1276420-96-2Relevant articles and documents
Chemical transformations of N-morpholinylacetic acid hydrazide and steric structure of its derivatives
Nurkenov,Fazylov,Satpaeva, Zh. B.,Kulakov,Turdybekov,Turdybekov,Talipov,Ibragimov
, p. 520 - 525 (2013)
The reaction of N-morpholinylacetic acid hydrazide with various isothiocyanates and potassium thiocyanate resulted in the corresponding potentially biologically active thiosemicarbazide derivatives. Potassium N′-(2-morpholin-4-ylacetyl)hydrazinocarbothioate was synthesized and involved into heterocyclization in acidic environment to yield cyclic 5-(morpholinomethyl)-1,3,4-thiadiazole-2-thione. The structure of the synthesized compounds was established by IR, 1H NMR spectroscopy, mass spectrometry, and XRD analysis.