1191382-28-1Relevant articles and documents
Stabilizing N-tosyl-2-lithioindoles with bis(N,N′-dimethylaminoethyl) ether-a non-cryogenic procedure for lithiation of N-tosylindoles and subsequent addition to ketones
Wu, Jiang-Ping,Sanyal, Sanjit,Lu, Zhi-Hui,Senanayake, Chris H.
scheme or table, p. 5667 - 5669 (2011/02/24)
A practical procedure suitable for large scale lithiation of N-tosylindoles and subsequent addition to ketones is described. Bis(N,N′-dimethylaminoethyl) ether was found to stabilize 2-lithio-N-tosylindole 1A at -25 °C [The temperatures cited are internal