100005-02-5Relevant academic research and scientific papers
NEW GENERATION OF THIOCARBONYL YLIDE AND ITS 1,3-CYCLOADDITION LEADING TO TETRAHYDROTHIOPHENE DERIVATIVES
Terao, Yoshiyasu,Tanaka, Masaki,Imai, Nobuyuki,Achiwa, Kazuo
, p. 3011 - 3014 (1985)
Thiocarbonyl ylide was found to be generated by thermolysis of bromo(trimethylsilylmethylthio)methyltrimethylsilane and its 1,3-cycloaddition provided a new method for synthesis of tetrahydrothiophenes.
Thiocarbonyl Ylides. VI. New Generation of Thiocarbonyl Ylides from Organosilicon Compounds Containing Sulfur and Their 1,3-Cycloadditions
Terao, Yoshiyasu,Aono, Masahiro,Imai, Nobuyuki,Achiwa, Kazuo
, p. 1734 - 1740 (2007/10/02)
Thermolysis of bromo(trimethylsilyl)methyltrimethylsilylmethyl sulfide was found to give a thiocarbonyl ylide, the 1,3-cycloaddition of which proved a new method for the synthesis of tetrahydrothiophenes.The effect of the silyl group of the ylide on the regio- and stereoselectivity in these 1,3-dipolar cycloaddtions is discussed.Keywords---thiocarbonyl ylide; 1,3-cycloaddition; organosilicon compound; thermolysis; tetrahydrothiophene; regioselectivity
