136028-18-7Relevant articles and documents
New Efficient Procedure for the Use of Diethoxyphosphoryl as a Protecting Group in the Synthesis of Polyazamacrocycles. Preparation of Polyazacyclophanes Derived from Resorcinol
Burguete, M. Isabel,Lopez-Diago, Laura,Garcia-Espana, Enrique,Galindo, Francisco,Luis, Santiago V.,Miravet, Juan F.,Sroczynski, Dariusz
, p. 10169 - 10171 (2003)
The synthesis of polyazamacrocycles containing an electron-rich aromatic subunit derived from resorcinol is described. The reported synthetic procedure is based on the use of diethoxyphosphoryl (Dep) as an amine protecting group. The new conditions employed for the cyclization reaction allow for a generalized use of Dep in the synthesis of polyazamacrocycles.