1428127-20-1Relevant articles and documents
Microwave-assisted efficient one-pot synthesis of 9-phenyl-9,10- disilatriptycene and its bridgehead functionalization
Kuribara, Takayoshi,Ishida, Shintaro,Kudo, Takako,Kyushin, Soichiro
, p. 2092 - 2098 (2013/05/09)
9-Phenyl-9,10-disilatriptycene (2) was synthesized by the reaction of bis(2-bromophenyl)silane (1) with magnesium in THF. On conventional heating, 2 and cis-9,10-diphenyl-9,10-dihydro-9,10-disilaanthracene (cis-3) were obtained in 31% and 36% yields, resp