113855-10-0Relevant articles and documents
Process for producing azacycloalkane derivatives
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, (2008/06/13)
A process for producing an azacycloalkane derivative represented by the following general formula (II): STR1 wherein m is an integer of from 1 to 3, n2 is an integer of from 2 to 10, and R represents an alkyl group having 3 to 12 carbon atoms, characterized by reacting a 1-(n-alkenyl)-azacycloalkan-2-one represented by the following general formula (I): STR2 wherein m is an integer of from 1 to 3, and n1 is an integer of from 0 to 8, with an alkyl mercaptan in the presence of a radical initiator in an organic solvent, treating the reaction mixture thus obtained with a reducing agent in a water-containing organic solvent, and then purifying the treated mixture by distillation.