131325-91-2Relevant academic research and scientific papers
Synthesis of Selenophosphinic and Tellurophosphinic Amides and Amidato Complexes. Crystal Structures of t-Bu2P(Te)NH(C6H11), > and 2>*C7H8
Bochmann, Manfred,Bwembya, Gabriel C.,Whilton, Nicola,Song, Xuejing,Hursthouse, Michael B.,et al.
, p. 1887 - 1892 (1995)
The reaction of t-Bu2PNHR' with selenium or tellurium affords the chalcogenophosphinic amides t-Bu2P(E)NHR' (E = Se or Te; R' = i-Pr or cyclo-C6H11).The compounds 2 were prepared similarly.The crystal structure of t-Bu2P(Te)NH(C6H11) was d
EINIGE NEUE THIOPHOSPHINSAEUREAMIDE R2P(S)NHR': SYNTHESE UND KERNRESONANZSPEKTROSKOPISCHE UNTERSUCHUNGEN
Kuchen, W.,Langsch, D.,Peters, W.
, p. 55 - 61 (2007/10/02)
P,P-Dialkylthiophosphinic acid amides R2P(S)HNR' (R=Me, iPr, tBu; R'=Me, Et, iPr, cHex, tBu, Ph, etc.) have been obtained by reaction of the corresponding aminophosphines with sulfur or by reaction of dimethylthiophosphorylhalides with primary amines.Their 31P- and 13C-NMR spectra are discussed.The di-t-butylthiophosphinic compounds proved to be remarkably stable against moisture and oxygen.
