133088-94-5Relevant articles and documents
New and efficient synthesis of ω-nitroalcohols and spiroketals by chemio- and regioselective reductive cleavage of 2-nitrocycloalkanones
Ballini, Roberto,Petrini, Marino,Rosini, Goffredo
, p. 7531 - 7538 (2007/10/02)
ω-Nitroalcohols have been prepared by a new and efficient chemio- and regioselective reductive cleavage performed on 2-nitrocycloketones with sodium borohydride in acetonitrile / water. This reaction opens a more practical and convenient route to the synthesis of spiroketals.