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149606-27-9

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Auristatin PEwith factory price
Cas No: 149606-27-9
No Data No Data 1 Wuhan Sun-shine Bio-technology Corporation Limited Contact Supplier
Auristatin PE
Cas No: 149606-27-9
No Data 1 Kilogram 100 Kilogram/Day HANGZHOU CLAP TECHNOLOGY CO,.LTD Contact Supplier
(2S)-2-[[(2S)-2-DIMETHYLAMINO-3-METHYL-BUTANOYL]AMINO]-N-[(3R,4S,5S)-3 -METHOXY-1-[(3R)-3-[(1R,2R)-1-METHOXY-2-(PHENETHYLCARBAMOYL)PROPYL]PYR ROLIDIN-1-YL]-5-METHYL-1-OXO-HEPTAN-4-YL]-N,3-DIMETHYL-BUT
Cas No: 149606-27-9
No Data No Data No Data Hangzhou Fandachem Co.,Ltd Contact Supplier
Soblitodin
Cas No: 149606-27-9
No Data No Data No Data Boc Sciences Contact Supplier
(2S)-2-[[(2S)-2-dimethylamino-3-methyl-butanoyl]amino]-N-[(3R,4S,5S)-3 -methoxy-1-[(3R)-3-[(1R,2R)-1-methoxy-2-(phenethylcarbamoyl)propyl]pyr rolidin-1-yl]-5-methyl-1-oxo-heptan-4-yl]-N,3-dimethyl-but
Cas No: 149606-27-9
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SOBLIDOTIN
Cas No: 149606-27-9
No Data No Data No Data Chemlyte Solutions Contact Supplier
Soblitodin
Cas No: 149606-27-9
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149606-27-9 Usage

InChI:InChI=1/C39H67N5O6/c1-13-27(6)35(43(10)39(48)33(25(2)3)41-38(47)34(26(4)5)42(8)9)31(49-11)24-32(45)44-23-17-20-30(44)36(50-12)28(7)37(46)40-22-21-29-18-15-14-16-19-29/h14-16,18-19,25-28,30-31,33-36H,13,17,20-24H2,1-12H3,(H,40,46)(H,41,47)/t27-,28+,30-,31+,33-,34-,35+,36+/m0/s1

149606-27-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name SOBLIDOTIN

1.2 Other means of identification

Product number -
Other names -

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:149606-27-9 SDS

149606-27-9Synthetic route

phenethylamine
64-04-0

phenethylamine

Dov-Val-Dil-Dap
163768-53-4

Dov-Val-Dil-Dap

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
With diethyl cyanophosphonate; triethylamine In N,N-dimethyl-formamide Yield given;
With triethylamine; diethyl cyano phosphate In DMF (N,N-dimethyl-formamide)
(3R,4S,5S)-4--3-methoxy-5-methylheptanoic acid
135383-56-1

(3R,4S,5S)-4--3-methoxy-5-methylheptanoic acid

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1: H2SO4 / CH2Cl2
2: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
3: 1,3-dicyclohexylcarbodiimide / CH2Cl2
4: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
5: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
6: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
7: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
8: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
9: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
tert-Butyl (3R,4S,5S)-3-methoxy-4--5-methylheptanoate
120205-58-5

tert-Butyl (3R,4S,5S)-3-methoxy-4--5-methylheptanoate

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
2: 1,3-dicyclohexylcarbodiimide / CH2Cl2
3: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
4: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
5: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
6: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
7: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
8: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
tert-Butyl (3R,4S,5S)-3-methoxy-4-(N-methylamino)-5-methylheptanoate
474645-22-2

tert-Butyl (3R,4S,5S)-3-methoxy-4-(N-methylamino)-5-methylheptanoate

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 1,3-dicyclohexylcarbodiimide / CH2Cl2
2: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
3: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
4: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
5: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
6: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
7: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
(3R,4S,5S)-tert-butyl 4-((S)-2-((S)-2-(dimethylamino)-3-methylbutanamido)-N,3-dimethylbutanamido)-3-methoxy-5-methylheptanoate
120205-53-0

(3R,4S,5S)-tert-butyl 4-((S)-2-((S)-2-(dimethylamino)-3-methylbutanamido)-N,3-dimethylbutanamido)-3-methoxy-5-methylheptanoate

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
2: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
3: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
4: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
tert-butyl (3R,4S,5S)-4-[(2S)-2-[[(benzyloxy)carbonyl]amino]-N,3-dimethylbutanamido]-3-methoxy-5-methylheptanoate
120205-52-9

tert-butyl (3R,4S,5S)-4-[(2S)-2-[[(benzyloxy)carbonyl]amino]-N,3-dimethylbutanamido]-3-methoxy-5-methylheptanoate

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
2: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
3: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
4: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
5: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
6: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
Dov-Val-Dil-Dap-OBzl
163768-52-3

Dov-Val-Dil-Dap-OBzl

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
2: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
(3R,4S,5S)-4-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-N,3-dimethylbutanamido]-3-methoxy-5-methylheptanoate
177423-00-6

(3R,4S,5S)-4-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-N,3-dimethylbutanamido]-3-methoxy-5-methylheptanoate

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
2: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
3: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
4: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
5: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
(3R,4S,5S)-4-(Benzyloxycarbonyl-methyl-amino)-3-methoxy-5-methyl-heptanoic acid methyl ester
149664-79-9

(3R,4S,5S)-4-(Benzyloxycarbonyl-methyl-amino)-3-methoxy-5-methyl-heptanoic acid methyl ester

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 10 steps
1: 1N aq. NaOH / dioxane / 3 h / Ambient temperature
2: H2SO4 / CH2Cl2
3: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
4: 1,3-dicyclohexylcarbodiimide / CH2Cl2
5: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
6: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
7: trifluoroacetic acid / CH2Cl2 / 1 h / Ambient temperature
8: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
9: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
10: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
(3R,4S,5S)-4-((S)-2-((S)-2-(dimethylamino)-3-methylbutanamido)-N,3-dimethylbutanamido)-3-methoxy-5-methylheptanoic acid
133120-89-5

(3R,4S,5S)-4-((S)-2-((S)-2-(dimethylamino)-3-methylbutanamido)-N,3-dimethylbutanamido)-3-methoxy-5-methylheptanoic acid

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: diethyl phosphorocyanidate, Et3N / dimethylformamide / a) 0 deg C, 2 h, b) RT, 16 h
2: H2 / 5percent Pd/C / 2-methyl-propan-2-ol; H2O / 2 h
3: diethyl phosphorocyanidate, Et3N / dimethylformamide
View Scheme
3-methoxy-2-methyl-N-phenethyl-3-pyrrolidin-2-yl-propionamide

3-methoxy-2-methyl-N-phenethyl-3-pyrrolidin-2-yl-propionamide

(3R,4S,5S)-4-((S)-2-((S)-2-(dimethylamino)-3-methylbutanamido)-N,3-dimethylbutanamido)-3-methoxy-5-methylheptanoic acid
133120-89-5

(3R,4S,5S)-4-((S)-2-((S)-2-(dimethylamino)-3-methylbutanamido)-N,3-dimethylbutanamido)-3-methoxy-5-methylheptanoic acid

TZT-1027
149606-27-9

TZT-1027

Conditions
ConditionsYield
With triethylamine; diethyl cyano phosphate In DMF (N,N-dimethyl-formamide)

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