132270-92-9Relevant articles and documents
On the route to the N-phosphoryl sulfamic acid
Mielniczak,Lopusinski
, p. 785 - 791 (2007/10/03)
Synthesis of the previously unknown N-diethyl phosphorosulfamate 15 was accomplished by direct sulfamation of diethyl phosphoroamidate 4 with sulfur trioxide-DMF complex 14. The acid 15 was isolated in form of benzyl-16 and cyclohexylammonium 17 salts, which were found to be unstable in water solution. The other possible routes to sulfamate 15 were briefly tested.
Organic Phoshorus Compounds. XVI. On the Chemistry of the Isocyanatophosphoric Acid Diethyl Ester
Moll, Rainer,Jentzsch, Renate,Fischer, Gerhard W.
, p. 439 - 443 (2007/10/02)
A one-pot procedure for preparing ureidophosphoric acid dialkyl esters 2 from POCl3, urea, and alcohols via ureidophosphoric acid dichloride 1 was worked out. 2 (R=Et) was used as starting material for isocyanatophosphoric acid diethyl ester (4, R=Et), th