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943606-84-6

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Basic Information
CAS No.: 943606-84-6
Name: 1-chloro-6-Methyl-5-nitroisoquinoline
Article Data: 9
Molecular Structure:
Molecular Structure of 943606-84-6 (1-chloro-6-Methyl-5-nitroisoquinoline)
Formula: C10H7ClN2O2
Molecular Weight: 222.631
Synonyms: 1-chloro-6-Methyl-5-nitroisoquinoline
Density: 1.419±0.06 g/cm3(Predicted)
Boiling Point: 377.6±37.0 °C(Predicted)
PSA: 58.71000
LogP: 3.62800
Related products
Synthetic route
943606-83-5

6-methyl-5-nitroisoquinoline 2-oxide

943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

Conditions
ConditionsYield
With trichlorophosphate In chloroform at 70℃; for 3h;96%
With trichlorophosphate In 1,2-dichloro-ethane at 70℃; for 3h;86%
With trichlorophosphate In 1,2-dichloro-ethane Reflux;55%
With trichlorophosphate In 1,2-dichloro-ethane Reflux;55%
With trichlorophosphate In 1,2-dichloro-ethane at 70℃;0.88 g
188121-31-5

6-methyl-5-nitroisoquinoline

943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

Conditions
ConditionsYield
With trichlorophosphate In 1,2-dichloro-ethane Reflux;55%
With trichlorophosphate In 1,2-dichloro-ethane for 7h; Reflux;55%
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
2: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
2: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 °C
2: trichlorophosphate / 1,2-dichloro-ethane / 3 h / 70 °C
View Scheme
70810-28-5

6-methylisoquinoline N-oxide

943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

Conditions
ConditionsYield
With potassium nitrate; trichlorophosphate In chloroform; sulfuric acid
42398-73-2

6-methylisoquinoline

943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sulfuric acid; potassium nitrate / 0 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
3: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 2 steps
1: potassium nitrate; sulfuric acid / 0 °C
2: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 2 steps
1: sulfuric acid; potassium nitrate / 3 h / 0 °C
2: trichlorophosphate / 1,2-dichloro-ethane / 7 h / Reflux
View Scheme
Multi-step reaction with 3 steps
1: sulfuric acid; potassium nitrate / 0 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
3: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 3 steps
1: sulfuric acid; potassium nitrate / 1.5 h / 0 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 °C
3: trichlorophosphate / 1,2-dichloro-ethane / 3 h / 70 °C
View Scheme
104-87-0

4-methyl-benzaldehyde

943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: chloroform / 90 °C
2.1: chloroformic acid ethyl ester; triethyl phosphite / chloroform / 24 h / 0 - 20 °C
2.2: 0 °C / Reflux
3.1: sulfuric acid; potassium nitrate / 0 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
5.1: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 3 steps
1.1: chloroform / 90 °C
1.2: 24 h / 0 - 20 °C
1.3: 0 - 20 °C / Reflux
2.1: potassium nitrate; sulfuric acid / 0 °C
3.1: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 3 steps
1.1: chloroform / 90 °C
1.2: 24 h / 0 - 20 °C
1.3: 12 h / 0 °C / Reflux
2.1: sulfuric acid; potassium nitrate / 3 h / 0 °C
3.1: trichlorophosphate / 1,2-dichloro-ethane / 7 h / Reflux
View Scheme
Multi-step reaction with 4 steps
1.1: chloroform / 90 °C
1.2: 24 h / 0 - 20 °C
1.3: 0 °C / Reflux
2.1: sulfuric acid; potassium nitrate / 0 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
4.1: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
Multi-step reaction with 4 steps
1.1: chloroform / 22 - 65 °C
1.2: 23 h / -3 - 20 °C
1.3: 10.5 h / 52 °C
2.1: sulfuric acid; potassium nitrate / 1.5 h / 0 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 °C
4.1: trichlorophosphate / 1,2-dichloro-ethane / 3 h / 70 °C
View Scheme
54879-70-8

(2,2-Dimethoxy-ethyl)-[1-p-tolyl-meth-(Z)-ylidene]-amine

943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: chloroformic acid ethyl ester; triethyl phosphite / chloroform / 24 h / 0 - 20 °C
1.2: 0 °C / Reflux
2.1: sulfuric acid; potassium nitrate / 0 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
4.1: trichlorophosphate / 1,2-dichloro-ethane / Reflux
View Scheme
943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

98-18-0

m-aminobenzenesulfonamide

C16H14N4O4S

Conditions
ConditionsYield
With trifluoroacetic acid In isopropyl alcohol at 20 - 90℃; for 18h; Inert atmosphere;99.4%
943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

37045-73-1

3-(methylsulfonamido)aniline

1446113-45-6

N-(3-((6-methyl-5-nitroisoquinolin-1-yl)amino)phenyl)methanesulfonamide

Conditions
ConditionsYield
In isopropyl alcohol at 120℃; for 1.5h; Sealed tube;99%
In isopropyl alcohol at 120℃; for 1.5h; Sealed tube;99%
943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

10272-07-8

3,5-Dimethoxyaniline

C18H17N3O4

Conditions
ConditionsYield
With trifluoroacetic acid In isopropyl alcohol at 20 - 90℃; for 16h; Inert atmosphere;98.4%
943606-84-6

1-chloro-6-methyl-5-nitroisoquinoline

54060-30-9

3-acetylenephenylamine

C18H13N3O2

Conditions
ConditionsYield
With trifluoroacetic acid In isopropyl alcohol at 20 - 90℃; for 16h; Inert atmosphere;95.4%
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