10480-25-8Relevant academic research and scientific papers
Imino Diels-Alder reactions: Efficient synthesis of 2-aryl-4-(2'- oxopyrrolidinyl-1')-1,2,3,4-tetrahydroquinolines catalyzed by Antimony(III) Sulfate
Srinivasa, Aswathanarayana,Mahadevan, Kittappa M.,Hulikal, Vijaykumar
, p. 255 - 259 (2008)
Antimony(III) sulfate is found to catalyze the imino Diels-Alder reaction of Schiff's bases with N-vinylpyrrolidin-2-one to afford 2-aryl-4-(2'- oxopyrrolidinyl-1')-1,2,3,4-tetrahydroquinolines. One-pot synthesis of 1,2,3,4-tetrahydroquinolines from 3-nit
Ru Nanoparticles-Loaded Covalent Organic Framework for Solvent-Free One-Pot Tandem Reactions in Air
Chen, Gong-Jun,Li, Xiao-Bo,Zhao, Chen-Chen,Ma, Hui-Chao,Kan, Jing-Lan,Xin, Yu-Bin,Chen, Cheng-Xia,Dong, Yu-Bin
supporting information, p. 2678 - 2685 (2018/03/13)
Condensation of benzene-1,3,5-tricarbohydrazide with benzene-1,4-dicarboxaldehyde generated a new covalent organic framework, COF-ASB (1), in which the organic units are held together via hydrazone linkage to form porous frameworks. COF-ASB (1) is highly crystalline and displays good chemical and thermal stability and is permanently porous. In addition, 1 can be an ideal support to load Ru nanoparticles (Ru NPs) to generate Ru@COF-ASB (2). The obtained composite material is able to highly promote one-pot tandem synthesis of imine products from benzyl alcohols and corresponding amines under solvent-free conditions in air.
Synthesis of some novel 2-substituted benzothiazole derivatives containing benzylamine moiety as monoamine oxidase inhibitory agents
Kaya, Betül,Sa?l?k, Begüm Nurpelin,Levent, Serkan,?zkay, Yusuf,Kaplanc?kl?, Zafer As?m
, p. 1654 - 1661 (2016/10/09)
In the present work, 12 new 2-(5-substituted-benzothiazol-2-ylsulfanyl)-N-(substitutedbenzyl)-N-(4-substitutedphenyl) acetamide derivatives (4a–l) was designed and synthesized. The structures of the synthesized compounds were clarified using Fourier trans
Mechanochemical milling promoted solvent-free imino Diels-Alder reaction catalyzed by FeCl3: Diastereoselective synthesis of cis-2,4-diphenyl-1,2,3,4-tetrahydroquinolines
Tan, Ya-Jun,Zhang, Ze,Wang, Fang-Jian,Wu, Hao-Hao,Li, Qing-Hai
, p. 35635 - 35638 (2014/11/07)
Under mechanochemical ball-milling at room temperature, FeCl3 promoted Diels-Alder cycloaddition of styrene with in situ generated N-aryl aldimines in the absence of any solvent afforded exclusively cis-2,4-diphenyltetrahydroquinolines in good to excellent yields within 90 minutes. The isolation work up just involves washing the resulting reaction mixture with water and recrystallization from EtOH-H2O. The advantages of high diastereoselectivity, short reaction time, free use of organic solvent, low cost, employment of cheap, easily available and nontoxic catalyst, and simple work-up procedure make this protocol a very efficient and green alternative to traditional methods for constructing these kinds of heterocyclic skeletons.
NOVEL 3,3-DIMETHYL TETRAHYDROQUINOLINE DERIVATIVES
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Page/Page column 104-105, (2011/11/01)
A compound of formula (I) as well as pharmaceutically acceptable salt thereof, wherein R1 to R5 have the significance given in claim 1, can be used as a medicament.
NOVEL 3,3-DIMETHYL TETRAHYDROQUINOLINE DERIVATIVES
-
Page/Page column 40, (2011/10/31)
A compound of formula (I) as well as pharmaceutically acceptable salt thereof, wherein R1 to R5 have the significance given in claim 1, can be used as a medicament.
AMINOHALOBORANE IN ORGANIC SYNTHESIS. VIII. A ONE-STEP SYNTHESIS OF 2-AMINOBENZHYDROLS FROM ANILINES
Toyoda, Tatsuo,Sasakura, Kazuyuki,Sugasawa, Tsutomu
, p. 173 - 176 (2007/10/02)
2-Aminobenzhydrols were obtained regiospecifically from anilines and benzaldehydes with the aid of phenyldichloroborane and triethylamine via N-anilinophenylchloroborane.
