135192-69-7Relevant articles and documents
Addition of Twisted 1,1-Bis(thioacyl)-2,2-diaminoethylenes to Dimethyl Acetylenedicarboxylate. 2. Structure Determination of Two Isomeric Spiroadducts by X-Ray Crystallography and of a Rearrangement Product by the 2D INADEQUATE Technique
Khan, Agha Zul-Qarnain,Sandstroem, Jan,Bergquist, Karl-Eric,Cheng, Chih-Yi,Wang, Sue-Lein
, p. 4919 - 4925 (2007/10/02)
1,3-Dialkyl-2-(4,4-dimethyl-2,6-dithioxocyclohexylidene)imidazolidines (twisted push-pull ethylenes) react smoothly with dimethyl acetylenedicarboxylate (DMAD) but require at least 3 equiv of DMAD for complete consumption.Chromatography of the complex rea