1222074-16-9Relevant academic research and scientific papers
3, 4, 5-trisubstituted -1, 2, 4-triazole thioether derivative as well as synthesis method and application thereof
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Paragraph 0055; 0056, (2020/03/29)
The invention discloses 3,4,5-trisubstituted-1,2,4-triazole thioether derivatives, and a synthesis method and application thereof. The structural formula of the derivatives is disclosed as Formula I. The invention also discloses a synthesis method of the compounds and application of the compounds in bactericides for killing scab of wheat, green smut of rice, anthracnose of chili, late diseases of potato, seedling blight, Fusarium and Alternaria Nees.
Synthesis and crystal structure of novel sulfone derivatives containing 1,2,4-triazole moieties
Xu, Weiming,Song, Baoan,Bhadury, Pinaki,Song, Yang,Hu, Deyu
experimental part, p. 766 - 779 (2010/05/02)
Some 3-(Substituted methylthio)-4-phenyl-5-(3,4,5-trimethoxyphenyl)-4H-1,2, 4-triazole derivatives were synthesized in six steps starting from easily accessible gallic acid. The resulting sulfides were then catalytically oxidized to the title sulfones with H2O2. The products were obtained in high yield under mild conditions and practically devoid of any by-products. The structures were confirmed by elemental analysis, IR, 1H- and 13C-NMR spectral data. Furthermore, a detailed X-ray crystallography structural analysis of model triazole 7g was carried out.
