106456-85-3Relevant articles and documents
Thioacetalization of carbonyl compounds by zeolite HSZ-360 as a new, effective heterogeneous catalyst
Ballini, Roberto,Barboni, Luciano,Maggi, Raimondo,Sartori, Giovanni
, p. 767 - 772 (1999)
Thioacetal can be efficiently obtained at room temperature by simply dissolving the appropriate carbonyl compounds and 1,2-ethanedithiol, in dichloromethane, with zeolite HSZ-360 as a new heterogeneous catalyst. Satisfactory to good yields are obtained ev
Iron(III) fluoride: A highly efficient and versatile catalyst for the protection of carbonyl compounds under solvent-free conditions
Bandgar, Babasaheb P.,Kamble, Vinod T.,Kulkarni, Ashwini
, p. 607 - 610 (2005)
Carbonyl compounds are successfully converted into oxathioacetals and dithioacetals with 2-mercaptoethanol and ethane-1,2-dithiol using a catalytic amount of iron(m) fluoride under solvent-free conditions. The catalysts were recovered and reused in variou
Indium-Catalyzed Reductive Dithioacetalization of Carboxylic Acids with Dithiols: Scope, Limitations, and Application to Oxidative Desulfurization
Nishino, Kota,Minato, Kohei,Miyazaki, Takahiro,Ogiwara, Yohei,Sakai, Norio
, p. 3659 - 3665 (2017/04/11)
In this study an InI3-TMDS (1,1,3,3-tetramethyldisiloxane) reducing system effectively catalyzed the reductive dithioacetalization of a variety of aromatic and aliphatic carboxylic acids with 1,2-ethanedithiol or 1,3-propanedithiol leading to the one-pot preparation of either 1,3-dithiolane derivatives or a 1,3-dithiane derivative. Also, the intact indium catalyst continuously catalyzed the subsequent oxidative desulfurization of an in situ formed 1,3-dithiolane derivative, which led to the preparation of the corresponding aldehydes.
Silica-supported phosphorus pentoxide: A reusable catalyst for S,S-acetalization of carbonyl groups under ambient conditions
Shaterian, Hamid Reza,Azizi, Kobra,Fahimi, Nafiseh
experimental part, p. 85 - 91 (2012/01/06)
Phosphorus pentoxide supported on silica gel (P2O 5/SiO2) efficiently acts as a highly active and reusable catalyst for cyclic and non-cyclic S,S-acetalization of a variety of carbonyl compounds under mild, solvent-free an