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120116-88-3

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Cyazofamid in stock
Cas No: 120116-88-3
USD $ 2.0-2.0 / Kilogram 1 Kilogram 1-10 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality Cyazofamid supplier in China
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USD $ 1.0-3.0 / Metric Ton 1 Metric Ton 10 Metric Ton/Day Hebei yanxi chemical co.,LTD. Contact Supplier
Cyazofamid
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4-Chloro-2-cyano-N,N-dimethyl-5-(p-tolyl)-1H-imidazole-1-sulfonamide
Cas No: 120116-88-3
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
Cyazofamid CAS:120116-88-3
Cas No: 120116-88-3
USD $ 1.0-1.0 / Kilogram 1 Kilogram 2000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
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New production CAS 120116-88-3 with best quality
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USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
BLOOM TECH Advanced API/Technology support CYAZOFAMID CAS 120116-88-3
Cas No: 120116-88-3
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120116-88-3 Usage

Definition

ChEBI: A member of the class of imidazoles carrying dimethylsulfamyl, cyano, chloro and 4-tolyl substituents at positions 1, 2, 4 and 5 respectively. A fungicide used mainly for controlling Oomycete and Plasmodiophora diseases on potatoe and tomatoes. It is a skin and eye irritant and is moderately toxic to birds, most aquatic organisms, honeybees and earthworms.

Uses

Cyazofamid is a imidazole fungicide for use on food crops.

Uses

Agricultural fungicide.
InChI:InChI=1/C13H13ClN4O2S/c1-9-4-6-10(7-5-9)12-13(14)16-11(8-15)18(12)21(19,20)17(2)3/h4-7H,1-3H3

120116-88-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 20, 2017

Revision Date: Aug 20, 2017

1.Identification

1.1 GHS Product identifier

Product name cyazofamid

1.2 Other means of identification

Product number -
Other names Cyazofamid

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:120116-88-3 SDS

120116-88-3Synthetic route

5-chloro-4-(4-methylphenyl)-1H-imidazole-2-carbonitrile
120118-14-1

5-chloro-4-(4-methylphenyl)-1H-imidazole-2-carbonitrile

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
With potassium carbonate In ethyl acetate for 3h; Reflux;96.2%
With potassium carbonate In ethyl acetate for 6h; Solvent; Reflux;94%
With potassium carbonate In cyclohexane; ethyl acetate Concentration; Solvent; Reflux;86%
With potassium carbonate In ethyl acetate Reflux;
With potassium carbonate In ethyl acetate at 75℃; for 10.5h;68 g
C13H14N4O2S

C13H14N4O2S

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
With N-chloro-succinimide In acetonitrile at 20℃; for 4h; Time;95%
5-(4'-methylphenyl)imidazole-2-carboxylic acid

5-(4'-methylphenyl)imidazole-2-carboxylic acid

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: thionyl chloride / 5 h / 85 °C / Cooling with ice
2: ammonia / methanol / 36 h / 0 °C
3: thionyl chloride / 12 h / 85 °C
4: N-chloro-succinimide / acetonitrile / 3 h / 25 °C
5: potassium carbonate / ethyl acetate / 6 h / Reflux
View Scheme
5-(4'-methylphenyl)imidazole-2-carboxylic acid ethyl ester

5-(4'-methylphenyl)imidazole-2-carboxylic acid ethyl ester

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: ammonia / methanol / 36 h / 0 °C
2: thionyl chloride / 12 h / 85 °C
3: N-chloro-succinimide / acetonitrile / 3 h / 25 °C
4: potassium carbonate / ethyl acetate / 6 h / Reflux
View Scheme
C11H11N3O

C11H11N3O

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: thionyl chloride / 12 h / 85 °C
2: N-chloro-succinimide / acetonitrile / 3 h / 25 °C
3: potassium carbonate / ethyl acetate / 6 h / Reflux
View Scheme
para-methylacetophenone
122-00-9

para-methylacetophenone

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: selenium(IV) oxide / 1,4-dioxane; water / 5 h / 50 - 110 °C
2: hydroxylamine hydrochloride / water; methanol / 2 h / Reflux
3: thionyl chloride / ethyl acetate / 3 h / Reflux
4: potassium carbonate / ethyl acetate / 3 h / Reflux
View Scheme
Multi-step reaction with 4 steps
1.1: acetic acid; bromine / 7 h / 42 °C
2.1: hydroxylamine / methanol / 12 h / 50 °C
3.1: ammonia / methanol / 32 h / 0 °C
3.2: 10 h / 88 °C
3.3: 2.5 h / 28 °C
4.1: potassium carbonate / ethyl acetate / Reflux
View Scheme
4-methylphenylglyoxal
1075-47-4

4-methylphenylglyoxal

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydroxylamine hydrochloride / water; methanol / 2 h / Reflux
2: thionyl chloride / ethyl acetate / 3 h / Reflux
3: potassium carbonate / ethyl acetate / 3 h / Reflux
View Scheme
2,2-dibromo-1-(4-methylphenyl)ethanone
13664-98-7

2,2-dibromo-1-(4-methylphenyl)ethanone

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: hydroxylamine / methanol / 12 h / 50 °C
2.1: ammonia / methanol / 32 h / 0 °C
2.2: 10 h / 88 °C
2.3: 2.5 h / 28 °C
3.1: potassium carbonate / ethyl acetate / Reflux
View Scheme
1-hydroxy-4-(4-methylphenyl)-3-oxide-1H-imidazole-2-carboxaldehyde oxime

1-hydroxy-4-(4-methylphenyl)-3-oxide-1H-imidazole-2-carboxaldehyde oxime

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium metabisulfite / N,N-dimethyl acetamide; acetonitrile / 4 h / 80 - 105 °C
2: sulfuryl dichloride / N,N-dimethyl acetamide; acetonitrile / 20 - 25 °C
3: potassium carbonate / ethyl acetate / 10.5 h / 75 °C
View Scheme
4(5)-(4-tolyl)-1H-imidazole
670-91-7

4(5)-(4-tolyl)-1H-imidazole

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide
120116-88-3

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium carbonate / ethyl acetate / 6 h / 77 °C
2: copper(l) iodide; dipotassium peroxodisulfate / N,N-dimethyl-formamide / 12 h / 110 °C
3: N-chloro-succinimide / acetonitrile / 4 h / 20 °C
View Scheme

120116-88-3Upstream product

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