1170322-26-5

Basic information

• Product Name: O,O-dibutyl S-p-tolyl phosphorothioate
• Synonyms: O,O-dibutyl S-p-tolyl phosphorothioate
• CAS NO: 1170322-26-5
• Molecular Weight: 316.401
• Mol File: 1170322-26-5.mol
• Article Data: 16

Chemical Properties

• CAS DataBase Reference: O,O-dibutyl S-p-tolyl phosphorothioate(CAS DataBase Reference)
• NIST Chemistry Reference: O,O-dibutyl S-p-tolyl phosphorothioate(1170322-26-5)
• EPA Substance Registry System: O,O-dibutyl S-p-tolyl phosphorothioate(1170322-26-5)

Safety Data

• Hazardous Substances Data: 1170322-26-5(Hazardous Substances Data)

Upstream product

• 1809-19-4 dibutyl hydrogen phosphite 
• 103-19-5 di(p-tolyl) disulfide 
• 106-45-6 para-thiocresol 
• 98-59-9 p-toluenesulfonyl chloride 
• 536-57-2 p-toluene sulfinic acid 
• 102-85-2 tri-n-butyl phosphite 
• 933-00-6 p-methylbenzenesulfenyl chloride 
• 109-47-7 dibutyl hydrogen phosphite 

Relevant articles and documents

Electrochemical Dehydrogenative Phosphorylation of Thiols

We report herein a new approach for the synthesis of organothiophosphates from phosphonates and thiols through electrochemical reaction. The reactions were conducted without the addition of oxidant, transition-metal base, or base at room temperature. This

Electrochemically driven synthesis of phosphorothioates from trialkyl phosphites and aryl thiols

A facile and elegant protocol for synthesis of phosphorothioates from trialkyl phosphites and aryl thiols via indirect electrochemical oxidation mediated by KI has been successfully developed. KI as a redox mediator, enabled the reaction of trialkyl phosp

An Alternative Metal-Free Aerobic Oxidative Cross-Dehydrogenative Coupling of Sulfonyl Hydrazides with Secondary Phosphine Oxides

An alternative metal-free, efficient and practical approach for the preparation of phosphinothioates is established via the aerobic oxidative cross-dehydrogenative coupling (CDC) of sulfonyl hydrazides with secondary phosphine oxides catalyzed by tetrabutylammonium iodide (TBAI) in the presence of atmospheric oxygen. The strategy provides an array of diverse phosphinothioates in good to excellent yields. Furthermore, two representative bioactive molecules are synthesized on up to gram scale by utilizing this method.

Synthetic method of thiophosphate compound

The invention discloses a synthetic method of a phosphorothioate compound. The preparation method comprises the following steps: with thiol as a reaction substrate and trichloroisocyanuric acid (TCCA)as an accelerant, reacting the reaction substrate and the accelerant in an organic solvent at normal temperature and normal pressure for 10-20 minutes, then adding phosphite triester, continuing reacting for 10-20 minutes, and after the reaction is finished, carrying out separation treatment to obtain the phosphorothioate compound. According to the synthesis method disclosed by the invention, thereaction is carried out at normal temperature and normal pressure without special requirements; reaction time is short; and reaction substrate universality is good.