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11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Cas No: 1024598-06-8
USD $ 100.0-100.0 / Kilogram 1 Kilogram 50 Metric Ton/Day Metric Ton/Day Zibo Hangyu Import&Export Co., Ltd Contact Supplier
11-Phenyl-11, 12-dihydroindolo[2,3-a]carbazole CAS NO.1024598-06-8
Cas No: 1024598-06-8
USD $ 2.0-2.0 / Gram 100 Gram 100 Metric Ton/Month Hebei yanxi chemical co.,LTD. Contact Supplier
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Cas No: 1024598-06-8
No Data 1 Kilogram 20 Metric Ton/Quarter Henan Allgreen Chemical Co.,Ltd Contact Supplier
High Quality 99% 1024598-06-8 11-phenylindolo[2,3-a]carbazole Manufacturer
Cas No: 1024598-06-8
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Cas No: 1024598-06-8
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
11-Phenyl-indolo[2,3-a]carbazole
Cas No: 1024598-06-8
USD $ 1.0-2.0 / Kilogram 1 Kilogram 100 Kilogram/Day Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Cas No: 1024598-06-8
USD $ 1.0-1.0 / Kilogram 1 Kilogram 2000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Cas No: 1024598-06-8
USD $ 45.0-45.0 / Gram 1 Gram 200 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
China Biggest factory Supply High Quality 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole CAS 1024598-06-8
Cas No: 1024598-06-8
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1024598-06-8 Usage

1024598-06-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole

1.2 Other means of identification

Product number -
Other names N-(2-Indanyl)aniline

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1024598-06-8 SDS

1024598-06-8Synthetic route

bromobenzene
108-86-1

bromobenzene

11,12-dihydroindolo[2,3-a]carbazole
60511-85-5

11,12-dihydroindolo[2,3-a]carbazole

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h;83%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 24h; Inert atmosphere; Reflux;75%
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 17h; Inert atmosphere;73%
9-phenyl-9H-carbazol-1-amine
855180-11-9

9-phenyl-9H-carbazol-1-amine

(2-bromophenyl)boronic acid
244205-40-1

(2-bromophenyl)boronic acid

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Stage #1: 9-phenyl-9H-carbazol-1-amine With hydrogen bromide; dihydrogen peroxide In water; acetonitrile at -20℃;
Stage #2: (2-bromophenyl)boronic acid With palladium diacetate; caesium carbonate; (RP,RP)-1,2-bis[(o-anisyl)(phenyl)phosphino]ethane In 1-methyl-pyrrolidin-2-one at 20℃; Inert atmosphere; Reflux;
78.4%
2-(2-nitrophenyl)-9-phenyl-9H-carbazole
1361125-94-1

2-(2-nitrophenyl)-9-phenyl-9H-carbazole

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 12h; Inert atmosphere;71.5%
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 24h; Inert atmosphere;55%
iodobenzene
591-50-4

iodobenzene

11,12-dihydroindolo[2,3-a]carbazole
60511-85-5

11,12-dihydroindolo[2,3-a]carbazole

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 3h; Inert atmosphere; Reflux;65%
With 18-crown-6 ether; copper; potassium carbonate In 1,2-dichloro-benzene for 12h; Reflux; Inert atmosphere;64%
With 18-crown-6 ether; copper In 1,2-dichloro-benzene for 12h; Reflux; Inert atmosphere;64%
bromobenzene
108-86-1

bromobenzene

tri-tert-butyl phosphine
13716-12-6

tri-tert-butyl phosphine

11,12-dihydroindolo[2,3-a]carbazole
60511-85-5

11,12-dihydroindolo[2,3-a]carbazole

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0) In water; toluene55%
iodobenzene
591-50-4

iodobenzene

indolo[2,3-a]carbazole
222-19-5

indolo[2,3-a]carbazole

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane for 24h; Inert atmosphere; Reflux;51%
phenylhydrazine hydrochloride
59-88-1

phenylhydrazine hydrochloride

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4.08 h / 20 - 65 °C / Inert atmosphere
1.2: 15 h / 100 °C
2.1: potassium carbonate; copper(l) iodide; quinoline / 72 h / 190 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere
1.2: 12 h / 100 °C
2.1: copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C
1.2: 100 °C
2.1: copper; potassium carbonate; 18-crown-6 ether / 1,2-dichloro-benzene / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere
1.2: 12 h / 100 °C
2.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: ethanol / 0.5 h
1.2: 10 h / 65 °C
2.1: copper; 18-crown-6 ether; potassium carbonate / 1,2-dichloro-benzene / 48 h / 180 °C
View Scheme
cyclohexane-1,2-dione
765-87-7

cyclohexane-1,2-dione

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4.08 h / 20 - 65 °C / Inert atmosphere
1.2: 15 h / 100 °C
2.1: potassium carbonate; copper(l) iodide; quinoline / 72 h / 190 °C / Inert atmosphere
View Scheme
phenyl hydrazine hydrochloride

phenyl hydrazine hydrochloride

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere
1.2: 12 h / 100 °C / Inert atmosphere
2.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere
View Scheme
(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid
1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; water; ethanol / 24 h / 120 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 12 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere
View Scheme
2-nitrophenyl bromide
577-19-5

2-nitrophenyl bromide

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; water; ethanol / 24 h / 120 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 12 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); calcium carbonate / 1,4-dioxane / 12 h / Reflux
2: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere
3: caesium carbonate; palladium diacetate; tri-tert-butyl phosphine / toluene / 20 °C / Inert atmosphere; Reflux
View Scheme
2-(2-nitrophenyl)-9-phenyl-9H-carbazole
1361125-94-1

2-(2-nitrophenyl)-9-phenyl-9H-carbazole

A

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

B

5-phenyl-5,11-dihydro-indolo[3,2-b]carbazole
1316311-27-9

5-phenyl-5,11-dihydro-indolo[3,2-b]carbazole

Conditions
ConditionsYield
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 24h; Inert atmosphere; Overall yield = 63 %;
benzene-1,4-diboronic acid bispinacol ester
99770-93-1

benzene-1,4-diboronic acid bispinacol ester

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); calcium carbonate / 1,4-dioxane / 12 h / Reflux
2: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere
3: caesium carbonate; palladium diacetate; tri-tert-butyl phosphine / toluene / 20 °C / Inert atmosphere; Reflux
View Scheme
2,2''-dinitro-p-terphenyl
34673-74-0

2,2''-dinitro-p-terphenyl

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere
2: caesium carbonate; palladium diacetate; tri-tert-butyl phosphine / toluene / 20 °C / Inert atmosphere; Reflux
View Scheme
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2,4‐bis({[1,1'‐biphenyl]‐4‐yl})‐6‐chloro‐1,3,5‐triazine

2,4‐bis({[1,1'‐biphenyl]‐4‐yl})‐6‐chloro‐1,3,5‐triazine

C51H33N5

C51H33N5

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide; mineral oil for 6h; Inert atmosphere;90%
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 12h;81%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-chloro-4-(4-chlorophenyl)-6-phenyl-1,3,5-triazine
30894-93-0

2-chloro-4-(4-chlorophenyl)-6-phenyl-1,3,5-triazine

C39H24ClN5

C39H24ClN5

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In toluene for 3h; Reflux;88%
iodobenzene
591-50-4

iodobenzene

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

11,12-diphenyl-11,12-dihydro-indolo[2,3-a]carbazole

11,12-diphenyl-11,12-dihydro-indolo[2,3-a]carbazole

Conditions
ConditionsYield
With 3,5-ditertbutyl salicylic acid; copper; potassium carbonate for 48h; Reflux; Inert atmosphere;87%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-bromo-5-phenyl-1,3-oxazole
92629-11-3

2-bromo-5-phenyl-1,3-oxazole

2-phenyl-5-(12-phenylindolo[2,3-a]carbazole-11(12H)-yl)oxazole

2-phenyl-5-(12-phenylindolo[2,3-a]carbazole-11(12H)-yl)oxazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h;86%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-bromobenzo[d]benzo[4,5]imidazo[2,1-b]thiazole
1611489-35-0

2-bromobenzo[d]benzo[4,5]imidazo[2,1-b]thiazole

C37H22N4S

C37H22N4S

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux;85%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

1,4-bromoiodobenzene
589-87-7

1,4-bromoiodobenzene

C30H19BrN2

C30H19BrN2

Conditions
ConditionsYield
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 3h; Reflux; Inert atmosphere;85%
With copper(l) iodide; potassium carbonate; rac-diaminocyclohexane In 5,5-dimethyl-1,3-cyclohexadiene Reflux;
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

C28H21Br

C28H21Br

C52H36N2

C52H36N2

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere;84.7%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

3'-bromospiro[fluorene-9,9'-xanthene]

3'-bromospiro[fluorene-9,9'-xanthene]

C49H30N2O

C49H30N2O

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere;84.7%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2'-bromo-10,10-dimethyl-10H-spiro[anthracene-9,9'-fluorene]

2'-bromo-10,10-dimethyl-10H-spiro[anthracene-9,9'-fluorene]

C52H36N2

C52H36N2

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere;84.7%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-chloro-5-fluoro-1-bromo-3-(2-phenylpropan-2-yl)benzene

2-chloro-5-fluoro-1-bromo-3-(2-phenylpropan-2-yl)benzene

C39H28BrClN2

C39H28BrClN2

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 120℃;84%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

C58H33ClN2

C58H33ClN2

C82H48N4

C82H48N4

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate In tetrahydrofuran at 80℃; for 12h; Inert atmosphere;82.1%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

3-bromo-5-chloro-1,1’-biphenyl
126866-35-1

3-bromo-5-chloro-1,1’-biphenyl

C36H23ClN2

C36H23ClN2

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In toluene for 6h; Reflux;81%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

C16H8F3NO3S2

C16H8F3NO3S2

C39H23N3S

C39H23N3S

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene at 130℃; for 3h;80%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

C21H11BrN2S

C21H11BrN2S

C45H26N4S

C45H26N4S

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane for 24h; Reflux;80%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

3-bromobenzo[d]benzo[4,5]imidazolo[2,1-b]thiazole

3-bromobenzo[d]benzo[4,5]imidazolo[2,1-b]thiazole

C37H22N4S

C37H22N4S

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux;80%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

3-bromobenzo[4’,5’]imidazo[2’,1’:2,3]thiazolo[5,4-b]pyridine
1465269-57-1

3-bromobenzo[4’,5’]imidazo[2’,1’:2,3]thiazolo[5,4-b]pyridine

C36H21N5S

C36H21N5S

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux;80%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-(4-bromobenzenyl)-4,6-diphenyl-1,3,5-triazine
23449-08-3

2-(4-bromobenzenyl)-4,6-diphenyl-1,3,5-triazine

11-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-12-phenyl-11,12-dihydroindolo[2,3-a]carbazole

11-(4-(4,6-diphenyl-1,3,5-triazin-2-yl)phenyl)-12-phenyl-11,12-dihydroindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 80℃; for 24h; Inert atmosphere;80%
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 110℃; for 5h; Buchwald-Hartwig Coupling; Inert atmosphere;50%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

3-bromobiphenyl
2113-57-7

3-bromobiphenyl

C36H24N2

C36H24N2

Conditions
ConditionsYield
With 1-dodecylbenzene; 3,5-ditertbutyl salicylic acid; copper; potassium carbonate for 18h; Inert atmosphere; Reflux;80%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

C33H20ClN3O

C33H20ClN3O

C57H35N5O

C57H35N5O

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux;80%
5-bromo-2-phenyl-1,3-thiazole
53715-67-6

5-bromo-2-phenyl-1,3-thiazole

11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-phenyl-5-(12-phenylindolo[2,3-a]carbazole-11(12H)-yl)thiazole

2-phenyl-5-(12-phenylindolo[2,3-a]carbazole-11(12H)-yl)thiazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h;79%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

2-chloro-4,6-diphenyl-1,3,5-triazine
3842-55-5

2-chloro-4,6-diphenyl-1,3,5-triazine

11-(4,6-diphenyl-1,3,5-triazin-2-yl)-12-phenyl-11,12-dihydroindolo[2,3-a]carbazole
1024598-01-3

11-(4,6-diphenyl-1,3,5-triazin-2-yl)-12-phenyl-11,12-dihydroindolo[2,3-a]carbazole

Conditions
ConditionsYield
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide at 60℃; for 12h;
78%
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide at 60℃; for 12h;
78%
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide for 1.16667h;
Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide for 4h;
54.6%
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide; paraffin oil at 20℃; for 0.5h;
Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide; paraffin oil at 20℃; for 7h;
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine
89972-76-9

4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine

C45H29N5

C45H29N5

Conditions
ConditionsYield
With copper(l) iodide; 18-crown-6 ether; potassium carbonate at 175℃; for 36h; Inert atmosphere;78%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

C30H16F3N5O3S

C30H16F3N5O3S

C53H31N7

C53H31N7

Conditions
ConditionsYield
With 1,10-Phenanthroline; potassium carbonate; copper(I) bromide In toluene at 110 - 120℃; for 7h; Inert atmosphere;76.2%
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

5-bromo-2,4-di(pyridin-2-yl)thiazole

5-bromo-2,4-di(pyridin-2-yl)thiazole

5-(12-phenylindolo[2,3-a]carbazole-11(12H)-yl)-2,4-di(pyridine-2-yl)thiazole

5-(12-phenylindolo[2,3-a]carbazole-11(12H)-yl)-2,4-di(pyridine-2-yl)thiazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h;76%
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