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14080-23-0

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2-Cyanopyrimidine
Cas No: 14080-23-0
No Data No Data Metric Ton/Day Changzhou Litong Chemical Co., Ltd. Contact Supplier
2-Cyanopyrimidine
Cas No: 14080-23-0
No Data 1 Gram 10 Metric Ton/Day Hangzhou KieRay Chem Co.,Ltd. Contact Supplier
2-Cyanopyrimidine Manufacturer/High quality/Best price/In stock
Cas No: 14080-23-0
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High purity 14080-23-0 2-Cyanopyrimidine
Cas No: 14080-23-0
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
High quality 2-Cyanopyrimidine supplier in China
Cas No: 14080-23-0
No Data No Data Metric Ton/Day Simagchem Corporation Contact Supplier
Good quality 2-Cyanopyrimidine manufacturer with GMP
Cas No: 14080-23-0
No Data 1 Kilogram 1 Metric Ton/Month Hangzhou Think Chemical Co. Ltd Contact Supplier
Factory Supply 2-Cyanopyrimidine
Cas No: 14080-23-0
No Data 1 1 Ality Chemical Corporation Contact Supplier
2-Cyanopyrimidine
Cas No: 14080-23-0
No Data 1 Kilogram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
2-Cyanopyrimidine
Cas No: 14080-23-0
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
2-Cyanopyrimidine
Cas No: 14080-23-0
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier

14080-23-0 Usage

Chemical Properties

White to yellow to brown solid
InChI:InChI=1/C5H3N3/c6-4-5-7-2-1-3-8-5/h1-3H

14080-23-0 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (646830)  2-Pyrimidinecarbonitrile  97% 14080-23-0 646830-5G 248.04CNY Detail
Aldrich (646830)  2-Pyrimidinecarbonitrile  97% 14080-23-0 646830-25G 748.80CNY Detail

14080-23-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-Cyanopyrimidine

1.2 Other means of identification

Product number -
Other names 2CPM

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:14080-23-0 SDS

14080-23-0Synthetic route

tetraethylammoniumcyanide
13435-20-6

tetraethylammoniumcyanide

N,N,N-trimethylpyrimidin-2-aminium chloride
14395-12-1

N,N,N-trimethylpyrimidin-2-aminium chloride

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.5h;93%
In dichloromethane for 0.5h; Ambient temperature;84%
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

sodium cyanide
143-33-9

sodium cyanide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In dimethyl sulfoxide; isopropyl alcohol at 30 - 35℃; for 5h;93%
In N,N-dimethyl-formamide at 60 - 70℃; for 24h;49%
With trimethylamine In N,N-dimethyl-formamide at 25℃; for 66h; Product distribution; Thermodynamic data; ΔH, E(a); var. catalysts, solvents and times;95 % Chromat.
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

dicyanozinc
557-21-1

dicyanozinc

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With racemic 2-di-tert-butylphosphino-1,1'-binaphthyl; palladium(II) trifluoroacetate; zinc In N,N-dimethyl acetamide at 80℃; for 6h;86.6%
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

sodium cyanide
773837-37-9

sodium cyanide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In water; dimethyl sulfoxide82%
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

potassium cyanide
151-50-8

potassium cyanide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; water In dimethyl sulfoxide at 20℃; for 48h;80%
With tetraethylammonium acetate In water; N,N-dimethyl-formamide at 90℃; for 48h;27%
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

potassium cyanide

potassium cyanide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With 3-quinuclidinol In dimethyl sulfoxide at 70℃; for 2.5h;71%
With 1,4-diaza-bicyclo[2.2.2]octane In water; dimethyl sulfoxide at 20℃; for 48h;65%
With 1,4-diaza-bicyclo[2.2.2]octane In dimethyl sulfoxide at 20℃; for 48h;
pyrimidine-2-diazonium o-benzenedisulfonimide

pyrimidine-2-diazonium o-benzenedisulfonimide

tetra-n-butylammonium cyanide
10442-39-4

tetra-n-butylammonium cyanide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
In acetonitrile at 22℃; for 1h; Sandmeyer Reaction;69%
pyrimidin-2-carbaldehyde oxime
39232-40-1

pyrimidin-2-carbaldehyde oxime

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With Burgess Reagent In dichloromethane at 25℃; for 2h; Dehydration;63%
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

trimethylamine
75-50-3

trimethylamine

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With benzene Erwaermen des Reaktionsprodukts mit KCN in Gegenwart von Acetamid;
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With sodium sulfite Erhitzen des Reaktionsprodukts mit KCN im Vakuum;
With 1,4-diaza-bicyclo[2.2.2]octane; sodium hydroxide In water; dimethyl sulfoxide
In water; dimethyl sulfoxide
pyrimidine-2-carboxamide
88511-48-2

pyrimidine-2-carboxamide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With trichlorophosphate
pyrimidine N-oxide
17043-94-6

pyrimidine N-oxide

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

A

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

B

Pyrimidine-4-carbonitrile
42839-04-3

Pyrimidine-4-carbonitrile

Conditions
ConditionsYield
With triethylamine In acetonitrile for 0.17h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
potassium cyanide
151-50-8

potassium cyanide

N,N,N-trimethylpyrimidin-2-aminium chloride
14395-12-1

N,N,N-trimethylpyrimidin-2-aminium chloride

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With tetramethlyammonium chloride In dichloromethane; water at 25℃; for 2h; Yield given;
5-bromo-pyrimidine-2-carboxylic acid amide
38275-60-4

5-bromo-pyrimidine-2-carboxylic acid amide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Raney nickel; ethanol; diethyl ether / Hydrogenation.Reagens 4:wss.Na2CO3
2: POCl3
View Scheme
methyl 5-bromo-2-pyrimidinecarboxylate
89581-38-4

methyl 5-bromo-2-pyrimidinecarboxylate

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: methanol; NH3
2: Raney nickel; ethanol; diethyl ether / Hydrogenation.Reagens 4:wss.Na2CO3
3: POCl3
View Scheme
sodium cyanide
773837-37-9

sodium cyanide

2-bromopyrimidine
4595-60-2

2-bromopyrimidine

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In dimethyl sulfoxide at 20℃; for 1h;
pyrimidine-2-carbothioamide
4537-73-9

pyrimidine-2-carbothioamide

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Conditions
ConditionsYield
With methylene blue; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 25℃; Sealed tube; Irradiation;25.7 mg
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

sodium methylate
124-41-4

sodium methylate

methyl ester of imino-pyrimidine acid
57871-18-8

methyl ester of imino-pyrimidine acid

Conditions
ConditionsYield
In methanol at 20℃; for 1h;100%
In methanol
In methanol at 20℃;
In methanol
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

pyrimidine-2-carboxamidine hydrochloride

pyrimidine-2-carboxamidine hydrochloride

Conditions
ConditionsYield
With sodium methylate; ammonium chloride In methanol at 20℃; for 18h;100%
Stage #1: 2-cyanopyrimidine With sodium methylate In methanol for 48h;
Stage #2: With ammonium chloride In methanol for 24h;
84%
Stage #1: 2-cyanopyrimidine With sodium methylate In methanol at 20℃; for 24h;
Stage #2: With ammonium chloride; acetic acid In methanol at 20℃; for 24h;
37.9%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

pyrimidine-2-carboximidohydrazide
1005-03-4

pyrimidine-2-carboximidohydrazide

Conditions
ConditionsYield
With hydrazine hydrate In ethanol at 20℃; for 2h;100%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

pyrimidine-2-carboxamide
88511-48-2

pyrimidine-2-carboxamide

Conditions
ConditionsYield
With manganese(IV) oxide; water In isopropyl alcohol at 100℃; under 5171.62 Torr; for 0.05h; Catalytic behavior; Temperature;99%
With cerium(IV) oxide; water at 30℃; for 3h;92%
With C14H30ClN3PRh; water at 100℃; for 1h; Catalytic behavior; Inert atmosphere; Schlenk technique;89%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

ethanol
64-17-5

ethanol

2-ethoxy pyrimidine
3739-82-0

2-ethoxy pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 2h;98%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-methyl-propan-1-ol
78-83-1

2-methyl-propan-1-ol

2-isobutoxypyrimidine
10132-13-5

2-isobutoxypyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 2h;98%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

4-Methylbenzyl alcohol
589-18-4

4-Methylbenzyl alcohol

2-[(4-methylbenzyl)oxy]pyrimidine

2-[(4-methylbenzyl)oxy]pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 4h;97%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-methylisothiourea sulphate
14527-26-5, 867-44-7

2-methylisothiourea sulphate

2-(methylsulfanyl)pyrimidine
823-09-6

2-(methylsulfanyl)pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 2h;97%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

S-cyclopropylmethylisothiourea hydrobromide
63667-17-4

S-cyclopropylmethylisothiourea hydrobromide

2-[(cyclopropylmethyl)thio]pyrimidine

2-[(cyclopropylmethyl)thio]pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 4h;97%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

benzyl alcohol
100-51-6

benzyl alcohol

2-(benzyloxy)pyrimidine
4214-64-6

2-(benzyloxy)pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 5h; Solvent; Reagent/catalyst; Temperature;96%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-phenylethanol
60-12-8

2-phenylethanol

2-phenethoxypyrimidine

2-phenethoxypyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 3h;96%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

Cyclopropylmethanol
2516-33-8

Cyclopropylmethanol

2-(cyclopropylmethoxy)pyrimidine

2-(cyclopropylmethoxy)pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 5h;96%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

C6H12N2S*BrH

C6H12N2S*BrH

2-[(cyclobutylmethyl)thio]pyrimidine

2-[(cyclobutylmethyl)thio]pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 4h;96%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-pent-4-enyl-isothiourea; hydrobromide

2-pent-4-enyl-isothiourea; hydrobromide

2-(pent-4-en-1-ylthio)pyrimidine

2-(pent-4-en-1-ylthio)pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 4h;96%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-(1H-tetrazol-5-yl)pyrimidine
13600-33-4

2-(1H-tetrazol-5-yl)pyrimidine

Conditions
ConditionsYield
With sodium azide; betaine; zinc(II) chloride In water at 20℃; for 20h;95%
With sodium azide; water; zinc(II) chloride at 25℃; for 24h; Micellar solution;88%
With sodium azide; zinc(II) chloride In water at 25℃; for 24h;88%
2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-aminomethylpyrimidine
75985-45-4

2-aminomethylpyrimidine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In ethanol under 760.051 Torr; for 12h; Inert atmosphere;95%
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In methanol; water at 20℃; for 3h;44%
With hydrogen; Pd-C; ammonia In ethanol
pyrrolidine
123-75-1

pyrrolidine

2-cyanopyrimidine
14080-23-0

2-cyanopyrimidine

2-(pyrrolidine-1-yl)pyrimidine
192197-34-5

2-(pyrrolidine-1-yl)pyrimidine

Conditions
ConditionsYield
With caesium carbonate In dimethyl sulfoxide at 80℃; for 5h;95%

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