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CAS No.: | 934-55-4 |
---|---|
Name: | POTASSIUM BENZENESULFONATE |
Article Data: | 12 |
Molecular Structure: | |
Formula: | C6H6 O3 S . K |
Molecular Weight: | 196.268 |
Synonyms: | Benzenesulfonicacid, potassium salt (8CI,9CI); Potassium benzenesulfonate |
Density: | 1.409g/cm3 |
Melting Point: | 50-51oC (ANHYDROUS) |
Boiling Point: | °Cat760mmHg |
Flash Point: | °C |
PSA: | 65.58000 |
LogP: | 1.67150 |
1-naphthalene methanol
Benzyl phenyl sulfone
A
(E)-2-styrylnaphthalene
B
potassium benzenesulfonate
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate In 1,4-dioxane at 125℃; for 5h; Inert atmosphere; Schlenk technique; Glovebox; | A 76% B n/a |
4-Methylbenzyl alcohol
Benzyl phenyl sulfone
A
E-1-methyl-4-styryl-benzene
B
potassium benzenesulfonate
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate In 1,4-dioxane at 125℃; for 5h; Inert atmosphere; Schlenk technique; Glovebox; | A 72% B n/a |
Benzyl phenyl sulfone
4-Methoxybenzyl alcohol
A
E-1-(phenyl)-2-(4'-methoxyphenyl)ethene
B
potassium benzenesulfonate
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate In 1,4-dioxane at 125℃; for 5h; Inert atmosphere; Schlenk technique; Glovebox; | A 71% B n/a |
Benzyl phenyl sulfone
para-Chlorobenzyl alcohol
A
(E)-1-(4-chlorophenyl)-2-phenylethene
B
potassium benzenesulfonate
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate In 1,4-dioxane at 125℃; for 5h; Inert atmosphere; Schlenk technique; Glovebox; | A 70% B n/a |
biphenyl-4-yl methanol
Benzyl phenyl sulfone
A
(E)-4-phenylstilbene
B
potassium benzenesulfonate
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate In 1,4-dioxane at 125℃; for 5h; Inert atmosphere; Schlenk technique; Glovebox; | A 69% B n/a |
diphenyl sulphone
A
biphenyl
B
potassium benzenesulfonate
C
potassium benzenesulfinate
Conditions | Yield |
---|---|
With 1-indoline; potassium tert-butylate; oxygen In benzene at 80℃; for 15h; Inert atmosphere; | A 26% B 28% C 58% |
Conditions | Yield |
---|---|
With 5,10,15,20-tetrakisphenylporphyrin; oxygen In ethanol; tert-butyl alcohol at 15℃; for 0.1h; Irradiation; | A 51% B 28% |
Benzyl phenyl sulfone
benzyl alcohol
A
(1E)-1,3-diphenylpropene
B
potassium benzenesulfonate
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate In 1,4-dioxane at 125℃; for 5h; Inert atmosphere; Schlenk technique; Glovebox; | A 35% B n/a |
diethyl ether
potassium ethyl xanthogenate
benzenesulfonyl chloride
A
bis-ethoxythiocarbonyldisulfane
B
diphenyl disulfone
C
potassium benzenesulfonate
potassium ethyl xanthogenate
benzenesulfonyl chloride
A
O,S-Diethyl dithiocarbonate
B
diphenyl disulfone
C
potassium benzenesulfonate
Conditions | Yield |
---|---|
at 0℃; analoge Reaktion mit anderen Sulfonsaeurechloriden; |