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98977-36-7

Basic Information
CAS No.: 98977-36-7
Name: 1-Boc-3-piperidone
Molecular Structure:
Molecular Structure of 98977-36-7 (1-Boc-3-piperidone)
Formula: C10H17NO3
Molecular Weight: 199.25
Synonyms: tert-butyl 3-oxopiperidine-1-carboxylate;1-N-Boc-3-piperidone;N-Boc-3-piperidinone;N-(tert-Butoxycarbonyl)-3-piperidinone;3-Oxopiperidine, N-BOC protected;N-Boc-3-piperidone;1-Boc-3-piperidone, 98%;Boc-3-piperidone;tert-butyl-3-oxopiperidine-1-carboxylate;3-Oxo-piperidine-1-carboxylic acid tert-butyl ester;
EINECS: 629-575-1
Density: 1.099 g/cm3
Melting Point: 35-40 °C(lit.)
Boiling Point: 289.825 °C at 760 mmHg
Flash Point: 129.082 °C
Solubility: It is insoluble in water.
Appearance: white to yellow low melting solid
Hazard Symbols:
Risk Codes:
Safety: 24/25
Transport Information:
PSA: 46.61000
LogP: 1.52430
Synthetic route
85275-45-2

N-tert-butoxycarbonyl-3-piperidinol

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With sodium hypochlorite solution; sodium hydrogencarbonate; potassium bromide In dichloromethane at 5 - 10℃; pH=8.5; Reagent/catalyst;99.4%
With Dess-Martin periodane In dichloromethane at 20℃; for 22h; Inert atmosphere;97%
With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide In diethyl ether; water; toluene at 0 - 4℃;95%

1-benzyl-piperidin-3-one hydrochloride hydrate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With hydrogen; palladium dihydroxide In methanol; dichloromethane97%
40114-49-6

1-benzyl-3-piperidone

24424-99-5

di-tert-butyl dicarbonate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: 1-benzyl-3-piperidone With hydrogenchloride; palladium 10% on activated carbon; hydrogen In methanol; water at 20℃; for 2h;
Stage #2: With N-ethyl-N,N-diisopropylamine In methanol; water for 0.5h;
Stage #3: di-tert-butyl dicarbonate In methanol; water at 20℃; for 5h; Concentration; Reagent/catalyst;
84.2%
1179348-67-4

C12H23NO4S

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)diiridium(I) dichloride In 1,2-dichloro-ethane at 70℃;82%
With bis(1,5-cyclooctadiene)diiridium(I) dichloride In 1,2-dichloro-ethane at 70℃; for 18h; Inert atmosphere;82%
79-37-8

oxalyl dichloride

85275-45-2

N-tert-butoxycarbonyl-3-piperidinol

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With ammonium chloride; trimethylamine In dichloromethane; dimethyl sulfoxide78%
276872-89-0

tert-butyl 3-methylidenepiperidine-1-carboxylate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With 2,6-dimethylpyridine; sodium periodate; ruthenium(III) chloride trihydrate In dichloromethane; water; acetonitrile at 20℃; for 1h; Inert atmosphere;68%
24424-99-5

di-tert-butyl dicarbonate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0℃; for 2h; Yield given;
With sodium hydrogencarbonate In tetrahydrofuran for 4h;2.93 g
With sodium hydrogencarbonate In tetrahydrofuran; water for 4h;

C12H24NO3S(1+)*Cl(1-)

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 1h; Swern oxidation;
24424-99-5

di-tert-butyl dicarbonate

1-benzyl-3-piperidone monohydrochloride monohydrate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: 1-benzyl-3-piperidone monohydrochloride monohydrate With hydrogen; palladium on activated charcoal In methanol under 2844.31 Torr;
Stage #2: di-tert-butyl dicarbonate With sodium hydrogencarbonate In tetrahydrofuran for 48h;
56.6 g
6859-99-0

3-hydroxypiperazine

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaOH / tetrahydrofuran; H2O / 1 h / 20 °C
2: triethylamine; SO3*NMe3; DMSO / 18 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: NaOH / H2O; tetrahydrofuran / 1 h / 20 °C
2: 15.6 g / triethylamine; trioxide-trimethylamine complex / dimethylsulfoxide / 18 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: NaOH / tetrahydrofuran; H2O / 1 h / 20 °C
2: 15.6 g / DMSO; SO3*Me3N; triethylamine / 18 h / 20 °C
View Scheme
24424-99-5

di-tert-butyl dicarbonate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaOH / tetrahydrofuran; H2O / 1 h / 20 °C
2: triethylamine; SO3*NMe3; DMSO / 18 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: NaOH / H2O; tetrahydrofuran / 1 h / 20 °C
2: 15.6 g / triethylamine; trioxide-trimethylamine complex / dimethylsulfoxide / 18 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: 90 percent / NaHCO3 / tetrahydrofuran / 14 h
2: tetrapropylammonium perruthenate; NMO; 4A molecular sieves / CH2Cl2; acetonitrile / 1 h
View Scheme
50606-58-1

N-benzyl-3-piperidinone hydrochloride

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / Pd/C / methanol; H2O / 16 h / 2844.31 Torr
2: 2.93 g / aq. NaHCO3 / tetrahydrofuran / 4 h
View Scheme
24424-99-5

di-tert-butyl dicarbonate

1.) NaH; 2.) SOCl2

1.) NaH; 2.) SOCl2

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaOH / tetrahydrofuran; H2O / 1 h / 20 °C
2: 15.6 g / DMSO; SO3*Me3N; triethylamine / 18 h / 20 °C
View Scheme
6859-99-0

3-hydroxypiperazine

A

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

B

p-F-C6H4-Hal

p-F-C6H4-Hal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: CH2Cl2
2: SO3*pyridine; Et3N / CH2Cl2
View Scheme
24424-99-5

di-tert-butyl dicarbonate

A

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

B

p-F-C6H4-Hal

p-F-C6H4-Hal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: CH2Cl2
2: SO3*pyridine; Et3N / CH2Cl2
View Scheme
6859-99-0

3-hydroxypiperazine

paraformaldehyde

paraformaldehyde

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: Cr2O3, Ac2O, Py / CH2Cl2
View Scheme
24424-99-5

di-tert-butyl dicarbonate

pentacarbonyl<1-<<(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl>oxy>-(E)-3-phenyl-2-propenylidene>chromium

pentacarbonyl<1-<<(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl>oxy>-(E)-3-phenyl-2-propenylidene>chromium

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: Cr2O3, Ac2O, Py / CH2Cl2
View Scheme
61995-16-2

1-Benzyl-3,3-dihydroxypiperidine hydrobromide

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / 10percent Pd/C / ethanol; H2O / 2205.2 Torr
2: triethylamine / tetrahydrofuran / 2 h / 0 °C
View Scheme
40114-49-6

1-benzyl-3-piperidone

34619-03-9

tert-butyldicarbonate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With hydrogen; triethylamine; 20% palladium hydroxide on carbon In methanol at 50℃; under 3102.97 Torr; for 0.666667h;
6859-99-0

3-hydroxypiperazine

aqueous sodium hypochlorite

aqueous sodium hypochlorite

aqueous sodium bisulphite

aqueous sodium bisulphite

24424-99-5

di-tert-butyl dicarbonate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With potassium bromide; sodium chloride; sodium hydrogencarbonate In dichloromethane; water
114615-82-6

tetrapropylammonium perruthennate

7529-22-8

4-methylmorpholine N-oxide

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
molecular sieves In dichloromethane
85275-45-2

N-tert-butoxycarbonyl-3-piperidinol

87413-09-0

Dess-Martin periodane

sodium thiosulfate

A

(1H-Benzoimidazol-2-ylmethyl)-(2-piperidin-3-ylidene-ethyl)-(5,6,7,8-tetrahydro-quinolin-8-yl)-amine (hydrobromide salt)

(1H-Benzoimidazol-2-ylmethyl)-(2-piperidin-3-ylidene-ethyl)-(5,6,7,8-tetrahydro-quinolin-8-yl)-amine (hydrobromide salt)

B

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With NaHCO3 In dichloromethaneA 1.80 g (95%)
B n/a
144243-24-3

tert‐butyl 3‐aminopiperidine‐1‐carboxylate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With recombinant Rhodobacter sphaeroides amine-transaminase In dimethyl sulfoxide at 20℃; pH=7.5; aq. buffer; Enzymatic reaction;
143900-43-0

tert-butyl (3R)-3-hydroxypiperidine-1-carboxylate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane at 20℃;
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

piperidin-3-one hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In dichloromethane; ethyl acetate at 20℃; for 1.5h;100%
With hydrogenchloride In water at 20℃;63%
With hydrogenchloride In 1,4-dioxane; dichloromethane at 20℃; for 3h;
With hydrogenchloride In diethyl ether; dichloromethane at 20℃; for 3h;
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1576-35-8

toluene-4-sulfonic acid hydrazide

396730-46-4

1,1-dimethylethyl 3-[2-[(4-methylphenyl)sulphonyl]hydrazono]-1-piperidinecarboxylate

Conditions
ConditionsYield
In dichloromethane for 2h;100%
75-16-1

methylmagnesium bromide

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1104083-27-3

tert-butyl 3-hydroxy-3-methylpiperidine-1-carboxylate

Conditions
ConditionsYield
With ammonium chloride In tetrahydrofuran; diethyl ether at 0 - 20℃; for 18h; Inert atmosphere;100%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

3-amino-piperidin-3-yl-phosphonic acid

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With acetamide; acetic acid; acetyl chloride at 20℃; Cooling with ice;
Stage #2: With phosphorus trichloride at 75℃; Cooling with ice;
Stage #3: With hydrogenchloride In water for 8h; Reflux;
100%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

625471-18-3

tert-butyl (3S)-3-aminopiperidine-1-carboxylate

Conditions
ConditionsYield
With pyridoxal 5'-phosphate; isopropylamine In dimethyl sulfoxide at 50℃; for 50h; pH=7.5; Reagent/catalyst; Temperature; Enzymatic reaction; enantioselective reaction;99%
With pyridoxal 5'-phosphate; transaminase pQR2189; isopropylamine In aq. phosphate buffer; dimethyl sulfoxide at 35℃; for 18h; pH=7.5; Kinetics; Reagent/catalyst;60 %Chromat.

7-chloroisoquinolin-5-amine

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

tert-butyl 3-((7-chloroisoquinolin-5-yl)amino)piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 7-chloroisoquinolin-5-amine; 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With acetic acid at 20℃; for 0.5h;
Stage #2: With sodium tris(acetoxy)borohydride at 20℃; for 18h;
99%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

143900-44-1

tert-butyl (3S)-3-hydroxypiperidine-1-carboxylate

Conditions
ConditionsYield
With rac-octan-2-ol In aq. buffer at 35℃; for 12h; pH=8; Reagent/catalyst; pH-value; Temperature; Enzymatic reaction; enantioselective reaction;98.08%
With D-glucose; NADP In aq. phosphate buffer; ethanol at 30℃; for 4h; pH=6; enantioselective reaction;96%
With recombinant Rhodococcus erythropolis DSM 43297 ketoredutase; nicotinamide adenine dinucleotide In aq. phosphate buffer; isopropyl alcohol at 50℃; for 0.5h; pH=7.0; Enzymatic reaction; stereoselective reaction;95%
37595-74-7

N,N-phenylbistrifluoromethane-sulfonimide

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

149108-74-7

5-trifluoromethanesulfonyloxy-3,4-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; for 0.333333h;
Stage #2: N,N-phenylbistrifluoromethane-sulfonimide In tetrahydrofuran at -78 - 0℃; for 3.25h;
98%
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 2h;
Stage #2: N,N-phenylbistrifluoromethane-sulfonimide In tetrahydrofuran at -78 - 20℃;
85%
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere;
Stage #2: N,N-phenylbistrifluoromethane-sulfonimide In tetrahydrofuran at 20℃; Inert atmosphere;
44%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

100-58-3

phenylmagnesium bromide

5-phenyl-1,2,3,6-tetrahydropyridine

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester; phenylmagnesium bromide In tetrahydrofuran at 0℃; for 1.5h; Inert atmosphere;
Stage #2: With trifluoroacetic acid at 22 - 75℃;
98%
867-13-0

diethoxyphosphoryl-acetic acid ethyl ester

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

tert-butyl 3-(2-ethoxy-2-oxoethylidene)piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran at 0℃; for 0.5h;
Stage #2: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester In tetrahydrofuran at 20℃; for 5h; Horner-Wadsworth-Emmons Olefination;
98%
870-46-2

t-butoxycarbonylhydrazine

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1305274-91-2

tert-butyl (3E)-3-[(tert-butoxycarbonyl)hydrazono]piperidine-1-carboxylate

Conditions
ConditionsYield
In toluene at 60℃; for 4h;95%
551-93-9

2-aminoacetophenone

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1347747-90-3

C18H22N2O2

Conditions
ConditionsYield
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate; N,N-dimethyl-formamide at 90℃; Friedlaender reaction;95%
914382-66-4

(S)-cyclopentyl 2-amino-4-methylpentanoate 4-methylbenzenesulfonate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1351815-36-5

cyclopentyl N-[1-(tert-butoxycarbonyl)piperidin-3-yl]-L-leucinate

Conditions
ConditionsYield
Stage #1: (S)-cyclopentyl 2-amino-4-methylpentanoate 4-methylbenzenesulfonate; 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With sodium tris(acetoxy)borohydride In 1,1-dichloroethane at 20℃; for 18h;
Stage #2: With sodium hydrogencarbonate In 1,1-dichloroethane; water at 20℃; for 0.333333h;
95%
19947-75-2

5-amino-3,4-dimethylisoxazol

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

tert-butyl 3-[(3,4-dimethyl-1,2-oxazol-5-yl)amino]piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 5-amino-3,4-dimethylisoxazol; 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With acetic acid In 1,2-dichloro-ethane at 25℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 0 - 25℃; for 48h;
95%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

4301-14-8

acetylenemagnesium bromide

287192-85-2

tert-butyl 3-ethynyl-3-hydroxypiperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester; acetylenemagnesium bromide In tetrahydrofuran at 0℃; for 4h;
Stage #2: With ammonium chloride In tetrahydrofuran; water
94%
In tetrahydrofuran at 0 - 20℃; for 12h;80%
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

871726-72-6

4-((dimethylamino)methylene)-3-oxopiperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
at 100℃; for 2h;94%
In N,N-dimethyl-formamide at 80℃; for 12h;
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

C10H18N2O2

Conditions
ConditionsYield
With ammonium acetate In ethanol for 7h; Reflux; Large scale;93.7%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

143900-43-0

tert-butyl (3R)-3-hydroxypiperidine-1-carboxylate

Conditions
ConditionsYield
With recombinant Chryseobacterium sp. CA 49 ketoreductase; nicotinamide adenine dinucleotide In aq. phosphate buffer; isopropyl alcohol at 40℃; for 6h; pH=7.0; Enzymatic reaction; stereoselective reaction;93%
With SmADH31 Kinetics; Enzymatic reaction; stereoselective reaction;89%

5-bromo-3-methyl-6-oxo-1,6-dihydropyridine-2-carboxamide

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

6-bromo-8-methyl-2H-spiro[imidazo[1,5-a]pyridine-3,3'-piperidine]-1,5-dione hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane at 110℃; for 16h; Sealed tube;93%
1035096-74-2

1-(5-Amino-1H-indazol-1-yl)-2,2-dimethylpropan-1-one Maleate

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1035096-75-3

tert-butyl 3-(1-pivaloyl-1H-indazol-5-ylamino)piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 1-(5-Amino-1H-indazol-1-yl)-2,2-dimethylpropan-1-one Maleate; 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane
91%
Stage #1: 1-(5-Amino-1H-indazol-1-yl)-2,2-dimethylpropan-1-one Maleate; 3-oxo-piperidine-1-carboxylic acid tert-butyl ester In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere;
Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane
Stage #3: With sodium hydrogencarbonate In 1,2-dichloro-ethane
1643-73-8

(4-fluorobenzyl)magnesium chloride

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

tert-butyl 3-(4-fluorobenzyi)-3-hydroxypiperidine-1-carboxylate

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 3h;90%
In tetrahydrofuran at 20℃; for 3h;
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

610-14-0

2-nitrobenzyl chloride

tert-butyl 4-(2-nitrobenzoyl)-3-carbonylpiperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With lithium diisopropyl amide In tetrahydrofuran at -78 - -40℃; for 1h; Inert atmosphere;
Stage #2: 2-nitrobenzyl chloride In tetrahydrofuran at -40 - 30℃; for 3h; Inert atmosphere;
90%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

518308-79-7

6-(4-chlorophenyl)-2-oxo-4-(piperidin-1-yl)-2H-pyran-3-carbonitrile

tertbutyl 8-(4-chlorophenyl)−5-cyano-6-(piperidin-1-yl)−3,4-dihydroquinoline-1(2H)-carboxylate

Conditions
ConditionsYield
With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.8h; Irradiation; Sonication; Green chemistry;89%
With sodium amide; dimethyl sulfoxide at 25 - 35℃; for 3h; regioselective reaction;
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

388573-73-7

6-(4-chloro-phenyl)-2-oxo-4-(4-phenyl-piperazin-1-yl)-2H-pyran-3-carbonitrile

tertbutyl 8-(4-chlorophenyl)−5-cyano-6-(4-phenylpiperazin-1-yl)−3,4-dihydroquinoline-1(2H)-carboxylate

Conditions
ConditionsYield
With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.833333h; Irradiation; Sonication; Green chemistry;89%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

1000576-83-9

tert-butyl 3-(dimethylamino)piperidinyl-1-carboxylate

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃;
Stage #2: With sodium hydrogencarbonate In water; 1,2-dichloro-ethane
88%
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

124-40-3

dimethyl amine

1000576-83-9

tert-butyl 3-(dimethylamino)piperidinyl-1-carboxylate

Conditions
ConditionsYield
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester; dimethyl amine In tetrahydrofuran; dichloromethane at 20℃; for 0.0833333h;
Stage #2: With sodium tris(acetoxy)borohydride In tetrahydrofuran; dichloromethane at 20℃;
88%
Stage #1: 3-oxo-piperidine-1-carboxylic acid tert-butyl ester; dimethyl amine In ethanol at 0 - 20℃; for 2h;
Stage #2: With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; for 16h;
98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

C10H19NO3

Conditions
ConditionsYield
With NAD; isopropyl alcohol In aq. phosphate buffer at 30℃; for 12h; pH=7; Reagent/catalyst; Microbiological reaction; Green chemistry; Enzymatic reaction; stereoselective reaction;88%
271-29-4

6-azaindole

98977-36-7

3-oxo-piperidine-1-carboxylic acid tert-butyl ester

tert-butyl 5-(1H-pyrrolo[2,3-c]pyridin-3-yl)-3,4-dihydropyridine-1(2H)-carboxylate

Conditions
ConditionsYield
With potassium hydroxide In methanol; water at 75℃; for 48h;87%
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Specification

1-Boc-3-piperidone, with the CAS Number 98977-36-7, is also called 1-(tert-Butoxycarbonyl)-3-piperidone~tert-Butyl 3-oxo-1-piperidinecarboxylate; 1-Boc-3-piperidinone; T-BUTYL-3-PIPERIDONE-1-CARBOXYLATE; TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE; N-Boc-3-piperidone. And it is white to yellow solid or liquid. 1-Boc-3-piperidone is useful in stereocontrolled synthesis of chiral compounds.

Physical properties about 1-Boc-3-piperidone are: (1)ACD/LogP: 0.761; (2)ACD/LogD (pH 5.5): 0.76; (3)ACD/LogD (pH 7.4): 0.76; (4)ACD/BCF (pH 5.5): 2.23; (5)ACD/BCF (pH 7.4): 2.23; (6)ACD/KOC (pH 5.5): 61.81; (7)ACD/KOC (pH 7.4): 61.81; (8)#H bond acceptors: 4; (9)#Freely Rotating Bonds: 2; (10)Index of Refraction: 1.481; (11)Molar Refractivity: 51.57 cm3; (12)Molar Volume: 181.195 cm3; (13)Polarizability: 20.444 10-24cm3; (14)Surface Tension: 39.5019989013672 dyne/cm; (15)Density: 1.1 g/cm3; (16)Flash Point: 129.082 °C; (17)Enthalpy of Vaporization: 52.915 kJ/mol; (18)Boiling Point: 289.825 °C at 760 mmHg; (19)Vapour Pressure: 0.0020000000949949 mmHg at 25°C

You can still convert the following datas into molecular structure:
(1)SMILES:CC(C)(C)OC(=O)N1CCCC(=O)C1;
(2)Std. InChI:InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3;
(3)Std. InChIKey:RIFXIGDBUBXKEI-UHFFFAOYSA-N