1116682-85-9Relevant academic research and scientific papers
Heterocyclic synthesis using nitrilimines: Part 9. Synthesis of new 1,3,4-thiadiazin-5-one derivatives
Dalloul, Hany M.,Mohamed, El-Hossain A. R.,El-Shorafa, Ali Z.
experimental part, p. 585 - 590 (2009/02/03)
A series of new 3,5,6-thiadiaza-4-hexenoates (4a-k) were synthesized from the reaction of the corresponding hydrazonoyl halides 1 with ethyl mercaptoacetate (3). These compounds underwent intramolecular cyclization to 1,3,4-thiadiazin-5-one derivatives (5a-k) in the presence of MeONa or LiH. The structures of the synthesized compounds were confirmed by their elemental analyses and spectral data.
