152419-80-2Relevant academic research and scientific papers
BIS(4-VINYLTHIOPHENYL) BRIDGE COMPOUNDS
Nesterov, V. V.,Tarasov, A. V.,Afonin, A. V.,Moskvichev, Yu. A.,Amosova, S. V.
, p. 1526 - 1530 (2007/10/02)
Bis(vinylthiophenyl) bridge compounds were obtained for the first time by the reaction of acetylene with di(4-mercaptophenyl) ether, di(4-mercaptophenyl) sulfide, 4,4'-dimercaptobiphenyl, and bis(4-mercaptophenyl)methane in DMSO.The effect of temperature on the product yield was investigated.An alternative preparative method is proposed for the synthesis of these compounds by the dehydrochlorination of the corresponding bis(2-chloroethylthiophenyl) compounds, produced by the quantitative reaction of the dithiols with 1,2-dichloroethane.
