
ConditionsYield
at 160℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
919-30-2

3-aminopropyltriethoxysilane

609-36-9

rac-Pro-OH

C14H30N2O4Si

Conditions
ConditionsYield
at 200℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
Conditions
ConditionsYield
at 200℃; for 0.05h; Product distribution / selectivity; Microwave irradiation (300 W);100%
919-30-2

3-aminopropyltriethoxysilane

6746-94-7

Cyclopropylacetylene

1262853-89-3

ethyl (1-cyclopropyl-vinyl) phosphinate

Conditions
ConditionsYield
With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); hypophosphorous acid; trifluoroacetic acid In toluene for 12h; Reflux; regioselective reaction;100%
20769-85-1

2-bromoisobutyric acid bromide

919-30-2

3-aminopropyltriethoxysilane

908595-77-7

2-bromo-2-methyl-(N-3-(triethoxysilyl)propyl)propanamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h;100%
With triethylamine In toluene at 0 - 20℃; for 26h;78%
With triethylamine In toluene at 0 - 20℃; Inert atmosphere;7.1 g
With triethylamine In toluene at 0 - 20℃; for 26h; Inert atmosphere;
With triethylamine In toluene at 0 - 20℃; for 26h; Inert atmosphere;
919-30-2

3-aminopropyltriethoxysilane

1430737-67-9

C46H32F4N4O8P2

1610459-21-6

C82H120N8O20P2Si4

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; Inert atmosphere; Schlenk technique;100%
919-30-2

3-aminopropyltriethoxysilane

41430-70-0

ethyl ester of perfluoropelargonic acid

N-[3-(triethoxysilyl)propyl]perfluoroheptanamide

Conditions
ConditionsYield
In ethanol at 60℃; for 2h;100%
919-30-2

3-aminopropyltriethoxysilane

2-((4-azidomethyl)phenyl )-4,4-dimethyloxazol-5(4H)-one

N-(2-(3-(triethoxysilyl)propylcarbamoyl)propan-2-yl)-4-(azidomethyl)benzamide

Conditions
ConditionsYield
In toluene at 20℃; for 12h;100%
1943-83-5

2-chloroethyl isothiocyanate

919-30-2

3-aminopropyltriethoxysilane

(EtO)3Si-CH2CH2CH2-NH-CO-NH-CH2CH2-Cl

Conditions
ConditionsYield
In pentane Solvent;100%
In pentane at -78 - 20℃; for 4.5h;100%
In ethanol at -78 - 50℃; for 2.5h;90.8%
In ethanol at -78 - -68℃; for 1.75h;
919-30-2

3-aminopropyltriethoxysilane

3-(diethylamino)phenyl 4-formylbenzoate

3-(diethylamino)phenyl 4-((3-(triethoxysilyl)propylimino)methyl)benzoate

Conditions
ConditionsYield
With magnesium sulfate In chloroform at 20℃; for 24h; Inert atmosphere;100%
919-30-2

3-aminopropyltriethoxysilane

3-(dimethylamino)phenyl 4-formylbenzoate

3-(dimethylamino)phenyl 4-((3-(triethoxysilyl)propylimino)methyl)benzoate

Conditions
ConditionsYield
With magnesium sulfate In chloroform at 20℃; for 24h; Inert atmosphere;100%
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  • Casno:

    919-30-2

    3-Aminopropyltriethoxysilane

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    Chemical Name 3-Aminopropyltriethoxysilane CAS No. 919-30-2 Molecular Fomula C9H23NO3Si Molecular weigh

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Specification

The 3-Aminopropyltriethoxysilane, with the CAS registry number 919-30-2, is also known as Trimethoxy[3-(2-oxiranylmethoxy)propyl]silane.It belongs to the product organic raw material. Its EINECS number is 213-048-4. This chemical's molecular formula is C9H23NO3Si and molecular weight is 221.37. What's more,Its systematic name is 3-Aminopropyltriethoxysilane.

Physical properties about 3-Aminopropyltriethoxysilane are:(1)ACD/LogP:  2.604; (2)# of Rule of 5 Violations:  0; (3)ACD/LogD (pH 5.5):  -0.49; (4)ACD/LogD (pH 7.4):  -0.13; (5)ACD/BCF (pH 5.5):  1.00; (6)ACD/BCF (pH 7.4):  1.00; (7)ACD/KOC (pH 5.5):  1.00; (8)ACD/KOC (pH 7.4):  1.16; (9)#H bond acceptors:  4; (10)#H bond donors:  2; (11)#Freely Rotating Bonds:  10; (12)Index of Refraction:  1.433; (13)Molar Refractivity:  61.233 cm3; (14)Molar Volume:  235.598 cm3; (15)Surface Tension:  27.0729999542236 dyne/cm; (16)Density:  0.94 g/cm3; (17)Flash Point:  104.444 °C; (18)Enthalpy of Vaporization:  45.853 kJ/mol; (19)Boiling Point:  222.079 °C at 760 mmHg; (20)Vapour Pressure:  0.104000002145767 mmHg at 25°C.

3-Glycidoxypropyltrimethoxysilane may cause damage to health.When you are using Sulphur, please be cautious about it as the following: (1)Harmful if swallowed; (2)Causes burns; (3)In case of contact with eyes, rinse immediately with plenty of water and seek medical advice; (4)In case of accident or if you feel unwell, seek medical advice immediately (show label where possible); (5)Wear suitable protective clothing, gloves and eye/face protection.The Safety Information of 3-Aminopropyltriethoxysilane as follows:(1)RIDADR:UN 2735 8/PG 2; (2)WGK Germany:1; (3)RTECS:TX2100000; (4)F:10-34; (5)TSCA:Yes; (6)HazardClass:8; (7)PackingGroup:III; (8)HS Code:29310095; (9)Transport Information:UN 3267.

You can still convert the following datas into molecular structure:
(1)SMILES:CCO[Si](CCCN)(OCC)OCC;
(2)Std. InChI:InChI=1S/C9H23NO3Si/c1-4-11-14(12-5-2,13-6-3)9-7-8-10/h4-10H2,1-3H3;
(3)Std. InChIKey:WYTZZXDRDKSJID-UHFFFAOYSA-N.

The toxicity data of 3-Aminopropyltriethoxysilane as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mammal (species unspecified) LD50 oral 4gm/kg (4000mg/kg)   Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 39(4), Pg. 86, 1974.
mammal (species unspecified) LD50 unreported > 4gm/kg (4000mg/kg)   Chemical Abstracts. Vol. 70, Pg. 36149, 1969.
mouse LD50 intraperitoneal 260mg/kg (260mg/kg)   Russian Chemical Reviws Vol. 38, Pg. 975, 1969.
mouse LD50 oral 4gm/kg (4000mg/kg) LUNGS, THORAX, OR RESPIRATION: EMPHYSEMA

BEHAVIORAL: EXCITEMENT

BLOOD: CHANGES IN LEUCOCYTE (WBC) COUNT
Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Substances. For English translation, see TNICS*. Vol. 11, Pg. 118, 1969.
rabbit LD50 skin 4mL/kg (4mL/kg)   Union Carbide Data Sheet. Vol. 1/19/1972,
rat LD50 oral 1780mg/kg (1780mg/kg)   American Industrial Hygiene Association Journal. Vol. 23, Pg. 95, 1962