102141-33-3Relevant articles and documents
Novel synthetic method to synthesize intermediate glycerophosphate from calcium glycerophosphate
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Paragraph 0050; 0053; 0053; 0054; 0055, (2018/10/19)
The invention relates to a novel synthetic method to synthesize intermediate glycerophosphate from calcium glycerophosphate, comprising the steps: adding glycerol into POCl3 and a catalyst under ice bath, allowing natural restoring to room temperature, stirring to allow reaction for 5-6 h, distilling in vacuum, and collecting glycerophosphate fraction. The catalyst is ionic-liquid-modified silica-supported pyrophosphoric acid catalyst.