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919-31-3

Basic Information
CAS No.: 919-31-3
Name: 2-CYANOETHYLTRIETHOXYSILANE
Article Data: 20
Molecular Structure:
Molecular Structure of 919-31-3 (2-CYANOETHYLTRIETHOXYSILANE)
Formula: C9H19 N O3 Si
Molecular Weight: 217.34
Synonyms: Propionitrile,3-(triethoxysilyl)- (6CI,7CI,8CI); (2-Cyanoethyl)triethoxysilane; (b-Cyanoethyl)triethoxysilane;3-(Triethoxysilyl)propionitrile; Cyanoethyltriethoxysilane; NSC 77092
Density: 0.964g/cm3
Boiling Point: 250.4°Cat760mmHg
Flash Point: 105.3°C
Solubility: Hydrolyzes in water.
Hazard Symbols:
Risk Codes: 36/37/38
Safety: Mildly toxic by ingestion and skin contact. A skin irritant. See also CYANIDE. When heated to decomposition it emits toxic fumes of NOx and CN.
PSA: 51.48000
LogP: 1.94848
Synthetic route
78-10-4

tetraethoxy orthosilicate

107-13-1

acrylonitrile

919-31-3

2-cyanoethyltriethoxysilane

Conditions
ConditionsYield
Stage #1: tetraethoxy orthosilicate at 100 - 105℃; for 2h; Molecular sieve; Large scale;
Stage #2: With titanium tetrachloride In water at 40 - 98℃; Large scale;
Stage #3: acrylonitrile Large scale; Further stages;
94.6%
998-30-1

Triethoxysilane

107-13-1

acrylonitrile

919-31-3

2-cyanoethyltriethoxysilane

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide at 56 - 59℃; for 2h; Large scale;94.5%
With lithium perchlorate at 25℃; for 2h; electrolysis;66%
64-17-5

ethanol

1071-22-3

2-cyanoethyltrichlorosilane

919-31-3

2-cyanoethyltriethoxysilane

Conditions
ConditionsYield
In dichloromethane for 3h; Heating;85%
19158-51-1

P-toluenesulfonyl cyanide

C8H19IO3SiZn

919-31-3

2-cyanoethyltriethoxysilane

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 25℃;67%
64-17-5

ethanol

18192-16-0

2-Cyanoethylsilan

919-31-3

2-cyanoethyltriethoxysilane

Conditions
ConditionsYield
With dihydrogen hexachloroplatinate; platinum
5089-72-5

3-[N-(2-aminoethyl)]aminopropyltriethoxysilane

919-31-3

2-cyanoethyltriethoxysilane

64-17-5

ethanol

18551-37-6

1,1,3,3-Tetraethoxy-1,3-bis-<2-cyan-ethyl>-disiloxan

919-31-3

2-cyanoethyltriethoxysilane

Conditions
ConditionsYield
With potassium hydroxide at 240℃; for 3h; Autoclave; Molecular sieve;
56907-19-8, 12081-12-8

bis(tetrahydrofurane)dichloridodioxidomolybdenum(VI)

919-31-3

2-cyanoethyltriethoxysilane

MoO2Cl2NCCH2CH2Si(OC2H5)3

Conditions
ConditionsYield
In dichloromethane mixed, stirred (30 min); filtered, concd. (to dryness), washed (hexane), dried (in vac.), elem. anal.;96%
919-31-3

2-cyanoethyltriethoxysilane

429-41-4

tetrabutyl ammonium fluoride

1393730-72-7

tetra-n-butylammonium octakis(2-cyanoethyl)octasilsesquioxane fluoride

Conditions
ConditionsYield
In tetrahydrofuran; water; toluene at 25℃; for 16h; Solvent; Inert atmosphere;96%
17455-13-9

18-crown-6 ether

919-31-3

2-cyanoethyltriethoxysilane

octakis(2-cyanoethyl)octasilsesquioxane fluoride-18-crown-6-potasium

Conditions
ConditionsYield
Stage #1: 18-crown-6 ether With potassium fluoride In toluene; acetonitrile at 20℃; for 0.25h; Inert atmosphere;
Stage #2: 2-cyanoethyltriethoxysilane In water; toluene; acetonitrile at 20℃; Inert atmosphere;
96%
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Chemistry

IUPAC Name: 3-Triethoxysilylpropanenitrile
Synonyms: (.beta.-Cyanoethyl)triethoxysilane ; (2-Cyanoethyl)triethoxysilane ; 3-(Triethoxysilyl)propionitrile ; Propanenitrile, 3- (triethoxysilyl)- ; Propionitrile, 3- (triethoxysilyl)-
Product Categories: Functional Materials;Si (Classes of Silicon Compounds);Silane Coupling Agents;Silane Coupling Agents (Intermediates);Si-O Compounds;Trialkoxysilanes
CAS NO:919-31-3
Molecular Formula of (2-Cyanoethyl)triethoxysilane (CAS NO.919-31-3) :C9H19NO3Si
Molecular Weight of (2-Cyanoethyl)triethoxysilane (CAS NO.919-31-3) :217.34
Molecular structure of (2-Cyanoethyl)triethoxysilane (CAS NO.919-31-3) :
Index of Refraction:1.425
Surface Tension: 27.6 dyne/cm 
Density: 0.964 g/cm3 
Flash Point: 105.3 °C 
Enthalpy of Vaporization: 48.77 kJ/mol 
Boiling Point: 250.4 °C at 760 mmHg 
Vapour Pressure: 0.0216 mmHg at 25°C 
Sensitive : Moisture Sensitive

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rabbit LD50 skin 5950uL/kg (5.95mL/kg)   American Industrial Hygiene Association Journal. Vol. 23, Pg. 95, 1962.
rat LD50 oral 5630mg/kg (5630mg/kg)   American Industrial Hygiene Association Journal. Vol. 23, Pg. 95, 1962.

Consensus Reports

Reported in EPA TSCA Inventory. Cyanide and its compounds are on the Community Right-To-Know List.

Safety Profile

Mildly toxic by ingestion and skin contact. A skin irritant. See also CYANIDE. When heated to decomposition it emits toxic fumes of NOx and CN.
Hazard Codes IrritantXi
Risk Statements 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements 26
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
WGK Germany 2
RTECS VV2750000
F 10-21
TSCA Yes