1224601-86-8Relevant academic research and scientific papers
Thiamine hydrochloride as a promoter for the efficient and green synthesis of 12-aryl-8,9,10,12 tetrahydrobenzoxanthene-11-one derivatives in aqueous micellar medium
Fatma, Shahin,Singh, Pravin K.,Ankit, Preyas,Shireen,Singh, Mandavi,Singh
, p. 6732 - 6736 (2013)
An environmentally benign, three-component, one-pot integrated chemical process has been developed for the synthesis of 12-aryl-8,9,10,12- tetrahydrobenzoxanthene-11-one by nucleophilic addition reaction between aldehyde and β-naphthol followed by Michael
Preparation and application of highly efficient and reusable TBAPIL@Si(CH2)3@nano-silica-based nano-catalyst for preparation of benzoxanthene derivatives
Agrwal, Akansha,Kumar, Vipin,Kasana, Virendra
, p. 2583 - 2595 (2021/02/26)
Tetrabutylammonium prolinate ionic liquid (TBAPIL) was prepared, and mesoporous silica nanoparticles (NPs) were synthesized. Both of these were linked through propyltriethoxysilane to prepare a reusable catalyst TBAPIL@Si(CH2)3@silica NPs (TBAPILS). The formation of TBAPIL was checked through Fourier-transform infrared spectroscopy (FT-IR) and nuclear magnetic resonance (NMR) analysis. X-ray diffraction analysis confirmed the structure of silica NPs and linking of TBPAIL on it. Transmission electron microscopy proved the flourishing development of silica NPs. Scanning electron microscopy graphs exposed the altering in morphology of silica NPs and TBAPILS. FT-IR analysis also confirmed the formation of TBAPILS catalyst. Moreover, the effectiveness of the TBAPILS was also checked for the synthesis of various derivatives of tetrahydrobenzoxanthenes-11-ones. The formation and structure of obtained compounds were confirmed by FT-IR, elemental analysis, 1HNMR and 13C NMR spectral analysis. The catalyst TBAPILS was found to be used successfully up to five cycles without significant loss of activity.
Preparation and characterization of Lewis acid grafted sulfonated carbon@titania composites for the multicomponent synthesis of 4H-pyrimido[2,1-b]benzothiazoles and benzoxanthenones under solvent-free conditions
Kour, Manmeet,Paul, Satya,Clark, James H.,Gupta, Vivek K.,Kant, Rajni
, p. 299 - 310 (2015/11/24)
A series of novel and highly efficient Lewis acids covalently grafted over sulfonic acid functionalized carbon@titania composites were successfully synthesized via sulfonation of carbon@titania composites followed by treatment with different Lewis acids l
Eco-friendly synthesis of tetrahydrobenzo[c]xanthenes catalyzed by functional ionic liquid in water
Yang, Jiaojiao,Yang, Jinming,Zhu, Ting,Wang, Pingping,Fang, Dong
, p. 1705 - 1710 (2014/02/14)
A clean procedure for the synthesis of tetrahydrobenzo[ c]xanthenes was established in the presence of a functional ionic liquid, 1-butyl-(4- dimethylamino)pyridinium hydroxide [BDMAP][OH]. The reaction was carried out via the one-pot multi-component cond
Pentafluorophenylammonium triflate (PFPAT): An efficient, practical, and cost-effective catalyst for one-pot condensation of β-naphthol, aldehydes and cyclic 1,3-dicarbonyl compounds
Khaksar, Samad,Behzadi, Nosratollah
, p. 845 - 848 (2013/02/23)
A pentafluorophenylammonium triflate (PFPAT) catalyst (10 mol%) efficiently promoted one-pot condensation of β-naphthol, aldehydes, and cyclic 1,3-dicarbonyl compounds in good to excellent yield under mild reaction conditions. These catalytic condensation
Ultrasound assisted synthesis of tetrahydrobenzo[c]xanthene-11-ones using CAN as catalyst
Sudha,Pasha
experimental part, p. 994 - 998 (2012/06/30)
Tetrahydrobenzo[c]xanthenes-11-ones was synthesized by a three component reaction of α-naphthol, aromatic aldehyde and dimedone. Ceric ammonium nitrate acts as a suitable eco-friendly catalyst for this method. Shorter reaction duration, mild reaction cond
A multicomponent, solvent-free, one-pot synthesis of benzoxanthenones catalyzed by HY zeolite: Their anti-microbial and cell imaging studies
Rama, Velladurai,Kanagaraj, Kuppusamy,Pitchumani, Kasi
supporting information; experimental part, p. 1018 - 1024 (2012/03/26)
An atom-economical, multicomponent condensation of naphthols, aldehydes, and cyclic 1,3-dicarbonyl compounds catalyzed by HY zeolites under solvent-free conditions is reported. This ecofriendly protocol offers several advantages such as a green and cost-e
A new strategy for the synthesis of benzoxanthenes catalyzed by proline triflate in water
Li, Jianjun,Lu, Lingmei,Su, Weike
supporting information; experimental part, p. 2434 - 2437 (2010/07/04)
Catalyzed by proline triflate, benzoxanthenes were obtained in good yields from the condensation of naphthols, aldehydes, and 1,3-dicarbonyl compounds in water. A possible mechanism of this reaction is proposed.
