1360461-79-5Relevant academic research and scientific papers
Expeditious synthesis and single crystal structure of new pyrazole-fused 1,4-oxazine
Zheng, Liang-Wen,Zhao, Bao-Xiang,Liu, Ying-Rui
experimental part, p. 691 - 695 (2012/08/27)
A series of 2,6-diphenyl-4H-pyrazolo[5,1-c][1,4]oxazin-4-ones has been synthesized via a lactonization of 1-(2-oxo-2-phenylethyl)-3-phenyl-1H-pyrazole- 5-carboxylic acids in the presence of Ac2O at reflux temperature. The products were isolated by simple filtration in excellent yields and were characterized by IR, 1H-NMR, and HRMS. The molecular structure was confirmed by the X-ray crystal analysis of one compound that was prone to crystallization.
