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Basic Information
CAS No.: 99896-85-2
Name: ARG-GLY-ASP
Article Data: 5
Molecular Structure:
Molecular Structure of 99896-85-2 (ARG-GLY-ASP)
Formula: C12H22N6O6
Molecular Weight: 346.343
Synonyms: L-Asparticacid, N-(N-L-arginylglycyl)-;10: PN: JP2003189848 PAGE: 2 claimed protein;1337: PN: US20090258017 SEQID: 1353claimed protein;13: PN:US6147189 SEQID: 1 claimed protein;1: PN: JP2009072081 PAGE: 7 claimed protein;1: PN: US20080262614 SEQID: 1unclaimed protein;1: PN: WO0004941PAGE: 31 claimed protein;1: PN:WO0147553 PAGE: 13 claimed protein;1: PN: WO2008150101 SEQID: 1claimed protein;24: PN: US6797807PAGE: 59-60 claimed protein;2:PN: JP2004344469 SEQID: 2 claimed protein;
Density: 1.61 g/cm3
Melting Point: 153-155℃ (ethyl ether )
Boiling Point: 597.205°C at 760 mmHg
Flash Point: 314.979°C
PSA: 220.72000
LogP: -0.58970
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Synthetic route

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Conditions
ConditionsYield
With methanol; triethylsilane; water; trifluoroacetic acid at 20℃; for 2h;72%
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Conditions
ConditionsYield
Stage #1: glycyl-L-aspartic acid; Nα,NG,NG'-tri-Boc-L-arginine N-hydroxysuccinimide ester With 4-methyl-morpholine In N,N-dimethyl-formamide at 20℃; for 24h; Addition;
Stage #2: With trifluoroacetic acid In chloroform Hydrolysis; deprotection;		54%
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Conditions
ConditionsYield
Multistep reaction;
...Expand
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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 4-toluenesulfonic acid; H2 / Pd/C / dimethylformamide / 48 h
2.1: N-methylmorpholine / dimethylformamide / 24 h / 20 °C
2.2: 54 percent / TFA, 50 percent / CHCl3
View Scheme
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p-cresol

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Conditions
ConditionsYield
In hydrogen fluoride
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Conditions
ConditionsYield
Multistep reaction;100%
...Expand
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Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 17h; Product distribution / selectivity; Sonographic reaction;59%
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 1h; Product distribution / selectivity;
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1,2-dioleyol-sn-glycero-3-phosphoethanolamine-n-[poly(ethyleneglycol)]-N-benzotriazole carbonate : Arg-Gly-Asp conjugate, 2:1 molar ratio, PEG MW = 3400

1,2-dioleyol-sn-glycero-3-phosphoethanolamine-n-[poly(ethyleneglycol)]-N-benzotriazole carbonate : Arg-Gly-Asp conjugate, 2:1 molar ratio, PEG MW = 3400

Conditions
ConditionsYield
In various solvent(s) at 4℃; for 4h; pH=7.5;
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Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 19h;

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Conditions
ConditionsYield
With methanol; triethylsilane; water; trifluoroacetic acid at 20℃; for 2h;72%
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Chemistry

Product Name: Arg-gly-asp (CAS NO.99896-85-2)


Molecular Formula: C12H22N6O6
Molecular Weight: 346.34g/mol
Mol File: 99896-85-2.mol
Storage Temperature: −20°C
Density: 1.61 g/cm3
Surface Tension: 76.3 dyne/cm
Structure Descriptors of Arg-gly-asp (CAS NO.99896-85-2):
  InChI : InChI=1/C12H22N6O6/c13-6(2-1-3-16-12(14)15)10(22)17-5-8(19)18-7(11(23)24)4-9(20)21/h6-7H,1-5,13H2,(H,17,22)(H,18,19)(H,20,21)(H,23,24)(H4,14,15,16)/t6-,7-/m0/s1  
  Smiles: NC(=N)NCCC[C@@H](C(NCC(=O)N[C@@H](CC(=O)O)C(O)=O)=O)N
Product Categories: Peptide; Cell Signaling Enzymes; ECM ProteinsCytoskeleton and Extracellular Matrix; Extracellular Matrix; Extracellular Matrix Peptides (ECM); Extracellular Matrix Peptides and ProteinsPeptides for Cell Biology; Fibronectin Fragments and Analogs; Matrix Metalloproteinases Products; Various Peptides

Specification

 Arg-gly-asp ,its CAS NO. is 99896-85-2,the synonyms is Arginyl-glycyl-asparagilin ; Arginyl-glycyl-aspartic acid ; F-336 ; N-(N-L-Arginylglycyl)-L-aspartic acid ; Rgd peptide ; Rgd tripeptide sequence ; L-Aspartic acid, N-(N-L-arginylglycyl)- .