1192716-89-4Relevant academic research and scientific papers
Microwave-assisted cycloadditions of 2-alkynylbenzonitriles with sodium azide: selective synthesis of tetrazolo[5,1-a]pyridines and 4,5-disubstituted-2H-1,2,3-triazoles
Tsai, Chih-Wei,Yang, Shyh-Chyun,Liu, Ya-Ming,Wu, Ming-Jung
experimental part, p. 8367 - 8372 (2009/12/24)
Under microwave irradiation (75 W), treatment of 2-alkynylbenzonitriles with 1.5 equiv of sodium azide in DMSO at 140 °C gave 4,5-disubstituted-2H-1,2,3-triazoles in 60-99% yields. Additionally, adding 8 equiv of ZnBr2 and using 8 equiv of sodi
