15043-17-1

Basic information

• Product Name: 17-hydroxyspartein-2-one
• Synonyms: 17-hydroxylupanine;Lupanine, 17-hydroxy-
• CAS NO: 15043-17-1
• Molecular Formula: C₁₅H₂₄N₂O₂
• Molecular Weight: 264.3633
• Mol File: 15043-17-1.mol
• Article Data: 1

Chemical Properties

• Boiling Point: 445.3°C at 760 mmHg
• Flash Point: 223.1°C
• Density: 1.25g/cm³
• Vapor Pressure: 8.4E-10mmHg at 25°C
• Refractive Index: 1.603
• CAS DataBase Reference: 17-hydroxyspartein-2-one(CAS DataBase Reference)
• NIST Chemistry Reference: 17-hydroxyspartein-2-one(15043-17-1)
• EPA Substance Registry System: 17-hydroxyspartein-2-one(15043-17-1)

Safety Data

• Hazardous Substances Data: 15043-17-1(Hazardous Substances Data)

Upstream product

• 550-90-3 (+)-lupanine 

Relevant articles and documents

A stereostructural study of 17-hydroxylupanine and its perchlorate

The bisquinolizidine carbinolamine 17-hydroxylupanine was synthesized de novo from lupanine using 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; its structure was established by NMR techniques. The equatorial position of the hydroxy group as well as the prevailing boat form of ring C were determined. As expected, the carbinolamine converted into the C17=N16 anhydronium perchlorate upon treatment with HClO4. NMR analysis of the salt revealed a conformational equilibrium within rings A and D, whereas rings B and C remain rigid.