130274-83-8Relevant articles and documents
Properties and Reactions of Substituted 1,2-Thiazetidine 1,1-Dioxides: Acylation of β-Sultams at C-4, Reduction of 4-Acyl-β-sultams, and Stereochemistry of 4-(α-Hydroxyalkyl)-β-sultams
Mueller, Martin,Otto, Hans-Hartwig
, p. 171 - 178 (2007/10/02)
Acylation of N-silylated and 2,3-substituted 1,2-thiazetidine 1,1-dioxides (β-sultams) results in the formation of 4-acylated β-sultams 2 and 8.The desilylation of 2 to 3 is easily done with TBAF either on silica gel or in ethanolic solution.The acylated