1308490-11-0

Basic information

• Product Name: 2-(4-broMophenoxy)-5-nitropyriMidine
• Synonyms: 2-(4-broMophenoxy)-5-nitropyriMidine
• CAS NO: 1308490-11-0
• Molecular Formula: C10H6BrN3O3
• Molecular Weight: 296.07694
• Mol File: 1308490-11-0.mol
• Article Data: 2

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 2-(4-broMophenoxy)-5-nitropyriMidine(CAS DataBase Reference)
• NIST Chemistry Reference: 2-(4-broMophenoxy)-5-nitropyriMidine(1308490-11-0)
• EPA Substance Registry System: 2-(4-broMophenoxy)-5-nitropyriMidine(1308490-11-0)

Safety Data

• Hazardous Substances Data: 1308490-11-0(Hazardous Substances Data)

Upstream product

• 10320-42-0 2-Chloro-5-nitropyrimidine 
• 106-41-2 4-bromo-phenol 

Relevant articles and documents

Pyrocatechol derivative and preparation method thereof

The invention discloses a pyrocatechol derivative and a preparation method of the derivative. The preparation method of the derivative comprises the following steps of: (1) taking an aryl phenol compound as a substrate, and 2-chlorine-5-nitryl pyrimidine as an orienting group, slowly adding a redistilled tetrahydrofuran solvent ice bath into sodium hydride in the presence of nitrogen for reactionto form a pyrimidine aryl phenol compound intermediate, (2) taking iodobenzene diacetate as an oxidant and palladium acetate as a catalyst, catalyzing the pyrimidine aryl phenol compound intermediatefor C-H activating reaction in a solvent, performing swab-off, and chromatographic separation and purification to form an acetoxylated phenylamine derivative, and (3) allowing the acetoxylated phenylamine derivative to react in a tetrahydrofuran solvent by using hydrazine hydrate, and performing quenching, washing, extraction, drying, swab-off, and chromatographic separation and purification to form an ortho-aminophenol derivative. The first two steps of the method can be achieved in a pot, and small-scale production of above a 'gram' level can be even achieved.