124676-08-0Relevant articles and documents
REDUCTION OF ARYLALKYLAZOMETHINES WITH SODIUM BOROHYDRIDE
Dumpis, M. A.,Kudryashova, N. I.,Veresova, M. A.
, p. 1332 - 1337 (2007/10/02)
The secondary amines R1R2C6H3CH2CH(CH3)NHCHR5CHR6(CH2)nC6H3R3R4 were synthesized by the reduction of the respective azomethines with sodium borohydride.The reaction was conducted in anhydrous methanol in the presence of hydrogen chloride with the azomethine and hydrogen chloride in a molar ratio of 1:1.The yield was 50-90percent.The erythro and threo isomers were isolated, and the data from the IR spectra of the isomers are given.