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Ethylbutylamine
Cas No: 13360-63-9
USD $ 2.0-2.0 / Kilogram
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1-10 Metric Ton/Month
Dayang Chem (Hangzhou) Co.,Ltd.
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N-EthylbutylaMine
Cas No: 13360-63-9
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20 Metric Ton/Month
Henan Allgreen Chemical Co.,Ltd
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Factory Supply Butyl(ethyl)amine
Cas No: 13360-63-9
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Ality Chemical Corporation
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N-Butylethylamine
Cas No: 13360-63-9
USD $ 1.2-5.0 / Kiloliter
5 Kiloliter
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Chemwill Asia Co., Ltd.
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Ethylbutylamine CAS 13360-63-9
Cas No: 13360-63-9
USD $ 1.0-10.0 / Kilogram
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Hebei Nengqian Chemical Import and Export Co., LTD
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Manufacturer supply CAS 13360-63-9 with best quality
Cas No: 13360-63-9
USD $ 139.0-210.0 / Kilogram
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1000 Kilogram/Day
Zhuozhou Wenxi import and Export Co., Ltd
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1-Butanamine, N-ethyl- 13360-63-9
Cas No: 13360-63-9
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Shanghai Upbio Tech Co.,Ltd
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1-Butanamine, N-ethyl-
Cas No: 13360-63-9
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Shandong Hanjiang Chemical Co., Ltd.
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1-Butanamine, N-ethyl-
Cas No: 13360-63-9
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Henan Wentao Chemical Product Co., Ltd.
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Ethylbutylamine
Cas No: 13360-63-9
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Xiamen Hisunny Chemical Co.,Ltd
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13360-63-9 Usage

Chemical Properties

Colorless to light yellow liqui

Uses

Intermediate.

General Description

A colorless liquid with an ammonia-like odor. Insoluble in water and less dense than water. Flash point 65°F. Vapors much heavier than air. Liquid and vapors strongly irritate skin, eyes and mucous membranes. Contact with liquid may cause burns.

Air & Water Reactions

Highly flammable. Insoluble in water.

Reactivity Profile

Ethylbutylamine can react vigorously with oxidizing materials . Neutralizes acids in exothermic reactions to form salts plus water. May be incompatible with isocyanates, halogenated organics, peroxides, phenols (acidic), epoxides, anhydrides, and acid halides. Flammable gaseous hydrogen may be generated in combination with strong reducing agents, such as hydrides.

Hazard

Flammable, dangerous fire risk. Toxic by ingestion.

Health Hazard

INHALATION: Irritation of mucous membranes and lungs. EYES: Irritation. Corrosive, may cause blindness - Irreversible. SKIN: Irritation. Corrosive. INGESTION: Nausea and salivation.

Check Digit Verification of cas no

The CAS Registry Mumber 13360-63-9 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,3,3,6 and 0 respectively; the second part has 2 digits, 6 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 13360-63:
(7*1)+(6*3)+(5*3)+(4*6)+(3*0)+(2*6)+(1*3)=79
79 % 10 = 9
So 13360-63-9 is a valid CAS Registry Number.

InChI:InChI=1/C6H15N/c1-3-5-6-7-4-2/h7H,3-6H2,1-2H3/p+1

13360-63-9 Well-known Company Product Price

Brand
(Code)Product description
CAS number
Packaging
Price
Detail

Alfa Aesar
(B22881) N-Ethyl-1-butylamine, 99%
13360-63-9
250g
876.0CNY
Detail

Alfa Aesar
(B22881) N-Ethyl-1-butylamine, 99%
13360-63-9
1000g
1452.0CNY
Detail

13360-63-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name	Ethylbutylamine

1.2 Other means of identification

Product number	-
Other names	1-Butanamine, N-ethyl-

1.3 Recommended use of the chemical and restrictions on use

Identified uses	For industry use only.
Uses advised against	no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number	-
Service hours	Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13360-63-9 SDS

13360-63-9Synthetic route

: (4-{tris[2-(perfluorohexyl)ethyl]silyl}benzyl) (butyl)(ethyl)carbamate

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 16h;	80%

: 122-56-5
tributyl borane

: 81375-29-3
O-(p-toluenesulfonyl)-N-ethylhydroxylamine

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
In tetrahydrofuran for 2h; Ambient temperature;	77%

: 917-54-4
methyllithium

: 33704-65-3
Butyl-phenylsulfanylmethyl-amine; hydrochloride

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
In diethyl ether at -60℃;	76%

: 75-04-7
ethylamine

: 109-73-9
N-butylamine

A: 102-82-9
tributyl-amine

B: 13360-63-9
N-ethylbutylamine

C: 4444-68-2
N,N-diethylbutylamine

D: 4458-33-7
di-n-butylethylamine

E: 111-92-2
dibutylamine

F: 109-89-7
diethylamine

G: 121-44-8
triethylamine

Conditions

Conditions	Yield
With hydrogen at 200℃; under 6000.6 Torr; Reagent/catalyst; Temperature;	A n/a B 60.7% C n/a D n/a E n/a F n/a G n/a

...Expand

: 75-04-7
ethylamine

: 71-36-3
butan-1-ol

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With hydrogen at 150℃; under 3750.38 Torr; for 8h; Temperature; Pressure; Reagent/catalyst;	55.3%
With hydrogen; nickel at 150℃;

: 109-74-0
propyl cyanide

: 64-17-5
ethanol

A: 13360-63-9
N-ethylbutylamine

B: 4853-56-9
(butylidene)butylamine

C: 109-73-9
N-butylamine

Conditions

Conditions	Yield
With Co(9.8%)/SiO2 catalyst; hydrogen at 129.84℃; under 9750.98 Torr; Reagent/catalyst; Temperature;	A 30.5% B 25.6% C 42.3%

: 14925-83-8
N,N-dichloro-n-butylamine

: 557-20-0
diethylzinc

A: 13360-63-9
N-ethylbutylamine

B: 109-73-9
N-butylamine

Conditions

Conditions	Yield
With Petroleum ether

: 1611-12-7
ethyl-butyliden-amine

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With nickel; Petroleum ether at 75℃; under 154457 Torr; Hydrogenation;
With ethanol; sodium
With ethanol; platinum Hydrogenation;

: 77228-69-4
N-benzyl-N-ethylbutan-1-amine

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With platinum(IV) oxide; acetic acid at 65 - 75℃; Hydrogenolyse;

: 75-04-7
ethylamine

: 123-72-8
butyraldehyde

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With ethanol; platinum Hydrogenation;
(i), (ii) H2, Pd-C, EtOH; Multistep reaction;
With potassium hydroxide; dipotassium hydrogenphosphate; phosphoric acid at 10 - 12℃; for 4h; electrochemical reductive amination, lead cathode, current density 0.05 A/cm2, pH 12; Yield given;

: 75-04-7
ethylamine

: 123-73-9
crotonaldehyde

A: 32280-46-9
N,N'-Diaethyl-1-methyl-1,3-propandiamin

B: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With methanol; nickel at 125℃; Hydrogenation;

: 75-04-7
ethylamine

: 123-73-9
crotonaldehyde

A: 13360-63-9
N-ethylbutylamine

B: 4444-68-2
N,N-diethylbutylamine

Conditions

Conditions	Yield
With methanol; nickel at 125℃; Hydrogenation;

: 64-17-5
ethanol

: 109-73-9
N-butylamine

A: 13360-63-9
N-ethylbutylamine

B: 111-92-2
dibutylamine

Conditions

Conditions	Yield
With nickel

: 6898-74-4
Acetaldehyd-butylimin

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With ethanol; platinum Hydrogenation;

: 109-65-9
1-bromo-butane

: 1946-09-4
diethyl N-ethylphosphoramidate

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
(i) aq. NaOH, HSO4, (ii) HCl; Multistep reaction;

: 26683-07-8
butyl-ethyl-tetrahydropyran-2-yl-amine

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
(hydrolysis);

: 74-85-1
ethene

: 109-73-9
N-butylamine

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With N,N,N,N,-tetramethylethylenediamine at 130 - 150℃; under 183877 Torr;

: 54944-19-3
phenyl-trichloromethyl-phosphinic acid ethyl ester

: 109-73-9
N-butylamine

: 13360-63-9
N-ethylbutylamine

: 64-67-5
diethyl sulfate

: 1077-18-5
N-benzylidenebutan-1-amine

: 13360-63-9
N-ethylbutylamine

: 97-94-9
triethyl borane

: 7332-00-5
n-butylazide

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
In xylene for 6h; Heating;	72 % Chromat.
In xylene for 6h; Rate constant; Heating;	72 % Chromat.

: 102711-05-7
C24H29NP(1+)*I(1-)

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With water; hydroxide

: (R)-5-Butylaminomethyl-2,7,8-trimethyl-2-((4R,8R)-4,8,12-trimethyl-tridecyl)-chroman-6-ol; hydrobromide

EtHal: EtHal

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With sodium hydroxide 1.) CH2Cl2, -20 deg C, 10 min, 2.) room temperature, 30 min, 3.) 70 deg C, 1 h; Yield given. Multistep reaction;

: (CO)5CrC(Me)(n-butylamine)

: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With Li{AlH4}

: 110-89-4
piperidine

: 885663-12-7
C14H21NO

A: 13707-23-8
N-(4-methylbenzoyl)piperidine

B: 13360-63-9
N-ethylbutylamine

Conditions

Conditions	Yield
With Al2(NMe2)6 In toluene at 90℃; for 16h; Equilibrium constant;

: 885663-12-7
C14H21NO

: 103-67-3
benzyl-methyl-amine

A: 13360-63-9
N-ethylbutylamine

B: 57409-40-2
4-methyl-N-benzyl-N-methylbenzamide

Conditions

Conditions	Yield
With Al2(NMe2)6 In toluene at 90℃; for 16h; Equilibrium constant;

: 13360-63-9
N-ethylbutylamine

: 287721-05-5
4-[phenyl(endo-8-methyl-8-azabicyclo[3.2.1]octan-3-yl)amino]benzoic acid

: N-butyl-N-ethyl-4-[(8-methyl-8-aza-bicyclo[3.2.1]oct-3-yl)-phenyl-amino]-benzamide

Conditions

Conditions	Yield
With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate Acylation;	100%

: 13360-63-9
N-ethylbutylamine

: 1286315-70-5
N-[3-(trimethylamino)methyl-4-hydroxyphenyl]-1,8-naphthalimide iodide

: 1286315-76-1
N-[3-(butylethylamino)methyl-4-hydroxyphenyl]-1,8-naphthalimide

Conditions

Conditions	Yield
In water; acetonitrile at 25℃; for 0.166667h; Quantum yield; Inert atmosphere; Irradiation;	100%

: 13360-63-9
N-ethylbutylamine

: 175140-70-2
4-N-(2,4,6-trimethylphenyl)-6-chloro-2-methyl-5-nitropyrimidin-4-amine

: 175139-13-6
4-N-(2,4,6-trimethylphenyl)-6-(N-n-butylethylamino)-2-methyl-5-nitropyrimidin-4-amine

Conditions

Conditions	Yield
With triethylamine In acetone Ambient temperature;	98%

: 75-15-0
carbon disulfide

: 13360-63-9
N-ethylbutylamine

: 163594-66-9
(N-ethyl-N'-n-butyldithiocarbamato) sodium

Conditions

Conditions	Yield
Stage #1: N-ethylbutylamine With sodium hydroxide In methanol; water at 0℃; for 0.333333h; Stage #2: carbon disulfide In methanol; water at 20℃;	98%
Stage #1: N-ethylbutylamine With sodium hydroxide In methanol; water at 0℃; for 0.333333h; Stage #2: carbon disulfide In methanol; water at 0 - 20℃;	98%
With sodium hydroxide In water	98%
With sodium hydroxide In water for 2h; Cooling with ice;

: 1945-84-2
2-ethynylpyridine

: 13360-63-9
N-ethylbutylamine

: (E)-N-ethyl-N-(2-(pyridine-2-yl)vinyl)butan-1-amine

Conditions

Conditions	Yield
With ethylene glycol at 150℃; for 8h; Inert atmosphere; Sealed tube; Green chemistry; regioselective reaction;	98%

: 13360-63-9
N-ethylbutylamine

: 169882-29-5
3-[2-bromo-4-(1-methylethyl)phenyl]-7-chloro-5-methyl-3H-1,2,3-triazolo[4,5-d]pyrimidine

: [3-(2-bromo-4-isopropyl-phenyl)-5-methyl-3H-[1,2,3]triazolo[4,5-d]pyrimidin-7-yl]-butyl-ethyl-amine

Conditions

Conditions	Yield
With triethylamine In ethanol Heating;	97%

: 13360-63-9
N-ethylbutylamine

: 1-methyl-3-{4-[tris-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-silanyl]-benzyloxycarbonyl}-3H-imidazol-1-ium; trifluoro-methanesulfonate

: (4-{tris[2-(perfluorohexyl)ethyl]silyl}benzyl) (butyl)(ethyl)carbamate

Conditions

Conditions	Yield
With dmap In dichloromethane at 20℃; for 16h;	91%

: 13360-63-9
N-ethylbutylamine

dichloromethylenedimethyliminium chloride: dichloromethylenedimethyliminium chloride

: 672953-00-3
[bis-(ethylbutylamino)-dimethylguanidinium] chloride

Conditions

Conditions	Yield
Stage #1: N-ethylbutylamine; dichloromethylenedimethyliminium chloride With triethylamine In dichloromethane at 0 - 20℃; for 4h; Stage #2: With sodium hydroxide In water Stage #3: With hydrogenchloride In diethyl ether; water pH=7;	91%

: N,N'-bis[3-(trimethylammonio)methyl-4-hydroxyphenyl]-1,4,5,8-naphthalenetetracarboxylic diimide diiodide

: 13360-63-9
N-ethylbutylamine

: C40H44N4O6

Conditions

Conditions	Yield
Stage #1: N,N'-bis[3-(trimethylammonio)methyl-4-hydroxyphenyl]-1,4,5,8-naphthalenetetracarboxylic diimide diiodide; N-ethylbutylamine With sodium dithionite In water; acetonitrile at 25℃; for 0.5h; Stage #2: With air In water; acetonitrile for 0.166667h; cooling; Further stages.;	90%

: 2579-22-8
Phenylpropargyl aldehyde

: 13360-63-9
N-ethylbutylamine

: (Z)-3-(butyl(ethyl)amino)-1-phenylprop-2-en-1-one

Conditions

Conditions	Yield
In ethanol at 60℃; for 0.25h; regioselective reaction;	90%

: 13360-63-9
N-ethylbutylamine

: 157286-81-2
4-chloro-2,5-dimethyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo-[2,3-d]pyrimidine

: butyl[2,5-dimethyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl]ethylamine

Conditions

Conditions	Yield
	89%
In dimethyl sulfoxide at 130℃; for 3h;	88%

: 75-15-0
carbon disulfide

: 13360-63-9
N-ethylbutylamine

: 10025-82-8
indium(III) chloride

: 878385-08-1
tris(N,N-ethylbutyldithiocarbamato)indium(III)

Conditions

Conditions	Yield
With sodium hydroxide In methanol NaOH and N,N-ethylbutylamine were dissplved in MeOH, CS2 was dropped slowly at 0°C for 1 h, InCl3 was added; ppt. was filtered, dtied in vacuo, and recrystd.; elem. anal.;	89%

: 13360-63-9
N-ethylbutylamine

: 197803-09-1
7-chloro-5-methyl-3-(2,4,6-trimethyl-pyridin-3-yl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

: butyl-ethyl-[5-methyl-3-(2,4,6-trimethyl-pyridin-3-yl)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-7-yl]-amine

Conditions

Conditions	Yield
With triethylamine In ethanol Heating;	86%

: 110-52-1
1,4-dibromo-butane

: 13360-63-9
N-ethylbutylamine

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1119616-46-4
N-butyl-N-ethylpyrrolidinium bis(trifluoromethanesulfonyl)imide

Conditions

Conditions	Yield
Stage #1: 1,4-dibromo-butane; N-ethylbutylamine With potassium carbonate In water at 120℃; for 0.333333h; Autoclave; Microwave irradiation; Green chemistry; Stage #2: bis(trifluoromethane)sulfonimide lithium In water at 20℃; for 1h; Green chemistry;	86%

: 111-24-0
1,5-dibromo-pentane

: 13360-63-9
N-ethylbutylamine

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1174233-40-9
N-butyl-N-ethylpiperidinium bis(trifluoromethanesulfonyl)imide

Conditions

Conditions	Yield
Stage #1: 1,5-dibromo-pentane; N-ethylbutylamine With potassium carbonate In water at 120℃; for 0.666667h; Autoclave; Microwave irradiation; Green chemistry; Stage #2: bis(trifluoromethane)sulfonimide lithium In water at 20℃; for 1h; Green chemistry;	86%

: 13360-63-9
N-ethylbutylamine

: 3-[(benzyloxy)(5-bromopentanoyl)amino]propanoic acid tert-butyl ester

: tert-butyl 3-{N-(benzyloxy)-5-[butyl(ethyl)amino]pentanamido}propanoate

Conditions

Conditions	Yield
In acetonitrile Reflux;	86%

: 13360-63-9
N-ethylbutylamine

: 102536-14-1
C18H16NO2P

: 102536-06-1
N-Butyl-N-ethyl-N'-phenyl-hydrazine

Conditions

Conditions	Yield
	85%

: 17426-48-1
1-(propa-1,2-dien-1-yl)pyrrolidin-2-one

: 13360-63-9
N-ethylbutylamine

: C13H24N2O

Conditions

Conditions	Yield
With tetrakis(actonitrile)copper(I) hexafluorophosphate In tetrahydrofuran at 20℃; for 18h; Inert atmosphere; diastereoselective reaction;	85%

: 13360-63-9
N-ethylbutylamine

: 40307-11-7
1-ethyl-4-ethynylbenzene

: (E)-N-ethyl-N-(4-ethylstyryl)butan-1-amine

Conditions

Conditions	Yield
With ethylene glycol at 150℃; for 8h; Inert atmosphere; Sealed tube; Green chemistry; regioselective reaction;	85%

: 13360-63-9
N-ethylbutylamine

: 557099-37-3
2-chloro-1,3-dinitro-5-(trifluoromethylthio)benzene

: 2,6-dinitro-4-trifluoromethylthio-N-ethyl-N-butylaniline

Conditions

Conditions	Yield
In ethanol for 0.5h;	84%
In methanol for 0.5h; Heating;	84%

: 13360-63-9
N-ethylbutylamine

: 842158-34-3
1-chloro-2,6-dinitrobenzene-4-(pentafluorosulfanyl)benzene

: 2,6-dinitro-4-pentafluorosulfanyl-N-ethyl-N-butylaniline

Conditions

Conditions	Yield
In ethanol for 0.5h;	84%

13360-63-9Upstream product

13360-63-9Downstream Products

13360-63-9Relevant articles and documents

Selective one-pot synthesis of asymmetric secondary amines via N-alkylation of nitriles with alcohols

Segobia,Trasarti,Apesteguía

, p. 178 - 185 (2019/11/13)

The synthesis of asymmetric secondary amines (ASA) is commonly achieved by N-alkylation of primary amines with alcohols. Here, we investigated the ASA synthesis via the direct amination of alcohols with nitriles, which avoids the synthesis, separation and purification of the primary amines in a first step. Specifically, the ASA synthesis via N-alkylation of butyronitrile (BN) with primary (n-propanol, iso-butanol and n-octanol) and secondary (2‐propanol, 2‐butanol and 2‐octanol) alcohols was studied on SiO2-supported Co, Ni and Ru catalysts. Competitive BN hydrogenation‐condensation reactions formed dibutylamine (the symmetric secondary amine) and tertiary amines as main secondary products. On Co/SiO2, the ASA selectivities for BN/primary alcohol reactions were between 49 and 58% at complete BN conversion, forming dibutylamine and tertiary amines as byproducts. For BN/secondary alcohol reactions, Co/SiO2 formed selectively (ASA + dibutylamine) mixtures containing 78–85% of ASA, thereby showing that the alcohol amination with nitriles is an attractive alternative route for the synthesis of valuable asymmetric secondary amines.

N-ethyl-n-butylamine production method

-

Paragraph 0047; 0050; 0053, (2017/01/05)

The invention relates to a production method of N-ethyl-n-butylamine. According to the production method, n-butanol and monoethylamine are taken as raw materials; a supported non-noble metal catalyst is used under hydrogen conditions; and amination synthe

Catalytic hydrogenation of amides to amines under mild conditions

Stein, Mario,Breit, Bernhard

supporting information, p. 2231 - 2234 (2013/03/28)

Under (not so much) pressure: A general method for the hydrogenation of tertiary and secondary amides to amines with excellent selectivity using a bimetallic Pd-Re catalyst has been developed. The reaction proceeds under low pressure and comparatively low temperature. This method provides organic chemists with a simple and reliable tool for the synthesis of amines. Copyright

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CAS

13360-63-9

13360-63-9

Basic information

Chemical Properties

Safety Data

13360-63-9 Suppliers

Recommended suppliersmore

13360-63-9 Usage

Chemical Properties

Uses

General Description

Air & Water Reactions

Reactivity Profile

Hazard

Health Hazard

Check Digit Verification of cas no

13360-63-9 Well-known Company Product Price

13360-63-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

1.Identification

1.1 GHS Product identifier

1.2 Other means of identification

1.3 Recommended use of the chemical and restrictions on use

1.4 Supplier's details

1.5 Emergency phone number

13360-63-9Synthetic route

13360-63-9Upstream product

13360-63-9Downstream Products

13360-63-9Relevant articles and documents

Selective one-pot synthesis of asymmetric secondary amines via N-alkylation of nitriles with alcohols

Segobia,Trasarti,Apesteguía

, p. 178 - 185 (2019/11/13)

N-ethyl-n-butylamine production method

-

Paragraph 0047; 0050; 0053, (2017/01/05)

Catalytic hydrogenation of amides to amines under mild conditions

Stein, Mario,Breit, Bernhard

supporting information, p. 2231 - 2234 (2013/03/28)