1394136-65-2Relevant academic research and scientific papers
Scalable synthesis of quaterrylene: Solution-phase 1H NMR spectroscopy of its oxidative dication
Thamatam, Rajesh,Skraba, Sarah L.,Johnson, Richard P.
, p. 9122 - 9124 (2013)
Quaterrylene is prepared in a single reaction and high yield by Scholl-type coupling of perylene, utilizing trifluoromethanesulfonic acid as catalyst and DDQ or molecular oxygen as oxidant. Dissolution in 1 M triflic acid/dichloroethane with sonication yields the aromatic quaterrylene oxidative dication, which is characterized by its 1H NMR spectrum.
