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1078-21-3

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Pharmaceutical grade 4-Amino-3-Phenylbutyric Acid phenibut 99% powder phenibut
Cas No: 1078-21-3
USD $ 1.0-2.0 / Kilogram 1 Kilogram 10 Metric Ton/Day Shaanxi Greenyo Biotech Co., Ltd. Contact Supplier
High purity 99% Phenibut Powder USP Standard manufacturer
Cas No: 1078-21-3
No Data 1 Gram 1 Metric Ton/Month Shaanxi Mingqi Chemical Co., Ltd Contact Supplier
4-Amino-3-phenylbutanoic acid
Cas No: 1078-21-3
No Data No Data No Data shanghai Longyu biotechnology Co.,Ltd Contact Supplier
Best price in stock Phenibut
Cas No: 1078-21-3
USD $ 5.0-10.0 / Kilogram 1 Kilogram 50000 Metric Ton/Month Shanlong Biotechnology (hebei) Co., Ltd. Contact Supplier
High purity 99% Phenibut Powder USP Standard manufacturer CAS NO.1078-21-3
Cas No: 1078-21-3
No Data 10 Gram 100 Metric Ton/Day Hebei ShengYang Biological Technology Co. Ltd Contact Supplier
Pharmaceutical Powder Nootropic Supplement Phenibut CAS 1078-21-3
Cas No: 1078-21-3
USD $ 1.0-1.0 / Gram 10 Gram 10 Kilogram/Day Hebei Yingong New Material Technology Co.,Ltd . Contact Supplier
Pharmaceutical Ingredients 99% Phenibut Powder
Cas No: 1078-21-3
USD $ 100.0-110.0 / Kilogram 1 Kilogram 1 Metric Ton/Week Shaanxi Yuantai Biological Technology Co., Ltd. Contact Supplier
Factory Supply 4-Amino-3-phenylbutanoic acid CAS 1078-21-3
Cas No: 1078-21-3
No Data 100 Gram 20000 Kilogram/Day Hubei XinRunde Chemical Co., Ltd Contact Supplier
Phenibut Nootropics powder
Cas No: 1078-21-3
No Data 1 Kilogram 500 Kilogram/Week Xi'an Yinherb Bio-Tech Co., Ltd. Contact Supplier
phenibut
Cas No: 1078-21-3
USD $ 31.0-52.0 / Kilogram 1 Kilogram 100 Kilogram/Day Shanghai Hohance Chemical Co., ltd Contact Supplier

1078-21-3 Usage

InChI:InChI=1/C10H13NO2.ClH/c11-7-9(6-10(12)13)8-4-2-1-3-5-8;/h1-5,9H,6-7,11H2,(H,12,13);1H

1078-21-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 19, 2017

Revision Date: Aug 19, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Amino-3-phenylbutyric acid hydrochloride

1.2 Other means of identification

Product number -
Other names fenigama

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1078-21-3 SDS

1078-21-3Synthetic route

4-nitro-3-phenylbutanoic acid
41441-41-2

4-nitro-3-phenylbutanoic acid

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol at 60℃; under 45004.5 Torr;98%
4-(1,3-dioxoisoindolin-2-yl)-3-phenyl-N-(quinolin-8-yl)butanamide

4-(1,3-dioxoisoindolin-2-yl)-3-phenyl-N-(quinolin-8-yl)butanamide

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
With hydrogenchloride In water at 130℃; for 24h; Sealed tube;95%
2-oxo-4-phenyl-3-ethoxycarbonylpyrrolidine
52450-32-5

2-oxo-4-phenyl-3-ethoxycarbonylpyrrolidine

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
With hydrogenchloride
4-phenylpyrrolidin-2-one

4-phenylpyrrolidin-2-one

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
With hydrogenchloride Heating;
3-cyano-3-phenyl propionic acid
14387-18-9

3-cyano-3-phenyl propionic acid

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In acetic acid under 15200 Torr;
(+-)-3-phenyl-glutaramic acid

(+-)-3-phenyl-glutaramic acid

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
With sodium hydroxide; sodium hypobromide
hydrogenchloride
7647-01-0

hydrogenchloride

3-phenyl-glutaric acid dihydrazide
72976-16-0

3-phenyl-glutaric acid dihydrazide

isopentyl nitrite
110-46-3

isopentyl nitrite

A

B

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
at 25℃; Kochen mit Bromwasserstoffsaeure;
benzyl alcohol

benzyl alcohol

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium hypochlorite; potassium bromide / water; dichloromethane / 0.21 h / 0 °C
2.1: potassium tert-butylate / toluene; methanol / 0.17 h / 20 °C / 4500.45 Torr / Inert atmosphere
2.2: 0.11 h / 25 °C / 4500.45 Torr / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / toluene; tetrahydrofuran / 1 h / 50 °C / 6000.6 Torr
4.1: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr
5.1: hydrogen; palladium 10% on activated carbon / methanol / 60 °C / 45004.5 Torr
View Scheme
benzaldehyde
100-52-7

benzaldehyde

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / toluene; methanol / 0.17 h / 20 °C / 4500.45 Torr / Inert atmosphere
1.2: 0.11 h / 25 °C / 4500.45 Torr / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / toluene; tetrahydrofuran / 1 h / 50 °C / 6000.6 Torr
3.1: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr
4.1: hydrogen; palladium 10% on activated carbon / methanol / 60 °C / 45004.5 Torr
View Scheme
methyl cinnamate
103-26-4

methyl cinnamate

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / toluene; tetrahydrofuran / 1 h / 50 °C / 6000.6 Torr
2: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr
3: hydrogen; palladium 10% on activated carbon / methanol / 60 °C / 45004.5 Torr
View Scheme
4-nitro-3-phenylbutanoic acid methyl ester
34687-03-1

4-nitro-3-phenylbutanoic acid methyl ester

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium hydroxide; water / toluene / 1 h / 50 °C / 3750.38 Torr
2: hydrogen; palladium 10% on activated carbon / methanol / 60 °C / 45004.5 Torr
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

2-Fluorobenzaldehyde
446-52-6

2-Fluorobenzaldehyde

methyl 2,4-dioxopentanoate
20577-61-1

methyl 2,4-dioxopentanoate

4-[3-acetyl-2-(2-fluoro-phenyl)-4-hydroxy-5-oxo-2,5-dihydro-pyrrol-1-yl]-3-phenyl-butyric acid

4-[3-acetyl-2-(2-fluoro-phenyl)-4-hydroxy-5-oxo-2,5-dihydro-pyrrol-1-yl]-3-phenyl-butyric acid

Conditions
ConditionsYield
In ethanol; water at 20℃; for 12h; Condensation;78%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

4-((tert-butoxycarbonyl)amino)-3-phenylbutanoic acid
189014-01-5

4-((tert-butoxycarbonyl)amino)-3-phenylbutanoic acid

Conditions
ConditionsYield
With sodium hydroxide In water; tert-butyl alcohol at 0 - 20℃;73%
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

benzyl alcohol
100-51-6

benzyl alcohol

C17H19NO2*(x)ClH

C17H19NO2*(x)ClH

Conditions
ConditionsYield
With thionyl chloride at 0 - 20℃; for 16h;66%
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

N,N'-diisopropyl-O-methylisourea
54648-79-2

N,N'-diisopropyl-O-methylisourea

C13H19NO2
129453-46-9

C13H19NO2

Conditions
ConditionsYield
In methanol for 120h; Ambient temperature;65%
phthalic anhydride
85-44-9

phthalic anhydride

4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

4-(1,3-dioxoisoindolin-2-yl)-3-phenylbutanoic acid

4-(1,3-dioxoisoindolin-2-yl)-3-phenylbutanoic acid

Conditions
ConditionsYield
In ethanol for 3h; Reflux;62%
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

4-phenylpyrrolidin-2-one
1198-97-6

4-phenylpyrrolidin-2-one

Conditions
ConditionsYield
With potassium hydroxide
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

(RS)-2-(2-oxo-4-phenylpyrrolidin-1-yl)acetamide
77472-70-9

(RS)-2-(2-oxo-4-phenylpyrrolidin-1-yl)acetamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: potassium hydroxide / ethanol / 65 - 75 °C
2: ethanol / 65 - 75 °C
3: acetic acid / ethanol
4: Heating
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

4-[(2-amino-2-oxoethyl)amino]-3-phenylbutanoic acid

4-[(2-amino-2-oxoethyl)amino]-3-phenylbutanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol / 65 - 75 °C
2: ethanol / 65 - 75 °C
3: acetic acid / ethanol
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

4-[bis(2-amino-2-oxoethyl)amino]-3-phenylbutanoic acid sodium salt

4-[bis(2-amino-2-oxoethyl)amino]-3-phenylbutanoic acid sodium salt

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: potassium hydroxide / ethanol / 65 - 75 °C
2: ethanol / 65 - 75 °C
3: acetic acid / ethanol
4: sodium hydroxide / ethanol / 65 - 75 °C
5: ethanol / 65 - 75 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

C10H12NO2(1-)*K(1+)

C10H12NO2(1-)*K(1+)

Conditions
ConditionsYield
With potassium hydroxide In ethanol at 65 - 75℃;
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

C12H15N2O3(1-)*K(1+)

C12H15N2O3(1-)*K(1+)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium hydroxide / ethanol / 65 - 75 °C
2: ethanol / 65 - 75 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

C12H15N2O3(1-)*Na(1+)

C12H15N2O3(1-)*Na(1+)

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: potassium hydroxide / ethanol / 65 - 75 °C
2: ethanol / 65 - 75 °C
3: acetic acid / ethanol
4: sodium hydroxide / ethanol / 65 - 75 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

N-(4-hydroxy-2-phenylbutyl)-2H-benzo[e][1,2,4]thiadiazine-3-carboxamide 1,1-dioxide

N-(4-hydroxy-2-phenylbutyl)-2H-benzo[e][1,2,4]thiadiazine-3-carboxamide 1,1-dioxide

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: sodium hydroxide / water; tert-butyl alcohol / 0 - 20 °C
2.1: potassium carbonate / tetrahydrofuran / 0.25 h / 20 °C
2.2: 20 °C
3.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C
4.1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 20 °C
5.1: sodium hydroxide / 3 h / 20 °C
6.1: borane-THF / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

tert-butyl (3-amino-2-phenylpropyl)carbamate
437708-57-1

tert-butyl (3-amino-2-phenylpropyl)carbamate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ethanol / 3 h / Reflux
2: triethylamine; diphenyl phosphoryl azide / 1,4-dioxane / 100 °C
3: hydrazine hydrate / ethanol / 2 h / 80 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

tert-butyl (3-(1,1-dioxido-2H-benzo[e][1,2,4]thiadiazine-3-carboxamido)-2-phenylpropyl)carbamate

tert-butyl (3-(1,1-dioxido-2H-benzo[e][1,2,4]thiadiazine-3-carboxamido)-2-phenylpropyl)carbamate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: ethanol / 3 h / Reflux
2.1: triethylamine; diphenyl phosphoryl azide / 1,4-dioxane / 100 °C
3.1: hydrazine hydrate / ethanol / 2 h / 80 °C
4.1: sodium hydrogencarbonate / dichloromethane / 0.17 h / 20 °C
4.2: 1 h / 20 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

N-(3-amino-2-phenylpropyl)-2H-benzo[e][1,2,4]thiadiazine-3-carboxamide 1,1-dioxide hydrochloride

N-(3-amino-2-phenylpropyl)-2H-benzo[e][1,2,4]thiadiazine-3-carboxamide 1,1-dioxide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: ethanol / 3 h / Reflux
2.1: triethylamine; diphenyl phosphoryl azide / 1,4-dioxane / 100 °C
3.1: hydrazine hydrate / ethanol / 2 h / 80 °C
4.1: sodium hydrogencarbonate / dichloromethane / 0.17 h / 20 °C
4.2: 1 h / 20 °C
5.1: hydrogenchloride / ethyl acetate / 2 h / 20 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

methyl 4-amino-3-phenylbutanoate hydrochloride
25271-46-9

methyl 4-amino-3-phenylbutanoate hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water; tert-butyl alcohol / 0 - 20 °C
2.1: potassium carbonate / tetrahydrofuran / 0.25 h / 20 °C
2.2: 20 °C
3.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C
View Scheme
4-amino-3-phenylbutanoic acid
1078-21-3

4-amino-3-phenylbutanoic acid

methyl 4-(1,1-dioxido-2H-benzo[e][1,2,4]thiadiazine-3-carboxamido)-3-phenylbutanoate

methyl 4-(1,1-dioxido-2H-benzo[e][1,2,4]thiadiazine-3-carboxamido)-3-phenylbutanoate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water; tert-butyl alcohol / 0 - 20 °C
2.1: potassium carbonate / tetrahydrofuran / 0.25 h / 20 °C
2.2: 20 °C
3.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C
4.1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 20 °C
View Scheme

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