100445-54-3

Basic information

• Product Name: 3-[(2,3-dichlorophenyl)amino]-5,5-dimethylcyclohex-2-en-1-one
• Synonyms: 3-(2,3-Dichloro-phenylamino)-5,5-dimethyl-cyclohex-2-enone
• CAS NO: 100445-54-3
• Molecular Formula: C₁₄H₁₅Cl₂NO
• Molecular Weight: 284.181
• Mol File: 100445-54-3.mol
• Article Data: 2

Chemical Properties

• Boiling Point: 379.9°C at 760 mmHg
• Flash Point: 183.6°C
• Density: 1.283g/cm³
• Vapor Pressure: 5.66E-06mmHg at 25°C
• Refractive Index: 1.599
• CAS DataBase Reference: 3-[(2,3-dichlorophenyl)amino]-5,5-dimethylcyclohex-2-en-1-one(CAS DataBase Reference)
• NIST Chemistry Reference: 3-[(2,3-dichlorophenyl)amino]-5,5-dimethylcyclohex-2-en-1-one(100445-54-3)
• EPA Substance Registry System: 3-[(2,3-dichlorophenyl)amino]-5,5-dimethylcyclohex-2-en-1-one(100445-54-3)

Safety Data

• Hazardous Substances Data: 100445-54-3(Hazardous Substances Data)

Upstream product

• 126-81-8 dimedone 
• 608-27-5 2,3-dichloroaniline 

Downstream Products

• 100485-05-0 1-(2,3-Dichloro-phenyl)-3-hydroxy-3,6,6-trimethyl-3,5,6,7-tetrahydro-1H-indole-2,4-dione 

Relevant articles and documents

NaHSO4/SiO2: An efficient catalyst for the synthesis of β-enaminones and 2-methylquinolin-4(1H)-ones under solvent-free condition

An efficient and simplified protocol for NaHSO4/SiO2 catalyzed solvent-free synthesis of β-enaminone and 2-methylquinolin-4(1H)- one derivatives under microwave irradiation is described. A series of functionalized derivatives have been synthesized in shorter reaction times with moderate to good yields. The use of milder catalyst in non-conventional method offers significant advantages over conventional methods, such as higher selectivities, simplicity, solvent-free reaction and non-environmental polluting conditions.