1187744-33-7Relevant articles and documents
Preparation and characterization of a novel DABCO based tetra cationic ionic liquid as a reusable catalyst for the multi-component synthesis of 2H-indazolo[2,1-b]phthalazine-trione and [1,2,4]triazoloquinazolinone derivatives under solvent-free condition
Safari, Niloufar,Shirini, Farhad,Tajik, Hassan
, (2019/10/16)
In current study, a new DABCO based tetra cationic ionic liquid, formulated as [C4(H-DABCO)2][HSO4]4 is easily prepared and characterized using FT-IR, 1H NMR,13C NMR, TGA, and DTG analysis, and also pH-metric titration method. In continue, the efficiency of the prepared catalyst in the acceleration of the synthesis of 2H-indazolo[2,1-b]phthalazine-trione and [1,2,4]triazoloquinazolinone derivatives, is investigated. Simple experimental procedure, using available and low-cost starting materials for the preparation of the catalyst, reusability of the catalyst, isolation of products without using chromatographic methods, short reaction times, high isolated yields, and solvent-free conditions are the most important features of the present method.
Introduction of a novel nano sized n-sulfonated br?nsted acidic homogeneous catalyst for the promotion of the synthesis of 2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-Triones
Goli-Jolodar, Omid,Shirini, Farhad,Seddighi, Mohadeseh
, p. 591 - 603 (2017/12/12)
In this research work, 4,4-(butane-1,4-diyl)bis(1-sulfo-1,4-diazabicyclo[2.2.2]octane-1,4-diium) tetrachloride (NS-C4(DABCO-SO3H)2 ·4Cl) as a new nano-sized N-sulfonic acid was prepared and characterized using different types of spectroscopic methods incl
β-Cyclodextrine-SO3H: The most efficient catalyst for one-pot synthesis of 2H-indazolo[2,1-b]phthalazine-triones under solvent-free conditions
Atar, Amol B.,Lee, Sang Dong,Cho, Byung Gwon,Cho, Dae Won,Jeong, Yeon Tae
, p. 1707 - 1728 (2016/03/16)
An environmentally benign and efficient method has been developed for the synthesis of a series of 2H-indazolo[2,1-b]phthalazine-triones derivatives with β-cyclodextrine-SO3H as a recyclable catalyst by simply combining of various aldehydes wit