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Borane-methyl sulfide complex Manufacturer/High quality/Best price/In stock
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Borane-dimethyl sulfide complex
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13292-87-0 Usage

Chemical Properties

clear colorless to light yellow solution
InChI:InChI=1/C2H6S.BH3/c1-3-2;/h1-2H3;1H3

13292-87-0 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (D1843)  Dimethyl Sulfide Borane  >90.0%(T) 13292-87-0 25mL 490.00CNY Detail
TCI America (D1843)  Dimethyl Sulfide Borane  >90.0%(T) 13292-87-0 100mL 1,250.00CNY Detail
Alfa Aesar (42965)  Borane-dimethyl sulfide complex, 2M in THF, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 100ml 536.0CNY Detail
Alfa Aesar (42965)  Borane-dimethyl sulfide complex, 2M in THF, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 500ml 2310.0CNY Detail
Alfa Aesar (42963)  Borane-dimethyl sulfide complex, 2M in toluene, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 100ml 1436.0CNY Detail
Alfa Aesar (42963)  Borane-dimethyl sulfide complex, 2M in toluene, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 500ml 5941.0CNY Detail
Alfa Aesar (L07705)  Borane-dimethyl sulfide complex, 94%    13292-87-0 25ml 529.0CNY Detail
Alfa Aesar (L07705)  Borane-dimethyl sulfide complex, 94%    13292-87-0 100ml 1519.0CNY Detail
Alfa Aesar (43327)  Borane-dimethyl sulfide complex, nominally 5M in ether, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 50ml 801.0CNY Detail
Alfa Aesar (43327)  Borane-dimethyl sulfide complex, nominally 5M in ether, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 250ml 2748.0CNY Detail
Alfa Aesar (42967)  Borane-dimethyl sulfide complex, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 5ml 198.0CNY Detail
Alfa Aesar (42967)  Borane-dimethyl sulfide complex, packaged under Argon in resealable ChemSeal? bottles    13292-87-0 25ml 495.0CNY Detail

13292-87-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name Borane-methyl sulfide complex

1.2 Other means of identification

Product number -
Other names Borane - Dimethyl Sulfide Complex

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13292-87-0 SDS

13292-87-0Synthetic route

A

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

B

dichloroborane-dimethyl sulfide

dichloroborane-dimethyl sulfide

Conditions
ConditionsYield
In not given equimolar mixt. of products not sepd., detd. by (11)B-NMR spectroscopy;
lithium borohydride

lithium borohydride

C8H14BBrS(CH3)2
70160-59-7

C8H14BBrS(CH3)2

A

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

B

9-bora-bicyclo[3.3.1]nonane
280-64-8

9-bora-bicyclo[3.3.1]nonane

Conditions
ConditionsYield
In tetrahydrofuran byproducts: LiBr; 0°C, 0.25 h; detected by 11B NMR;
boron dimethyl-trifluoro sulphide
353-43-5

boron dimethyl-trifluoro sulphide

hydrogen
1333-74-0

hydrogen

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

Conditions
ConditionsYield
With 1,2,2,6,6-pentamethylpiperidine In toluene at 75℃; under 15001.5 Torr; for 4h; Autoclave;> 90 %Spectr.
boron dimethyl-trifluoro sulphide
353-43-5

boron dimethyl-trifluoro sulphide

boron trifluoride diethyl etherate
109-63-7

boron trifluoride diethyl etherate

hydrogen
1333-74-0

hydrogen

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

Conditions
ConditionsYield
With 1,2,2,6,6-pentamethylpiperidine In toluene at 100℃; under 15001.5 Torr; for 2h; Autoclave;60 %Spectr.
dimethylsulfide
75-18-3

dimethylsulfide

diborane
19287-45-7

diborane

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

Conditions
ConditionsYield
at 0 - 5℃; for 1.25h; Inert atmosphere;
boron tribromide dimethyl sulfide complex
29957-59-3

boron tribromide dimethyl sulfide complex

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

dibromoborane dimethylsulfide
55671-55-1

dibromoborane dimethylsulfide

Conditions
ConditionsYield
In benzene at 80℃; for 18h; Inert atmosphere; Glovebox;100%
In not given molar ratio BH3SMe2:BBr3SMe2 1:2; followed by NMR;
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

2'-hydroxy-2-diphenylphosphinobiphenyl
155566-51-1

2'-hydroxy-2-diphenylphosphinobiphenyl

(2'-hydroxy-biphenyl-2-yl)-diphenylphosphane borane
917477-90-8

(2'-hydroxy-biphenyl-2-yl)-diphenylphosphane borane

Conditions
ConditionsYield
In tetrahydrofuran; dichloromethane (N2); addn. of soln. of borane complex in THF to soln. of phosphine deriv. in CH2Cl2 at room temp., stirring for 24 h; evapn., NMR;100%
formaldehyd
50-00-0

formaldehyd

Diethylphosphine
627-49-6

Diethylphosphine

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

(borane)diethylphosphinomethane alcohol
635689-45-1

(borane)diethylphosphinomethane alcohol

Conditions
ConditionsYield
Stage #1: Diethylphosphine; dimethylsulfide borane complex In tetrahydrofuran for 2h;
Stage #2: formaldehyd With potassium hydroxide In tetrahydrofuran; water for 4h;
100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

1-(dipropylphosphanylmethyl-propyl-phosphanyl)-propane
686353-30-0

1-(dipropylphosphanylmethyl-propyl-phosphanyl)-propane

C13H36B2P2
1422260-95-4

C13H36B2P2

Conditions
ConditionsYield
In diethyl ether for 2h; Inert atmosphere; Schlenk technique;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

[Ir(fac-bis[(2-diphenylphosphino)phenyl]phosphide)(COD)]
1420831-79-3

[Ir(fac-bis[(2-diphenylphosphino)phenyl]phosphide)(COD)]

[Ir(fac-bis[(2-diphenylphosphino)phenyl]phosphide)(BH3)(COD)]

[Ir(fac-bis[(2-diphenylphosphino)phenyl]phosphide)(BH3)(COD)]

Conditions
ConditionsYield
In toluene at 20℃; Inert atmosphere; Schlenk technique;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

N-benzhydryl-1,1-diphenylphosphinoamine
1425274-89-0

N-benzhydryl-1,1-diphenylphosphinoamine

C25H25BNP
1446469-42-6

C25H25BNP

Conditions
ConditionsYield
In toluene at 20℃; for 12h; Schlenk technique; Inert atmosphere; Glovebox;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

4-(dihexylamino)pyridine
95758-21-7

4-(dihexylamino)pyridine

4-dihexylaminopyridine borane

4-dihexylaminopyridine borane

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at 0℃; for 0.166667h; Schlenk technique;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

C26H24OP2

C26H24OP2

C26H30B2OP2

C26H30B2OP2

Conditions
ConditionsYield
In tetrahydrofuran; toluene for 16h; Schlenk technique; Inert atmosphere;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

C44H36Fe2OP2

C44H36Fe2OP2

C44H42B2Fe2OP2

C44H42B2Fe2OP2

Conditions
ConditionsYield
In tetrahydrofuran for 16h; Schlenk technique; Inert atmosphere;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

C19H32ClGeN

C19H32ClGeN

C19H35BClGeN

C19H35BClGeN

Conditions
ConditionsYield
In tetrahydrofuran; benzene at 20℃; for 0.5h; Inert atmosphere; Schlenk technique;100%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

4-methoxy-phenol
150-76-5

4-methoxy-phenol

tris(4-methoxiphenyloxy)borane
42080-75-1

tris(4-methoxiphenyloxy)borane

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 60℃; for 23h; Inert atmosphere; Schlenk technique;99.1%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

(1S,2R)-(+)-ephedrine
321-98-2

(1S,2R)-(+)-ephedrine

(2RP,4SC,5RC)-(+)-3,4-dimethyl-2,5-diphenyl-1,3,2-oxazaphospholidine borane

(2RP,4SC,5RC)-(+)-3,4-dimethyl-2,5-diphenyl-1,3,2-oxazaphospholidine borane

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; addn. of 1.3 equiv. of borane to ligand, stirring (room temp., overnight); solvent removal (vac.), chromy. (SiO2, Et2O/pentane=1:1);99%
(2R,5S)-2,3-diphenyl-1,3-diazaphosphabicyclo[3.3.0]octane

(2R,5S)-2,3-diphenyl-1,3-diazaphosphabicyclo[3.3.0]octane

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

(2R,5S)-2-phenyl-3-oxa-1-azaphosphabicyclo[3.3.0]octane-borane complex

(2R,5S)-2-phenyl-3-oxa-1-azaphosphabicyclo[3.3.0]octane-borane complex

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; addn. of 1.3 equiv. of borane to ligand, stirring (room temp., overnight); solvent removal (vac.), chromy. (SiO2, Et2O/pentane=1:1);99%
(2R,5S)-2,-phenyl-3-o-anisyl-1,3-diazaphosphabicyclo[3.3.0]octane

(2R,5S)-2,-phenyl-3-o-anisyl-1,3-diazaphosphabicyclo[3.3.0]octane

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

(2R,5S)-2-(2-methoxyphenyl)-3-oxa-1-aza-2-phosphabicyclo[3.3.0]octane(P-B)borane

(2R,5S)-2-(2-methoxyphenyl)-3-oxa-1-aza-2-phosphabicyclo[3.3.0]octane(P-B)borane

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; addn. of 1.3 equiv. of borane to ligand, stirring (room temp., overnight); solvent removal (vac.), chromy. (SiO2, Et2O/pentane=1:1);99%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

(NCN)0.5Si(NCN)CH(CH3)B(C2H4Si(NCN)0.5NCN)

(NCN)0.5Si(NCN)CH(CH3)B(C2H4Si(NCN)0.5NCN)

Conditions
ConditionsYield
With Si(CHCH2)(NCN)0.5 In toluene byproducts: SMe2; Ar-atmosphere; dropwise addn. of borane to Si-compd. at 0°C, slowwarming to room temp., stirring (room temp., 2 h); solvent removal (vac.), drying (70°C, 1E-3 mbar, 24 h); elem. anal.;99%
HSi(CHCH2)NCN

HSi(CHCH2)NCN

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

HSi(NCN)CH(CH3)B(C2H4SiHNCN)

HSi(NCN)CH(CH3)B(C2H4SiHNCN)

Conditions
ConditionsYield
In toluene byproducts: SMe2; Ar-atmosphere; dropwise addn. of borane to Si-compd. at 0°C, slowwarming to room temp., stirring (room temp., 2 h); solvent removal (vac.), drying (70°C, 1E-3 mbar, 24 h); elem. anal.;99%
CH3Si(CHCH2)NCN

CH3Si(CHCH2)NCN

dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

CH3Si(NCN)CH(CH3)B(C2H4Si(CH3)NCN)

CH3Si(NCN)CH(CH3)B(C2H4Si(CH3)NCN)

Conditions
ConditionsYield
In toluene byproducts: SMe2; Ar-atmosphere; dropwise addn. of borane to Si-compd. at 0°C, slowwarming to room temp., stirring (room temp., 2 h); solvent removal (vac.), drying (70°C, 1E-3 mbar, 24 h); elem. anal.;99%
dimethylsulfide borane complex
13292-87-0

dimethylsulfide borane complex

(s)-N-methylvalinol
78617-54-6

(s)-N-methylvalinol

(2R,4S)-3-methyl-4-isopropyl-2-phenyl-1,3,2-oxazaphospholidine-borane complex

(2R,4S)-3-methyl-4-isopropyl-2-phenyl-1,3,2-oxazaphospholidine-borane complex

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; addn. of 1.3 equiv. of borane to ligand, stirring (room temp., overnight); solvent removal (vac.), chromy. (SiO2, Et2O/pentane=1:1);99%

13292-87-0Upstream product

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Several per-O-methylated monosaccharides and polysaccharides were used as models in an attempt to identify more convenient reagents for accomplishing reductive cleavage of glycosidic linkages. Included in the model studies were methyl α- and β-d-glucopyranoside, methyl α- and β-d-mannopyrano...detailed

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