1450-19-7Relevant academic research and scientific papers
Disilane and preparation method thereof
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Paragraph 0074-0077, (2020/01/25)
The invention discloses disilane and a preparation method thereof. The preparation method of disilane includes: subjecting a uniformly mixed reaction system containing tertiary hydrosilane and a catalyst to dehydrogenation reaction at a temperature ranging from -10DEG C to 120DEG C to obtain disilane, wherein the catalyst comprises a silver salt. The invention also discloses the disilane preparedby the method. The method for preparation of the disilane by catalyzing tertiary silane dehydrogenation with the silver salt adopts the silver salt to activate the Si-H bond in the silane so as to realize construction of disilane. Therefore, the invention provides an efficient and simple method for preparation of the compound, and the application prospect is wide.
Die Chemie von Silylenoiden: Synthese und Reaktivitaet von (Alkoxysilyl)lithiumverbindungen
Tamao, Kohei,Kawachi, Atsushi
, p. 886 - 888 (2007/10/02)
Stichworte: Siliciumverbindungen * Silylenoide
