1160477-41-7Relevant academic research and scientific papers
Microwave-assisted synthesis of substituted fluoroazines using KF·2H2O
Shestopalov, Anatoliy M.,Fedorov, Alexander E.,Rodinovskaya, Liudmila A.,Shestopalov, Alexander A.,Gakh, Andrei A.
experimental part, p. 5257 - 5259 (2009/12/06)
This Letter describes a new microwave-assisted fluorination of azines using hydrated potassium fluoride in untreated DMSO under atmospheric conditions. It is thought that microwave irradiation promotes desolvation of the fluorine anion leading to halide n
Synthesis of 3-cyano-2-fluoropyridines
Shestopalov, Anatoliy M.,Rodinovskaya, Ludmila A.,Fedorov, Alexander E.,Kalugin, Victor E.,Nikishin, Kirill G.,Shestopalov, Alexandr A.,Gakh, Andrei A.
experimental part, p. 236 - 240 (2009/07/11)
The synthesis of 3-cyano-2-fluoropyridines from readily available precursors was achieved via nucleophilic substitution of a leaving group in the 2-postion with KF or Bu4NF in polar aprotic solvents such as DMF and DMSO. Ionic tetrahydrothiophe
