1219794-99-6Relevant articles and documents
Synthesis of per-deuterated alkyl amines for the preparation of deuterated organic pyromellitamide gelators
Yepuri, Nageshwar R.,Jamieson, Scott A.,Darwish, Tamim A.,Rawal, Aditya,Hook, James M.,Thordarson, Pall,Holden, Peter J.,James, Michael
supporting information, p. 2538 - 2541 (2013/06/27)
A general, direct and scalable synthesis of per-deuterated alkyl amines is reported, together with their incorporation into pyromellitamides, which form self-assembled gels in cyclohexane. The deuterium labelling of these gelators allows the study of the dynamic intermolecular interactions in these materials using solid-state 2H NMR spectroscopy.