1285540-40-0Relevant academic research and scientific papers
Microwave-assisted synthesis of propesticides 1,3,4-thiadiazole aminophosphonates
Wan, Rong,Wang, Peng,Han, Fen,Wang, Yao,Zhang, Jianqiang
, p. 864 - 870 (2011/04/22)
A novel and easy synthetic route to diethyl (5-substituted phenyl-1,3,4-thiadiazol-2-ylamino) (substituted phenyl) methylphosphonates has been achieved by the reaction of substituted benzylidene-5-(substituted phenyl)-1,3,4-thiadiazol-2-amines and diethyl phosphite under microwave irradiation. These 1,3,4-thiadiazole aminophosphonates were identified by infrared, 1H NMR, and elemental analyses. The target compounds were obtained in better yields (71-89%) and shorter time (10min) than with conventional heating.
