1136-27-2Relevant academic research and scientific papers
Microwave-accelerated methylation of starch
Singh, Vandana,Tiwari, Ashutosh
, p. 151 - 154 (2008)
A novel microwave-accelerated method for methylating soluble starch is described. Soluble starch could be fully methylated in 72% yield within 4.66 min using iodomethane and 30% potassium hydroxide under microwave irradiation. The completely methylated starch thus obtained was hydrolyzed with 60% HCO2H for 1.5 min under 80% MW power, followed by 0.05 M H2SO4 for 2.0 min under 100% MW power. The partially methylated monosaccharides were separated by preparative paper chromatography and identified by their melting points and optical rotations.
NEM LIGNANS FROM THE HEARTWOOD OF CLEISTANTHUS COLLINUS
Anjaneyulu, A. S. R.,Ramaiah, P. Atchuta,Row, L. Ramachandra,Venkateswarlu, R.,Pelter, A.,Ward, R. S.
, p. 3641 - 3652 (2007/10/02)
The isolation and characterisation of five new compounds and nine known compounds from the heartwood of Cleistanthus collinus are reported.The new compounds are wodeshiol 16, 3,4-dihydrotaiwanin C 20, and three new glycosides 24, 25 and 26 of diphyllin and taiwanin E.The 1H and 13C NMR spectra of these compounds are also reported.
