114382-95-5Relevant academic research and scientific papers
Nano-WO3-supported sulfonic acid: New, efficient and high reusable heterogeneous nano catalyst
Amoozadeh, Ali,Rahmani, Salman
, p. 96 - 107 (2014/12/11)
Nano-WO3-supported sulfonic acid [n-WO3-SO3H (n-WSA)] is easily prepared from the reaction of nano WO3 with chlorosulfonic acid as sulfonating agent. This new catalyst is characterized by X-ray diffraction(XRD), field emission scanning electron microscopy (FE-SEM), FT-IR spectroscopy, thermal gravimet-ric analysis (TGA), pH analysis and Hammett acidity function. Nano-WO3-supported sulfonic acid isused as an efficient and recyclable catalyst for some organic reactions such as synthesis of 1,8-dioxo-octahydroxanthene, tetrahydrobenzoxanthene and benzimidazolo quinazolinone derivatives. All of thereactions are very fast and the yields are excellent. The used catalyst was easily separated and reused for 10 runs without appreciable loss of its catalytic activity.
Nano-WO3-supported sulfonic acid: New, efficient and high reusable heterogeneous nano catalyst
Amoozadeh, Ali,Rahmani, Salman
, p. 96 - 107 (2015/02/18)
Nano-WO3-supported sulfonic acid [n-WO3-SO3H (n-WSA)] is easily prepared from the reaction of nano WO3 with chlorosulfonic acid as sulfonating agent. This new catalyst is characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), FT-IR spectroscopy, thermal gravimetric analysis (TGA), pH analysis and Hammett acidity function. Nano-WO3-supported sulfonic acid is used as an efficient and recyclable catalyst for some organic reactions such as synthesis of 1,8-dioxo-octahydroxanthene, tetrahydrobenzoxanthene and benzimidazolo quinazolinone derivatives. All of the reactions are very fast and the yields are excellent. The used catalyst was easily separated and reused for 10 runs without appreciable loss of its catalytic activity.
Chitosan synergistically enhanced by successive Fe3O4 and silver nanoparticles as a novel green catalyst in one-pot, three-component synthesis of tetrahydrobenzo[α]xanthene-11-ones
Mohammadi, Reza,Eidi, Esmaiel,Ghavami, Monireh,Kassaee, Mohammad Zaman
, p. 309 - 316 (2014/08/05)
Chitosan (CS) is modified with Fe3O4 nanoparticles composite through in situ co-precipitation of Fe3+ and Fe 2+ ions via NH4OH in an aqueous solution, resulting in magnetic Fe3O4
Niobium pentachloride catalyzed one-pot multicomponent condensation reaction of β-naphthol, aryl aldehydes and cyclic 1, 3-dicarbonyl compounds
Nasseri, Mohammad A.,Allahresani, Ali,Esmaeili, Abbas A.
, p. 91 - 96 (2014/03/21)
Niobium pentachloride catalyzed one-pot multicomponent condensation reaction of β-naphthol, aryl aldehydes and cyclic 1,3-dicarbonyl compounds. Thus, a variety of 8,9,10,12-tetrahydrobenzo[α] xanthen-11-one derivatives were produced in good to excellent y
Methanesulfonic acid-catalyzed one-pot synthesis of 12-aryl or 12-alkyl-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one derivatives
Liu, Yu-Heng,Li, Lei
, p. 861 - 864 (2012/10/29)
An efficient synthesis of 12-aryl or 12-alkyl-8,9,10,12-tetrahydrobenzo[a] xanthen-11-one derivatives has been developed under solvent-free conditions by one-pot condensation of aldehydes, 2-naphthol, and cyclic 1,3-dicarbonyl compounds in the presence of
A multicomponent, solvent-free, one-pot synthesis of benzoxanthenones catalyzed by HY zeolite: Their anti-microbial and cell imaging studies
Rama, Velladurai,Kanagaraj, Kuppusamy,Pitchumani, Kasi
supporting information; experimental part, p. 1018 - 1024 (2012/03/26)
An atom-economical, multicomponent condensation of naphthols, aldehydes, and cyclic 1,3-dicarbonyl compounds catalyzed by HY zeolites under solvent-free conditions is reported. This ecofriendly protocol offers several advantages such as a green and cost-e
Manganese perchlorate-catalyzed greener synthesis of 12-aryl or 12-alkyl-8,9,10,12- tetrahydrobenzo[alpha]xanthen-11-one derivatives under ultrasonication
Kaur, Bhupinder,Parmar, Anupama,Kumar, Harish
experimental part, p. 447 - 453 (2011/11/14)
A greener and more efficient protocol for the synthesis of 12-aryl or 12-alkyl-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one derivatives has been developed via one-pot, three-component reaction of aromatic aldehydes, 2-naphthol, and 1,3-cyclohexadione or 5,5
NMR spectral and structural studies on some xanthenones and their thiosemicarbazone derivatives: Crystal and molecular structure of 12-(2-chlorophenyl)-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one
Sethukumar,Vithya,Udhaya Kumar,Arul Prakasam
experimental part, p. 8 - 16 (2012/03/12)
A series of 12-aryl-8,9,10,12-tetrahydrobenzo[a]xanthen-11-ones [1a-9a] were prepared employing a three component one-pot reaction of aryl aldehyde, 2-naphthol and 1,3-cyclohexanedione using BF3·OEt2 as catalyst. Thiosemicarbazone de
One-pot, three-component condensation of aldehydes, 2-naphthol and 1,3-dicarbonyl compounds
Mo, Li-Ping,Chen, Hong-Li
experimental part, p. 157 - 161 (2011/04/17)
A practical and efficient procedure for the one-pot multicomponent couping of aryl aldehydes, 2-naphthol and cyclic 1,3-dicarbonyl compounds using perchloric acid adsorbed on silica gel (HClO4-SiO2) as a highly efficient, inexpensive
