1384975-44-3Relevant academic research and scientific papers
An amino-naphthol preparation method of compound
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Paragraph 0061; 0062; 0063; 0064, (2017/03/17)
The invention relates to a preparation method for aminonaphthol compound. The method includes the following steps: catalyst, aldehyde compound, secondary amine compound and naphthol are sequentially added into water and react under the temperature condition of 20 DEG C to 80 DEG C, and after reaction is complete, reaction liquid is obtained; the reaction liquid is sequentially extracted, dried, concentrated and separated by column chromatography according to the conventional method, so that product I or product II is obtained, and the structural formula of the product is shown in the figure. The preparation method has the advantages of mild conditions, short reaction time, simple post-processing, high yield and environment-friendliness, can realize mass production and has a good industrial application prospect.
Catalyst-free, one-pot, expeditious synthesis of aminoalkylnaphthols at room temperature
Mukhopadhyay, Chhanda,Rana, Sunil,Butcher, Ray J.
experimental part, p. 3077 - 3088 (2012/07/30)
Aminoalkylnaphthols possess several biological and catalytic activities. A methodology has been developed for the multicomponent one-pot synthesis of aminoalkylnaphthols in dichloromethane under catalyst-free conditions at room temperature. The present ap
